Method validation and comparison of acetonitrile and acetone extraction for the analysis of 169 pesticides in soya grain by liquid chromatography-tandem mass spectrometry

Journal of Chromatography A

Volumn 1216, Issue 21, 2009, Pages 4539-4552

  Pizzutti, Ionara R ^a   de Kok, André ^b   Hiemstra, Maurice ^b   Wickert, Cristine ^a   Prestes, Osmar D ^a  

^a FEDERAL UNIVERSITY OF SANTA MARIA   (Brazil)

^b National Reference Laboratory   (Netherlands)

Author keywords

Extraction; LC MS MS; Multi residue method; Pesticides; Soya grain

Indexed keywords

ACETONE EXTRACTIONS; CALIBRATION CURVES; COMPREHENSIVE STUDIES; DETECTION MODES; EXTRACTION METHODS; LC-MS/MS; LIMITS OF DETECTIONS; LIMITS OF QUANTIFICATIONS; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRIES; MAGNESIUM SULPHATE; MATRIX EFFECTS; MATRIXES; METHOD VALIDATIONS; MULTI-RESIDUE METHOD; PARTITIONING STEPS; RELATIVE STANDARD DEVIATIONS; ROUTINE ANALYSIS; SEVEN LEVELS; SIGNAL/NOISE RATIOS; SODIUM ACETATES; SOYA GRAIN;

ACETONE; ACETONITRILE; AGRICULTURAL CHEMICALS; BODY FLUIDS; CALIBRATION; CHROMATOGRAPHIC ANALYSIS; ELECTROSPRAY IONIZATION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIZATION OF GASES; LINEARIZATION; LIQUIDS; MAGNESIUM; MASS SPECTROMETERS; MASS SPECTROMETRY; METHANOL; PESTICIDES; RECOVERY; SEMICONDUCTOR SWITCHES; SODIUM; SPECTRUM ANALYSIS;

ORGANIC SOLVENTS;

ACETIC ACID; ACETONE; ACETONITRILE; MAGNESIUM SULFATE; METHANOL; PESTICIDE;

ACCURACY; ARTICLE; CALIBRATION; CONTROLLED STUDY; ELECTROSPRAY; EXTRACTION; INTERMETHOD COMPARISON; LIQUID CHROMATOGRAPHY; MASS FRAGMENTOGRAPHY; MASS SPECTROMETRY; NONHUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; SIGNAL NOISE RATIO; SOYBEAN; VALIDATION STUDY;

ACETONE; ACETONITRILES; CALIBRATION; CHROMATOGRAPHY, LIQUID; PESTICIDE RESIDUES; PESTICIDES; PLANT EXTRACTS; REPRODUCIBILITY OF RESULTS; SEEDS; SOYBEANS; TANDEM MASS SPECTROMETRY;

EID: 65249119734     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.03.064     Document Type: Article

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