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Organic Letters

Volumn 10, Issue 11, 2008, Pages 2215-2218

Thiophene donor - Acceptor [2]rotaxanes

(4) Ikeda, Taichi a Higuchi, Masayoshi a Sato, Akira a Kurth, Dirk G a,b

a NATIONAL INSTITUTE FOR MATERIALS SCIENCE (Japan)

b MAX PLANCK INSTITUTE OF COLLOIDS AND INTERFACES (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 59849127550 PISSN: 15237060 EISSN: None Source Type: Journal
DOI: 10.1021/ol800624c Document Type: Article

Times cited : (23)

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32
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- The single crystals of the [2]rotaxane 2T-Rx·4PF 6 were grown by vapor diffusion of i-Pr2O into a MeCN solution of 2T-Rx·4PF6. Crystal data for [2T-Rx·4PF6·6MeCN, C72H 98N4O6S2Si2· 4PF6·6MeCN, M, 2062.07, triclinic, a, 11.323(4) Å, b, 11.942(4) Å, c, 20.512(7) Å, R, 91.128(5)°, β, 101.002(5)°, γ, 114.600(5)°, V, 2460.2(15) Å3, space group P1, Z, 1, rcalcd, 1.392 g cm-3, μ(Mo Kα, 2.43 cm-1, F(000, 826.0, T, 120 K, red plate crystal, 0.60 x 0.30 x 0.10 mm, R1, 0.0650, wR 2F2, 0.1648, goodness of fit, 1.045
- 2) = 0.1648, goodness of fit = 1.045.

33
- 59849089364
- The distance between the proton b of the thiophene unit and the centroid of the p-phenylene unit.
- The distance between the proton b of the thiophene unit and the centroid of the p-phenylene unit.

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