Analysis of patulin in pear- and apple-based foodstuffs by liquid chromatography electrospray ionization tandem mass spectrometry

Journal of Agricultural and Food Chemistry

Volumn 59, Issue 14, 2011, Pages 7659-7665

  Desmarchelier, Aurelien ^a   Mujahid, Claudia ^a   Racault, Lucie ^a   Perring, Loïc ^a   Lancova, Katerina ^a  

^a NESTLÉ RESEARCH CENTER   (Switzerland)

Author keywords

isotope dilution; LC MS MS; liquid chromatography tandem mass spectrometry; Patulin; QuEChERS

Indexed keywords

ISOTOPE DILUTIONS; LC-MS/MS; LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY; PATULIN; QUECHERS;

ACETONITRILE; CEREAL PRODUCTS; CHROMATOGRAPHY; DAIRY PRODUCTS; ELECTROSPRAY IONIZATION; FRUIT JUICES; HIGH PRESSURE LIQUID CHROMATOGRAPHY; IONIZATION; ISOTOPES; LIQUIDS; MAGNESIUM; MASS SPECTROMETRY; SODIUM; SODIUM CHLORIDE; SODIUM SULFATE; SOLVENT EXTRACTION; SORPTION; WATER INJECTION;

FRUITS;

PATULIN;

APPLE; BABY FOOD; CHEMISTRY; CONFERENCE PAPER; ELECTROSPRAY MASS SPECTROMETRY; EVALUATION; FOOD CONTAMINATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOLATION AND PURIFICATION; METHODOLOGY; PEAR; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FOOD CONTAMINATION; INFANT FOOD; MALUS; PATULIN; PYRUS; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

MALUS X DOMESTICA; PYRUS;

EID: 79960577092     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf201461r     Document Type: Conference Paper

References (21)

1. Moake, M. M.; Padilla-Zakour, O. I.; Worobo, R. W. Comprehensive review of patulin control methods in foods Comp. Rev. Food Sci. Food Saf. 2005, 1, 8-21 (Pubitemid 44400591)
2. Barkai-Golan, R.; Paster, N. Regulations and limits for mycotoxins in fruits and vegetables. In Mycotoxins in Fruits and Vegetables, 1st ed.; Academic Press (Elsevier): San Diego, CA, 2008; pp 45-75.
3. Commission Regulation (EC) No. 1881/2006 of 19 December 2006 setting maximum levels for certain contaminants in foodstuffs. Off. J. Eur. Communities 2006, L 364, 5-24.
4. Shephard, G. S.; Legott, N. L. Chromatographic determination of the mycotoxin patulin in fruit and fruit juices J. Chromatogr., A 2000, 882, 17-22 (Pubitemid 30323693)
5. Katerere, D. R.; Stockenström, S. Determination of patulin in apple juice: comparative evaluation of four analytical methods J. AOAC Int. 2007, 90, 162-166 (Pubitemid 46786074)
6. Kawamoto, Y.; Bandoh, S.; Higashihara, K.; Miyagawa, H.; Goto, T. Development and single laboratory validation of a method for patulin determination in fruit juices World Mycotox. J. 2008, 1, 59-65
7. Eisele, T. A.; Gibson, M. Z. Syringe-cartridge solid phase extraction method for patulin in apple juice J. AOAC Int. 2003, 86, 1160-1163
8. 5-7 patulin as internal standard Food Chem. 2009, 115, 352-359
9. Rychlik, M.; Schieberle, P. Quantification of the mycotoxin patulin by a stable isotope dilution assay J. Agric. Food Chem. 1999, 47, 3749-3755 (Pubitemid 29449501)
10. Sewram, V.; Nair, J. J.; Nieuwoudt, T. W.; Leggott, N. L.; Shephard, G. S. Determination of patulin in apple juice by high-performance chromatography-atmospheric pressure chemical ionization mass spectrometry J. Chromatogr., A 2000, 897, 365-374
11. Katerere, D. R.; Stockenström, S.; Shephard, G. S. HPLC-DAD method for the determination of patulin in dried apple rings Food Control 2008, 19, 389-392 (Pubitemid 47576942)
12. Anastassiades, M.; Lehotay, S. J.; Stajnbaher, D.; Schenck, F. J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce J. AOAC Int. 2003, 86, 412-431
13. European Committee for Standardization (CEN), EN 15662:2008. Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method, 2008.
14. Lehotay, S. J. Determination of pesticide residues in foods by acetonitrile extraction and partitioning with magnesium sulfate: collaborative study J. AOAC Int. 2007, 90, 485-520 (Pubitemid 350067248)
15. Trebstein, A.; Lauber, U.; Humpf, H.-U. Analysis of fusarium toxins via HPLC-MS/MS multimethods: matrix effect and strategies for compensation Mycotoxin Res. 2009, 25, 201-213
16. Christensen, H. B.; Poulsen, M. E.; Rasmussen, P. H.; Christen, D. Development of an LC-MS/MS method for the determination of pesticides and patulin in apples Food Addit. Contam. 2009, 26, 1013-1023
17. Commission Decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and interpretation of results. Off. J. Eur. Communities 2002, L221, 8-36.
18. Accuracy (Trueness and Precision) of Measurement Methods and Results; Part 2: Basic Method for the Determination of Repeatability and Reproducibility of a Standard Measurement Method. ISO 5725-2; International Standards Organization: Geneva, Switzerland, 1994.
19. Rodriguez, M.; Orescan, D. B. Confirmation and quantitation of selected sulfonylurea, imidazolinone, and sulfonamide herbicides in surface water using electrospray LC/MS Anal. Chem. 1998, 70, 2710-2717
20. European Committee for Standardization (CEN), CEN/TR 16059:2010. Food analysis - performance criteria for single laboratory validated methods of analysis for the determination of mycotoxins. 2010.
21. Marìn, S.; Mateo, E. M.; Sanchis, V.; Valle-Algarra, F. M.; Ramos, A. J.; Jiménez, M. Patulin contamination in fruit derivatives, including baby food, from the spanish market Food Chem. 2011, 124, 563-568