Development of an analytical method for the determination of the residues of four pyrethroids in meat by GC-ECD and confirmation by GC-MS

Analytical and Bioanalytical Chemistry

Volumn 389, Issue 6, 2007, Pages 1791-1798

  Barbini, Danilo Attard ^a   Vanni, Fabiana ^a   Girolimetti, Silvana ^a   Dommarco, Roberto ^a  

^a ISTITUTO SUPERIORE DI SANITÀ   (Italy)

Author keywords

Beef meat; GC ECD; GC MS; Pesticides; Pyrethroid; Residues

Indexed keywords

ACETONE; CRUDE PETROLEUM; ETHERS; EXTRACTION; PESTICIDES; SOLVENTS;

BEEF MEAT; CLEAN-UP; ELECTRON CAPTURE DETECTORS; INSTRUMENTAL ANALYSIS; PYRETHROIDS;

MEATS;

ACETONE; ALKANE; INSECTICIDE; MAGNESIUM SILICATE; MAGNESIUM TRISILICATE; PYRETHROID; SOLVENT;

ANIMAL; ARTICLE; CALIBRATION; CHEMISTRY; FOOD CONTAMINATION; GAS CHROMATOGRAPHY; INSTRUMENTATION; MASS FRAGMENTOGRAPHY; MEAT; METHODOLOGY; NAPHTHA; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY;

ACETONE; ALKANES; ANIMALS; CALIBRATION; CHROMATOGRAPHY, GAS; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; INSECTICIDES; MAGNESIUM SILICATES; MEAT PRODUCTS; PYRETHRINS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLVENTS;

EID: 36849046183     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-007-1440-7     Document Type: Article

References (15)

1. Ministro della Salute (2004) Prodotti fitosanitari: limiti massimi di residui delle sostanze attive nei prodotti destinati all'alimentazione (D.M. 27 agosto 2004; G.U. n.292, 14 dicembre 2004). Ministro della Salute, Rome
2. Byford RL, Lockwood JA, Smith SM, Harmon CW, Johnson CC, Luther DG, Morris HF, Penny AJ (1986) Bull Environ Chem Toxicol 37:692-697
3. Sapiets A, Swaine H, Tandy MJ (1984) Cypermethrin. In: Zweig G, Sherma J (eds) Analytical methods for pesticides and plant growth regulators, vol XIII. Academic, Orlando, FL
4. Jacques A, Ong HL, Sheehan GW (1984) Cyhalothrin. In: Zweig G, Sherma J (eds) Analytical methods for pesticides and plant growth regulators, vol XIII. Academic, Orlando, FL
5. Papadopoulou-Mourkidou E (1993) The pyrethroid Insecticides. In: Sherma J, Cairns T (eds) Comprehensive analytical profiles of important pesticides. CRC Press, Boca Raton, FL
6. Kaushik N, Handa SK (1997) Chromatographia 46:209-212
7. Di Muccio A, Generali T, Attard Barbini D, Pelosi P, Ausili A, Vergori F, Girolimetti S (1997) J Chromatogr A 765:61-68
8. Di Muccio A, Stefanelli P, Funari E, Attard Barbini D, Generali T, Pelosi P, Girolimetti S, Amendola G, Vanni F, Di Muccio S (2002) Food Addit Contam 19:1148-1161
9. Lentza-Rizos C, Avramides EJ, Visi E (2001) J Chromatogr A 921:297-304
10. Argauer RJ, Eller KI, Pfeil RM, Brown RT (1997) J Agric Food Chem 45:180-184
11. Argauer RJ, Lehotay SJ, Brown RT (1997) J Agric Food Chem 45:3936-3939
12. Akre CJ, MacNeil JD (2006) J AOAC Int 89:1425-1431
13. AOAC (2006) Method 991.36. Official methods of analysis. Association of Official Analytical Chemists, Gaithersburg, MD
14. Di Muccio A, Ausili A, Vergori L, Camoni I, Dommarco R, Gambetti L (1990) Analyst 115:1167-1169
15. EC (2006) Quality control procedures for pesticide residues analysis (SANCO/10232/2006). European Community, Brussels