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16CuPc films to determine their film thickness.
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18
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84906414086
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note
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2 roughness as determined by AFM was 3.2 A for maximal scanned areas of 3 μm × 3 μm. This is in rather good agreement with the reflectivity data. The slight discrepancy is most likely due to the fact that AFM averages over a much smaller area (micrometers in AFM versus millimeters in X-ray reflectivity) and to the size effect of the tip.
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The values obtained by X-ray reflectivity are 12.6 ±1.6, 14.8 ± 0.8, 21.4 ± 2.5 A for the first, second, and third layers, respectively. The value for the third layer (almost unrealistic) has a large uncertainty due to its low partial coverage.
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21
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84906399694
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note
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The mean lateral domain sizes obtained from GIXD are smaller than the mean island lengths observed with AFM. This difference can be due to the existence of multiple domains inside an island or to the fact that the in-plane Bragg reflection simply does not correspond to the crystallographic direction along which the crystallite elongation takes place.
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23
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84906399695
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note
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The total coverage occupied by the interfacial layer, as deduced from the electronic density and height, is 4 Å.
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