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Volumn 10, Issue 4, 2008, Pages 517-520

Synthesis of substituted benzofurans via microwave-enhanced catch and release strategy

Author keywords

[No Author keywords available]

Indexed keywords

BENZOFURAN DERIVATIVE; BROMINE DERIVATIVE;

EID: 49049108318     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc8000162     Document Type: Article
Times cited : (25)

References (74)
  • 31
  • 67
    • 0041461964 scopus 로고    scopus 로고
    • For reviews on microwave-assisted combinatorial chemistry, see: a
    • For reviews on microwave-assisted combinatorial chemistry, see: (a) Lew, A.; Krutzik, P. O.; Hart, M. E.; Chamberlin, A. R. J. Comb. Chem. 2002, 4, 95-105.
    • (2002) J. Comb. Chem , vol.4 , pp. 95-105
    • Lew, A.1    Krutzik, P.O.2    Hart, M.E.3    Chamberlin, A.R.4
  • 69
    • 49049092734 scopus 로고    scopus 로고
    • The MW experiments were performed in a self-tuning single mode CEM Discover Focused Synthesizer apparatus. The instrument continuously adjusted the applied wattage to maintain the desired temperature
    • The MW experiments were performed in a self-tuning single mode CEM Discover Focused Synthesizer apparatus. The instrument continuously adjusted the applied wattage to maintain the desired temperature.
  • 71
    • 49049111520 scopus 로고    scopus 로고
    • We noted that the bromides darkened after about half an hour from recovery. It is however known that (halomethyl) phenols are chemically unstable and irritant compounds. Chauhan, M. S.; Dean, F. M.; McDonald, S.; Robinson, M. S. J. Chem. Soc., Perkin Trans. 1 1973, 35, 9-363.
    • We noted that the bromides darkened after about half an hour from recovery. It is however known that (halomethyl) phenols are chemically unstable and irritant compounds. Chauhan, M. S.; Dean, F. M.; McDonald, S.; Robinson, M. S. J. Chem. Soc., Perkin Trans. 1 1973, 35, 9-363.
  • 72
    • 0033063092 scopus 로고    scopus 로고
    • 4 in THF according to literature in 80% yield. However, the regenerated resin is less efficient than the original and the yields are lowered. Sieber, F.; Wentworth Jr., P.; Toker, J. D.; Wentworth, A. D.; Metz, W. A.; Reed, N. N.; Janda, K. D. J. Org. Chem. 1999, 64, 5188-5192.
    • 4 in THF according to literature in 80% yield. However, the regenerated resin is less efficient than the original and the yields are lowered. Sieber, F.; Wentworth Jr., P.; Toker, J. D.; Wentworth, A. D.; Metz, W. A.; Reed, N. N.; Janda, K. D. J. Org. Chem. 1999, 64, 5188-5192.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.