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1-ethoxyvinyl 2-furanoale has been used as an acylating agent to circumvent the intramolecular acylation by S. Akai, T. Naka, T. Fujita, Y. Takebe, T. Tsujino, Y. Kita, J. Org. Chem. 2002, 67, 411.
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43
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33846451033
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For representative examples see a
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For representative examples see a) S. Canova, V. Bellosta, A. Bigot, P. Mailliet, S. Mignani, J. Cossy. Org. Lett. 2007, 9, 145;
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53849087731
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An added benefit of toluene as the reaction solvent was realized upon completion of the reaction, in which the crude reaction mixture could directly be poured onto silica gel. thus, obviating the need for a workup procedure. This not only enhances the practicality of the procedure but also allows for the complete recovery of starting diols; many of which have high solubilities in aqueous media
-
An added benefit of toluene as the reaction solvent was realized upon completion of the reaction, in which the crude reaction mixture could directly be poured onto silica gel. thus, obviating the need for a workup procedure. This not only enhances the practicality of the procedure but also allows for the complete recovery of starting diols; many of which have high solubilities in aqueous media.
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53849088460
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Currently available from Aldrich, CAS No. 325006. costs US$46.30/gram for both enantiomers.
-
Currently available from Aldrich, CAS No. 325006. costs US$46.30/gram for both enantiomers.
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58
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53549123528
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For nitrile see a
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For nitrile see a) E. de Lemos, F.-H. Poree, A. Commercon, J.-F. Betzer, A. Pancrazi, J. Ardisson, Angew. Chem. 2007, 119, 1949;
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61
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For azide see
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c) For azide see K. Sahasrabudhe, V. Gracias, K. Furness, B. T. Smith, C. E. Katz, D. S. Reddy, J. Aubé, J. Am. Chem. Soc. 2003, 125, 7914.
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0037055060
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For representative examples see
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For representative examples see B. M. Trost, Z. T. Ball, T. Joge, J. Am. Chem. Soc. 2002, 124, 7922.
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For representative examples see a
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For representative examples see a) B. M. Trost, M. R. Machacek, Z. T. Ball, Org. Lett. 2003, 5, 1895;
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For representative examples see a
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For representative examples see a) B. M. Trost, Z. T. Ball, K. M. Laemmerhold, J. Am. Chem. Soc. 2005, 127, 10028;
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8444241745
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53849134386
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The majority of examples currently in the literature have acetyl groups
-
The majority of examples currently in the literature have acetyl groups.
-
-
-
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71
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1842505068
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For an example in which only one enantiomer can be accessed in high enantioselectivity with enzymatic desymmerization see D. B. Kastrinsky, D. L. Boger, J. Org. Chem. 2004, 69, 2284
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For an example in which only one enantiomer can be accessed in high enantioselectivity with enzymatic desymmerization see D. B. Kastrinsky, D. L. Boger, J. Org. Chem. 2004, 69, 2284.
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