메뉴 건너뛰기




Volumn 215, Issue 2, 2004, Pages 191-202

Development of a new analytical electron microscopy technique to quantify the chemistry of planar defects and to measure accurately solute segregation to grain boundaries

Author keywords

Electron energy loss spectroscopy (EELS); Energy dispersive X ray spectroscopy (EDXS); Grain boundary segregation; Interfaces; Microanalysis; Planar defects; Solute segregation; Transmission electron microscopy (TEM)

Indexed keywords

DISSOCIATION; ELECTRON ENERGY LEVELS; ELECTRON SCATTERING; ELECTRONS; ENERGY DISPERSIVE SPECTROSCOPY; ENERGY DISSIPATION; GRAIN BOUNDARIES; HIGH RESOLUTION TRANSMISSION ELECTRON MICROSCOPY; PROBES; SEGREGATION (METALLOGRAPHY); SOLUBILITY; STACKING FAULTS;

EID: 4344564837     PISSN: 00222720     EISSN: None     Source Type: Journal    
DOI: 10.1111/j.0022-2720.2004.01359.x     Document Type: Article
Times cited : (19)

References (43)
  • 1
    • 0343052722 scopus 로고    scopus 로고
    • Improved quantification of grain boundary segregation by EDS in a dedicated STEM
    • Alber, U., Müllejans, H. & Kühle, M. (1997) Improved quantification of grain boundary segregation by EDS in a dedicated STEM. Ultramicroscopy, 69, 105-116.
    • (1997) Ultramicroscopy , vol.69 , pp. 105-116
    • Alber, U.1    Müllejans, H.2    Kühle, M.3
  • 2
    • 84953078524 scopus 로고
    • Detection of nitrogen at (100) platelets in a type IaA/B diamond
    • Bruley, J. (1992) Detection of nitrogen at (100) platelets in a type IaA/B diamond. Philos. Mag. Lett. 66, 47-56.
    • (1992) Philos. Mag. Lett. , vol.66 , pp. 47-56
    • Bruley, J.1
  • 3
    • 0024611295 scopus 로고
    • Quantitative electro energy-loss spectroscopy microanalysis of platelet and voidite defects in natural diamond
    • Bruley, J. & Brown, L.M. (1989) Quantitative electro energy-loss spectroscopy microanalysis of platelet and voidite defects in natural diamond. Philos. Mag. A, 59, 247-261.
    • (1989) Philos. Mag. A , vol.59 , pp. 247-261
    • Bruley, J.1    Brown, L.M.2
  • 4
    • 0001126304 scopus 로고
    • Chemistry of basal-plane defects in zinc oxide - Antimony oxide (0.1 mol-%) ceramics
    • Bruley, J., Bremer, U. & Krasevec, V. (1992) Chemistry of basal-plane defects in zinc oxide - antimony oxide (0.1 mol-%) ceramics. J. Am. Ceram. Soc. 75, 3127-3128.
    • (1992) J. Am. Ceram. Soc. , vol.75 , pp. 3127-3128
    • Bruley, J.1    Bremer, U.2    Krasevec, V.3
  • 5
    • 0033204809 scopus 로고    scopus 로고
    • Scanning transmission electron microscopy analysis of grain boundaries in creep-resistant yttrium- and lanthanum-doped alumina microstructures
    • Bruley, J., Cho, J., Chan, H.M., Harmer, M.P. & Rickman, J.M. (1999) Scanning transmission electron microscopy analysis of grain boundaries in creep-resistant yttrium- and lanthanum-doped alumina microstructures. J. Am. Ceram Soc. 82, 2865-2870.
    • (1999) J. Am. Ceram Soc. , vol.82 , pp. 2865-2870
    • Bruley, J.1    Cho, J.2    Chan, H.M.3    Harmer, M.P.4    Rickman, J.M.5
  • 6
    • 0028515505 scopus 로고
    • Recent attempts to detect magnesium in a heavily doped sapphire bicrystal by spatially resolved electron energy-loss spectroscopy
    • Bruley, J., Höche, T., Kleebe, H.J. & Rühle, M. (1994) Recent attempts to detect magnesium in a heavily doped sapphire bicrystal by spatially resolved electron energy-loss spectroscopy. J. Am. Ceram. Soc. 77, 2273-2276.
    • (1994) J. Am. Ceram. Soc. , vol.77 , pp. 2273-2276
    • Bruley, J.1    Höche, T.2    Kleebe, H.J.3    Rühle, M.4
  • 8
    • 85167476713 scopus 로고
    • Study of electron beam spreading as a result of multiple small-angle scattering
    • Center, R.E. (1968) Study of electron beam spreading as a result of multiple small-angle scattering. Bull. Am. Phys. Soc. 13, 1586.
    • (1968) Bull. Am. Phys. Soc. , vol.13 , pp. 1586
    • Center, R.E.1
  • 10
    • 0346197289 scopus 로고    scopus 로고
    • Application of a new method for measuring small amounts of dopants at planar faults: Tin-rich inversion boundaries in zinc oxide
    • ed. by R. Cross, J. Engelbrecht, T. Sewell and M. Witcomb, Microscopy Society of Southern Africa, Onderstepoort
    • Daneu, N., Walther, T. & Recnik, A. (2002) Application of a new method for measuring small amounts of dopants at planar faults: tin-rich inversion boundaries in zinc oxide. Proceedings of the 15th International Cong. Electron Microsc., Durban, 3 (ed. by R. Cross, J. Engelbrecht, T. Sewell and M. Witcomb), pp. 63-64. Microscopy Society of Southern Africa, Onderstepoort.
    • (2002) Proceedings of the 15th International Cong. Electron Microsc., Durban , vol.3 , pp. 63-64
    • Daneu, N.1    Walther, T.2    Recnik, A.3
  • 11
    • 0019013744 scopus 로고
    • The spatial resolution of X-ray microanalysis in the scanning transmission electron microscope
    • Doig, P., Lonsdale, D. & Flewitt, P.E.J. (1980) The spatial resolution of X-ray microanalysis in the scanning transmission electron microscope. Philos. Mag, A, 41, 761-775.
    • (1980) Philos. Mag, A , vol.41 , pp. 761-775
    • Doig, P.1    Lonsdale, D.2    Flewitt, P.E.J.3
  • 14
    • 0031998238 scopus 로고    scopus 로고
    • Composition and chemical width of ultrathin amorphous films at grain boundaries in silicon nitride
    • Gu, H., Cannon, R.M. & Rühle, M. (1998) Composition and chemical width of ultrathin amorphous films at grain boundaries in silicon nitride. J. Mater. Res. 13, 376-387.
    • (1998) J. Mater. Res. , vol.13 , pp. 376-387
    • Gu, H.1    Cannon, R.M.2    Rühle, M.3
  • 15
    • 0029150094 scopus 로고
    • A quantitative approach for spatially resolved electron energy-loss spectroscopy of grain boundaries and planar defects on a subnanometer scale
    • Gu, H., Ceh, M., Stemmer, S., Müllejans, H. & Rühle, M. (1995) A quantitative approach for spatially resolved electron energy-loss spectroscopy of grain boundaries and planar defects on a subnanometer scale. Ultramicroscopy, 59, 215-227.
    • (1995) Ultramicroscopy , vol.59 , pp. 215-227
    • Gu, H.1    Ceh, M.2    Stemmer, S.3    Müllejans, H.4    Rühle, M.5
  • 16
    • 0027545078 scopus 로고
    • Annular dark-field imaging - Resolution and thickness effects
    • Hillyard, S. & Silcox, J. (1993a) Annular dark-field imaging - resolution and thickness effects. Ultramicroscopy, 49, 14-25.
    • (1993) Ultramicroscopy , vol.49 , pp. 14-25
    • Hillyard, S.1    Silcox, J.2
  • 17
    • 0027753682 scopus 로고
    • Thickness effects in ADF STEM zone-axis images
    • Hillyard, S. & Silcox, J. (1993b) Thickness effects in ADF STEM zone-axis images. Ultramicroscopy, 52, 325-334.
    • (1993) Ultramicroscopy , vol.52 , pp. 325-334
    • Hillyard, S.1    Silcox, J.2
  • 18
    • 0038105595 scopus 로고
    • Grain boundary activity measurements by Auger electron spectroscopy
    • Hondros, E.D. & Seah, M.P. (1972) Grain boundary activity measurements by Auger electron spectroscopy. Scripta Metall. 6, 1007-1012.
    • (1972) Scripta Metall. , vol.6 , pp. 1007-1012
    • Hondros, E.D.1    Seah, M.P.2
  • 20
    • 0018407566 scopus 로고
    • Electron-beam induced damage of organic solids - Implications for analytical electron microscopy
    • Isaacson, M. (1979) Electron-beam induced damage of organic solids - implications for analytical electron microscopy. Ultramicroscopy, 4, 193-199.
    • (1979) Ultramicroscopy , vol.4 , pp. 193-199
    • Isaacson, M.1
  • 21
    • 0009275622 scopus 로고    scopus 로고
    • Atomic-scale study of a transition phase precipitate and its interfacial chemistry in an Fe-15at%Mo-5at%V alloy
    • Isheim, D., Hellman, O.C., Seidman, D.N., Danoix, F., Bostel, A. & Blavette, D. (2001) Atomic-scale study of a transition phase precipitate and its interfacial chemistry in an Fe-15at%Mo-5at%V alloy. Microsc. Microanal. 7, 424-434.
    • (2001) Microsc. Microanal. , vol.7 , pp. 424-434
    • Isheim, D.1    Hellman, O.C.2    Seidman, D.N.3    Danoix, F.4    Bostel, A.5    Blavette, D.6
  • 22
    • 3543051746 scopus 로고    scopus 로고
    • Investigations of grain boundary embrittlement in the STEM
    • ed. by J. M. Rodenburg, Conference Series 153. Institute of Physics, Bristol
    • Keast, V.J. & Williams, D.B. (1997) Investigations of grain boundary embrittlement in the STEM. Proceedings of the EMAG 97, Cambridge (ed. by J. M. Rodenburg), pp. 299-302. Conference Series 153. Institute of Physics, Bristol.
    • (1997) Proceedings of the EMAG 97, Cambridge , pp. 299-302
    • Keast, V.J.1    Williams, D.B.2
  • 23
    • 0033349222 scopus 로고    scopus 로고
    • Quantitative compositional mapping of Bi segregation to grain boundaries in Cu
    • Keast, V.J. & Williams, D.B. (1999) Quantitative compositional mapping of Bi segregation to grain boundaries in Cu. Acta Mater. 47, 3999-4008.
    • (1999) Acta Mater. , vol.47 , pp. 3999-4008
    • Keast, V.J.1    Williams, D.B.2
  • 24
    • 0033921025 scopus 로고    scopus 로고
    • Quantification of boundary segregation in the analytical electron microscope
    • Keast, V.J. & Williams, D.B. (2000) Quantification of boundary segregation in the analytical electron microscope. J. Microsc. 199, 45-55.
    • (2000) J. Microsc. , vol.199 , pp. 45-55
    • Keast, V.J.1    Williams, D.B.2
  • 26
    • 0028420261 scopus 로고
    • Improvements in detection sensitivity by spatial difference electron energy-loss spectroscopy at interfaces in ceramics
    • Müllejans, H. & Bruley, J. (1994) Improvements in detection sensitivity by spatial difference electron energy-loss spectroscopy at interfaces in ceramics. Ultramicroscopy, 53, 351-360.
    • (1994) Ultramicroscopy , vol.53 , pp. 351-360
    • Müllejans, H.1    Bruley, J.2
  • 27
    • 0029610920 scopus 로고
    • Segregation-induced hole drilling at grain boundaries
    • Ozkaya, D., Yuan, J., Brown. L.M. & Flewitt, P.E.J. (1995) Segregation-induced hole drilling at grain boundaries. J. Microsc. 180, 300-306.
    • (1995) J. Microsc. , vol.180 , pp. 300-306
    • Ozkaya, D.1    Yuan, J.2    Brown, L.M.3    Flewitt, P.E.J.4
  • 28
    • 0034893839 scopus 로고    scopus 로고
    • Polytype induced exaggerated grain growth in ceramics
    • Recnik. A., Ceh, M. & Kolar, D. (2001a) Polytype induced exaggerated grain growth in ceramics. J. Eur. Ceram. Soc. 21, 2117-2121.
    • (2001) J. Eur. Ceram. Soc. , vol.21 , pp. 2117-2121
    • Recnik, A.1    Ceh, M.2    Kolar, D.3
  • 29
    • 0035526627 scopus 로고    scopus 로고
    • Structure and chemistry of basal-plane inversion boundaries in antimony oxide-doped zinc oxide
    • Recnik, A., Daneu, N., Walther, T. & Mader, W. (2001b) Structure and chemistry of basal-plane inversion boundaries in antimony oxide-doped zinc oxide. J. Am. Ceram. Soc. 84, 2657-2668.
    • (2001) J. Am. Ceram. Soc. , vol.84 , pp. 2657-2668
    • Recnik, A.1    Daneu, N.2    Walther, T.3    Mader, W.4
  • 30
    • 0001062997 scopus 로고
    • The single-scattering model and spatial resolution in X-ray analysis of thin foils
    • Reed, S.J.B. (1982) The single-scattering model and spatial resolution in X-ray analysis of thin foils. Ultramicroscopy, 7, 405-409.
    • (1982) Ultramicroscopy , vol.7 , pp. 405-409
    • Reed, S.J.B.1
  • 31
    • 0018259094 scopus 로고
    • Effect of solute misfit and temperature on irradiation-induced segregation in binary Ni alloys
    • Rehn, L.E., Okamoto, P.R., Potter, D.I. & Wiedersich, H. (1978) Effect of solute misfit and temperature on irradiation-induced segregation in binary Ni alloys. J. Nucl. Mater. 74, 242-251.
    • (1978) J. Nucl. Mater. , vol.74 , pp. 242-251
    • Rehn, L.E.1    Okamoto, P.R.2    Potter, D.I.3    Wiedersich, H.4
  • 34
    • 0029780178 scopus 로고    scopus 로고
    • Atomic scale studies of silver segregation at {222}MgO/Cu heterophase interfaces
    • Shashkov, D.A. & Seidman, D.N. (1996) Atomic scale studies of silver segregation at {222}MgO/Cu heterophase interfaces. Mater. Sci. Forum. 207, 429-432.
    • (1996) Mater. Sci. Forum. , vol.207 , pp. 429-432
    • Shashkov, D.A.1    Seidman, D.N.2
  • 35
    • 0033353140 scopus 로고    scopus 로고
    • Atomic-scale structure and chemistry of ceramic/metal interfaces - II. Solute segregation at MgO/Cu (Ag) and CdO/Ag (Au) interfaces
    • Shashkov, D.A., Muller, D.A. & Seidman, D.N. (1999) Atomic-scale structure and chemistry of ceramic/metal interfaces - II. Solute segregation at MgO/Cu (Ag) and CdO/Ag (Au) interfaces. Acta Mater. 47, 3953-3963.
    • (1999) Acta Mater. , vol.47 , pp. 3953-3963
    • Shashkov, D.A.1    Muller, D.A.2    Seidman, D.N.3
  • 36
    • 0027670012 scopus 로고
    • Coherence and multiple scattering in Z-contrast images
    • Treacy, M.M.J. & Gibson, J.M. (1993) Coherence and multiple scattering in Z-contrast images. Ultramicroscopy, 52, 31-53.
    • (1993) Ultramicroscopy , vol.52 , pp. 31-53
    • Treacy, M.M.J.1    Gibson, J.M.2
  • 37
    • 0033079349 scopus 로고    scopus 로고
    • A quantitative study of compositional profiles of chemical vapour-deposited strained silicon-germanium/ silicon layers by transmission electron microscopy
    • Walther, T. & Humphreys, C.J. (1999) A quantitative study of compositional profiles of chemical vapour-deposited strained silicon-germanium/ silicon layers by transmission electron microscopy. J. Cryst. Growth. 197, 113-128.
    • (1999) J. Cryst. Growth. , vol.197 , pp. 113-128
    • Walther, T.1    Humphreys, C.J.2
  • 38
    • 3543065369 scopus 로고    scopus 로고
    • A new method to measure small amounts of solute atoms on planar defects and application to inversion domain boundaries in doped zinc oxide
    • Proceedings Europ. Conference Structure and Composition of Interfaces in Solids. Kloster Irsee, Germany, August 2002
    • Walther, T., Daneu, N. & Recnik, A. (2004) A new method to measure small amounts of solute atoms on planar defects and application to inversion domain boundaries in doped zinc oxide. Proceedings Europ. Conference Structure and Composition of Interfaces in Solids. Kloster Irsee, Germany, August 2002. Interface Sci. 12, 267-275.
    • (2004) Interface Sci. , vol.12 , pp. 267-275
    • Walther, T.1    Daneu, N.2    Recnik, A.3
  • 39
    • 0346197288 scopus 로고    scopus 로고
    • Test of a new analytical method to measure the composition of a planar fault
    • ed. by R. Cross, J. Engelbrecht and M. Witcomb, Microscopy Society of Southern Africa, Onderstepoort
    • Walther, T., Recnik, A. & Daneu, N. (2002) Test of a new analytical method to measure the composition of a planar fault. Proceedings of the 15th International Cong. Electron Microsc., Durban, 1 (ed. by R. Cross, J. Engelbrecht and M. Witcomb), pp. 535-536. Microscopy Society of Southern Africa, Onderstepoort.
    • (2002) Proceedings of the 15th International Cong. Electron Microsc., Durban , vol.1 , pp. 535-536
    • Walther, T.1    Recnik, A.2    Daneu, N.3
  • 40
    • 0033171751 scopus 로고    scopus 로고
    • Relationship between electrical activity and grain boundary structural configuration in polycrystalline silicon
    • Wang, Z.J., Tsurekawa, S., Ikeda, K., Sekiguchi, T. & Watanabe, T. (1999) Relationship between electrical activity and grain boundary structural configuration in polycrystalline silicon. Interface Sci. 7, 197-205.
    • (1999) Interface Sci. , vol.7 , pp. 197-205
    • Wang, Z.J.1    Tsurekawa, S.2    Ikeda, K.3    Sekiguchi, T.4    Watanabe, T.5
  • 41
    • 0242443288 scopus 로고    scopus 로고
    • Quantification of elemental segregation to lath and grain boundaries in low-alloy steel by STEM X-ray mapping combined with the ξ-factor method
    • Watanabe, M. & Williams, D.B. (2003) Quantification of elemental segregation to lath and grain boundaries in low-alloy steel by STEM X-ray mapping combined with the ξ-factor method. Z. Metallkd. 94, 307-316.
    • (2003) Z. Metallkd. , vol.94 , pp. 307-316
    • Watanabe, M.1    Williams, D.B.2
  • 43


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.