Multiresidue analysis of organochlorine and pyrethroid pesticides in ground beef meat by gas chromatography-mass spectrometry

Journal of Environmental Science and Health - Part B Pesticides, Food Contaminants, and Agricultural Wastes

Volumn 44, Issue 4, 2009, Pages 350-356

  Stefanelli, Patrizia ^a   Santilio, Angela ^a   Cataldi, Lucilla ^a   Dommarco, Roberto ^a  

^a ISTITUTO SUPERIORE DI SANITÀ   (Italy)

Author keywords

Automated extraction; Mass spectrometry; Meat; Organochlorine; Pyrethroids

Indexed keywords

AUTOMATED EXTRACTION; CORRELATION COEFFICIENT; DETECTION LIMITS; FLORISIL; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GROUND BEEF; HEXACHLOROBENZENE; MARKET AREAS; MEAT SAMPLES; MULTI-RESIDUE ANALYSIS; MULTIRESIDUE METHOD; ORGANOCHLORINE; ORGANOCHLORINE PESTICIDES; PYRETHROID PESTICIDE; PYRETHROIDS; QUADRUPOLE MASS SPECTROMETRY; QUANTIFICATION LIMIT;

AUTOMATION; CHROMATOGRAPHIC ANALYSIS; ESTERS; GAS CHROMATOGRAPHY; LINEARIZATION; MASS SPECTROMETERS; MASS SPECTROMETRY; PESTICIDES; PROJECTILES; SOLVENT EXTRACTION; SPECTRUM ANALYSIS;

MEATS;

CHLORINATED HYDROCARBON; PESTICIDE; PESTICIDE RESIDUE; PYRETHROID;

GAS CHROMATOGRAPHY; HEXACHLOROBENZENE; MASS SPECTROMETRY; MEAT; ORGANOCHLORINE; PESTICIDE RESIDUE; PYRETHROID; SOLVENT;

ANIMAL; ARTICLE; CATTLE; CHEMISTRY; FOOD CONTAMINATION; MASS FRAGMENTOGRAPHY; MEAT; METHODOLOGY;

ANIMALS; CATTLE; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROCARBONS, CHLORINATED; MEAT; PESTICIDE RESIDUES; PESTICIDES; PYRETHRINS;

EID: 67649666905     PISSN: 03601234     EISSN: 15324109     Source Type: Journal    
DOI: 10.1080/03601230902801000     Document Type: Article

References (21)

1. European Commission. Commission Regulation (EC) 149/2008 of 29 January 2008 amending Regulation (EC) 396/2005 of the European Parliament and of the Council by establishing Annex II, III and IV setting maximum residue levels for products covered by Annex I thereto. Official Journal of the European Union L58/1 1.03.2008.
2. Garrido Frenich, A.; Martinez Vidal, J.L.; Cruz Sicilia, A.D.; Gonzalez Rodriguez, M.J.; Plaza Bonalos, P. Multiresidue analysis of organochlorine and organophosphorous pesticides in muscle of chicken, pork amd lamb by gas chromatography-triple quadrupole mass spectrometry. Analytica Chimica Acta 2006, 558, 42- 52.
3. Covaci, A.; Gheorghe, A.; Schepens, P. Distribution of organochlorine pesticides, polychlorinated biphenyls and α-HCH enanatiomers in pork tissues. Chemosphere 2004, 56, 757-766.
4. Lino, CM.; da Silveira, M.I.N. Extraction and clean-up methods for the determination of organochlorine pesticide residues in medicinal plants. J. Chromatogr. A1997, 769,275-283.
5. Manirakiza, P.; Covaci, A.; Schepens, P. Single step clean-up and GC-MS quantification of organochlorine pesticide residues in spice powder. Chromatographia 2000,52, 787-790.
6. Juhler, R.K. Supercritical fluid extraction of pesticides from meat: a systematic approach for optimisation. Analyst 1998, 123, 1551- 1556.
7. Lehotay, S.J.; Eller, K.I. Development of a method of analysis for 46 pesticides in fruit and vegetables by supercritical fluid extraction and gas chromatography/ion trap mass spectrometry. J. AOAC Int. 1995, 78, 821-830.
8. Nam, K.S.; King, W. Supercritical fluid extraction and enzyme immunoassay for pesticide detection in meat products. J. Agric. Food Chem. 1994,42,1469-1474.
9. Hopper, M.L. Automated one-step supercritical fluid extraction and clean-up system for the analysis of pesticide residues in fatty matrices. J. Chromatogr. A 1999,840, 93-105.
10. Pastor, A.; Vazquez, E.; Ciscar, R.; de la Guardia, M. Efficiency of the microwave-assisted extraction of hydrocarbons and pesticides from sediments. Anal. Chim. Acta 1997, 344, 241-249.
11. Adou, K.; Boutoyan, W.R.; Sweeney, P.J. Multiresidue method for the analysis of pesticide residues in fruits and vegetables by accelerated solvent extraction and capillary gas chromatography. J. of Agric food Chem. 2001,49,4153-4160.
12. Garrido-Frenich, A.; Romero-Gonzalez, R.; Martinez-Vidal, J.L.; Plaza-Bolanos, P.; Cuadros-Rodriguez, L.; Herrera-Abdo, M.A. Characterization of recovery profiles using gas chromatography- triple quadrupole mass spectrometry for the determination of pesticide residues in meat samples. J. Chromatogr. A 2006, 1133, 315-321.
13. Rimkus Gerhard, G.; Rummler, M.; Nausch, I. Gel permeation chromatography-high performance liquid chromatography combination as an automated clean-up technique for the multiresidue analysis of fats. J. Chromatogr. A, 1996, 737,9-14.
14. Attard Barbini, D.; Vanni, F.; Girolimetti, S.; Dommarco, R. Development of an analytical method for the determination of the residues of four pyrethroids in meat by GC-ECD and confirmation by GC-MS. Anal. Bioanal. Chem. 2007, 389, 1791- 1798.
15. Doong, R.; Lee, C. Determination of organochlorine pesticide residues in foods using solid-phase extraction clean-up cartridge. Analyst 1999,124, 1287-1289.
16. Pagliuca, G.; Gazzotti, T.; Zironi, E.; Sticca, P. Residue analysis of organophosphorous pesticides in animal matrices by dual column capillary gas chromatography with nitrose-phosphorous detection. J. Chromatogr. A 2005,1071, 67-70.
17. Schenck, F.J.; Donoghue, D.J. Determination of Organochlorine and organophosphorous pesticide residues in eggs using a solid phase extraction cleanup. J. Agric. Food Chem. 2000,48 (12), 6412- 6415.
18. Kodba, Z.C.; Voncina, D.B. A rapid method for the determination of organochlorine, pyrethroid pesticides and polychlorobiphenyls in fatty food using GC with electron capture detection. Chro- matographia 2007, 66, 619-624.
19. 18 cartridge. J. of Chromatography A 1997, 765, 61-68.
20. Park, J.W.; Abd El-Aty, A.M.; Lee, M.H.; Song, S.O.; Shim, J.H. Residue analysis of organophosphorous and organochlorine pesticides in fatty matrices by gas chromatography coupled with electron- capture detection. J. of Biosciences Section C. 2006, 61(5-6), 341- 346.
21. Di Muccio, A.; Pelosi, P.; Attard Barbini, D.; Generali, T.; Girolimetti, S.; Stefanelli, P.; Leonelli, A.; Amendola, G.; Vergori, L.; Fresquet, E.V. Determination of pyrethroid pesticide residues in fatty materials by solid-matrix dispersion partition, followed by mini-column size exclusion chromatography. J. of Chromatography A 1999,833,19-34.