Method validation for the analysis of 169 pesticides in soya grain, without clean up, by liquid chromatography-tandem mass spectrometry using positive and negative electrospray ionization

Journal of Chromatography A

Volumn 1142, Issue 2, 2007, Pages 123-136

  Pizzutti, Ionara R ^a   de Kok, André ^b   Zanella, Renato ^a   Adaime, Martha B ^a   Hiemstra, Maurice ^b   Wickert, Cristine ^a   Prestes, Osmar D ^a  

^a FEDERAL UNIVERSITY OF SANTA MARIA   (Brazil)

^b National Reference Laboratory   (Netherlands)

Author keywords

ESI ionization; LC MS MS; Multi residue method; Pesticides; Soya; Validation

Indexed keywords

GRAIN (AGRICULTURAL PRODUCT); IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

ESI IONIZATION; LC-MS/MS; MULTI RESIDUE METHOD; SOYA GRAINS; VALIDATION;

PESTICIDES;

ACETONE; DICHLOROMETHANE; METHANOL; PESTICIDE; PETROLEUM; SODIUM DIHYDROGEN PHOSPHATE; WATER;

ACCURACY; ARTICLE; CALIBRATION; CENTRIFUGATION; CONCENTRATION (PARAMETERS); ELECTROSPRAY; EVAPORATION; EXTRACTION; LIQUID CHROMATOGRAPHY; NONHUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SOYBEAN; TANDEM MASS SPECTROMETRY; VALIDATION STUDY;

CHROMATOGRAPHY, LIQUID; PESTICIDES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOYBEANS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

BIOCIDES; GRAIN; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETERS;

EID: 33846562415     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2006.12.030     Document Type: Article

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