Quantitative analysis of valiolamine through pre-column derivatization with phenylisocyanate using high-performance liquid chromatography with UV detection: Selection of reagent, identification of derivative and optimization of derivatization conditions

Journal of Pharmaceutical and Biomedical Analysis

Volumn 49, Issue 4, 2009, Pages 957-963

  Li, He ^a   Lee, Jae Ran ^a   Nguyen, Do Quynh Anh ^a   Kim, Sung Bae ^a   Seo, Yang Gon ^a   Chang, Yong Keun ^b   Hong, Soon Kwang ^c   Moon, Myung Hee ^b   Chung, In Young ^d   Kim, Chang Joon ^a  

^a Gyeongsang National University   (South Korea)

^b Korea Advanced Institute of Science and Technology (KAIST)   (South Korea)

^c Myong Ji University   (South Korea)

^d Kwangwoon University   (South Korea)

Author keywords

Derivatization; HPLC; Phenylisocyanate; UV detection; Valiolamine

Indexed keywords

1 FLUORO 2,4 DINITROBENZENE; 1 NAPHTHYL ISOTHIOCYANATE; AMINOCYCLITOL; DIMETHYL SULFOXIDE; PHENYL ISOCYANATE; TRIETHYLAMINE; UNCLASSIFIED DRUG; VALIENAMINE; VALIOLAMINE;

ACCURACY; AQUEOUS SOLUTION; ARTICLE; DERIVATIZATION; DRUG DETERMINATION; DRUG STABILITY; DRUG STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REACTION OPTIMIZATION; STANDARD; STREPTOMYCES HYGROSCOPICUS; THIN LAYER CHROMATOGRAPHY;

ANALYSIS OF VARIANCE; ANTI-BACTERIAL AGENTS; BACTERIA; BIOLOGICAL ASSAY; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, THIN LAYER; INDICATORS AND REAGENTS; INOSITOL; ISOCYANATES; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SOLVENTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; SPECTROPHOTOMETRY, ULTRAVIOLET; TEMPERATURE;

EID: 62949164447     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2009.02.020     Document Type: Article

References (53)

1. Shu Y.Z. J. Nat. Prod. 61 (1998) 1053-1071
2. Blidi L.E., Ahbala M., Bolte J., and Lemaire M. Tetrahedron Asymmetry 17 (2006) 2684-2688
3. Kameda Y.K., Asano N., Yoshikawa M., Takeuchi M., Yamaguchi T., and Matsui K. J. Antibiot. 37 (1984) 1301-1307
4. Asano N., Takeuchi M., Ninomiya K., Kameda Y., and Matsui K. J. Antibiot. 37 (1984) 859-867
5. Horii S., Fukase H., and Kameda Y. Carbohydr. Res. 140 (1985) 185-200
6. Ogawa S., Ohishi Y., Asada M., Tomoda A., Takahashi A., Ooki Y., Mori M., Itoh M., and Korenaga T. Org. Biomol. Chem. 2 (2004) 884-889
7. Ogawa S., and Kanto M. J. Nat. Prod. 70 (2007) 493-497
8. Sellier O., Van de Weghe P., Nouen D., Strehler C., and Eustache J. Tetrahedron Lett. 40 (1999) 853-856
9. Chen X., Fan Y., Zheng Y., and Shen Y. Chem. Rev. 103 (2003) 1955-1977
10. Mahmud T. Nat. Prod. Rep. 20 (2003) 137-166
11. Deng Z., and Bai L. Nat. Prod. Rep. 23 (2006) 811-827
12. Bai L., Li L., Xu H., Minagawa K., Yu Y., Zhang Y., Zhou X., Floss H.G., and Deng Z. Chem. Biol. 13 (2006) 387-397
13. Yu Y., Bai L., Minagawa K., Jian X., Li L., Li J., Chen S., Cao E., Mahmud T., Floss H.G., Zhou X., and Deng Z. Appl. Environ. Microbiol. 71 (2005) 5066-5076
14. Stead D.A. J. Chromatogr. B 747 (2005) 69-93
15. Chen X., Zheng Y., and Shen Y. J. Chromatogr. B 824 (2005) 341-347
16. Vermeij T.A.C., and Edelbroek P.M. J. Chromatogr. B 810 (2004) 297-303
17. Chollet D.F., Goumaz L., Juliano C., and Anderogg G. J Chromatogr. B 746 (2000) 311-314
18. Jiang Q., and Li S. J. Chromatogr. B 727 (1999) 119-123
19. Kijak P.J., Jackson J., and Shaikh B. J. Chromatogr. B 691 (1997) 377-382
20. Huang T.M., Deng C.H., Chen N.Z., Liu Z., and Duan G.L. J. Sep. Sci. 29 (2006) 2296-2302
21. Bahrami G., Mirzaeei S., Mohammadi B., and Kiani A. J. Chromatogr. B 822 (2005) 322-325
22. Jalalizadeh H., Souri E., Tehrani M.B., and Jahangiri A. J. Chromatogr. B 854 (2007) 43-47
23. Souri E., Jalalizadeh H., and Shafiee A. Chem. Pharm. Bull. 55 (2007) 1427-1430
24. Nicoli S., and Santi P. J. Pharm. Biomed. Anal. 41 (2006) 994-997
25. Zhou M., Wei G., Liu Y., Sun Y., Xiao S., Lu L., Liu C., and Zhong D. J. Chromatogr. B 798 (2003) 43-48
26. Isoherranen N., and Soback S. Clin. Chem. 46 (2000) 837-842
27. Lu J., Cwik M., and Kanyok T. J. Chromatogr. B 695 (1997) 329-335
28. Kim B.H., Lee S.C., Lee H.J., and Ok J.H. Biomed. Chromatogr. 17 (2003) 396-403
29. Kim B.H., Kim Y.K., and Ok J.H. J. Chromatogr. B 752 (2001) 173-177
30. Chen S.H., Liang Y.C., and Chou Y.W. J. Sep. Sci. 29 (2006) 607-612
31. Feng C.H., Lin S.J., Wu H.L., and Chen S.H. J. Chromatogr. B 780 (2002) 349-354
32. Tekko I.A., Bonner M.C., and Williams A.C. J. Pharm. Biomed. Anal. 41 (2006) 385-392
33. Aghazadeh-Habashi A., Sattari S., Pasutto F., and Jamali F. J. Pharm. Pharm. Sci. 5 (2002) 176-180
34. Liang Z.L., Leslie J., Adebowale A., Ashraf M., and Eddington N.D. J. Pharm. Biomed. Anal. 20 (1999) 807-814
35. Y.K. Kameda, S. Horii, US Patent 4,923,975 (1990).
36. Polson C., Sarkar P., Incledon B., Raguvaran V., and Grant R. J. Chromatogr. B 785 (2003) 263-275
37. Souverain S., Rudaz S., and Veuthey J.L. J. Pharm. Biomed. Anal. 35 (2004) 913-920
38. Chu W., Chan K.H., Jafvert C.T., and Chan Y.S. Chemosphere 69 (2007) 177-183
39. Sahasrabuddhey B., Jain A., and Verma K.K. Analyst 124 (1999) 1017-1021
40. Rakotomanga S., Baillet A., Pellerin F., and Baylocq-Ferrier D. Chromatographia 32 (1991) 125-129
41. Kameda Y., Asano N., Yoshikawa M., Takeuchi M., Yamaguchi T., and Matsui K. J. Antibiot. 37 (1984) 1301-1307
42. Drepper A., Peitzmann R., and Pape H. FEBS Lett. 388 (1996) 177-179
43. Chen S. Chromatographia 59 (2004) 697-703
44. Kleidernigg O.P., and Lindner W. Chromatographia 44 (1997) 465-472
45. Zhao S., Wang H., Zhang R., Tang L., and Liu Y.M. Electrophoresis 27 (2006) 3428-3433
46. Criado M.R., Torre S.P., Pereiro I.R., and Torrijos R.C. J. Chromatogr. A 1024 (2004) 155-163
47. Dunphy J.C., Pessler D.G., Morrall S.W., Evans K.A., Robaugh D.A., Fujimoto G., and Negahban A. Environ. Sci. Technol. 35 (2001) 1223-1230
48. El-Brashy A.M., and Al-Ghannam S.M. Analyst 122 (1999) 147-150
49. Sonnergaard J.M. Int. J. Pharm. 321 (2006) 12-17
50. Hadad G.M., El-Gindy A., and Mahmoud W.M.M. Chromatographia 66 (2007) 311-317
51. Kousoulos C., Tsatsou G., Dotsikas Y., Apostolou C., and Loukas Y.L. Biomed. Chromatogr. 22 (2008) 494-501
52. Box G.E.P., Hunter W.G., and Hunter J.S. Statistics for Experimenters: An Introduction to Design, Data analysis and Model Building (1978), John Wiley & Sons, New York
53. FDA. Guidance for industry bioanalytical method validation (2001), US Department of Health Services Food and Drug Administration