Primary and secondary phosphane complexes of metalloporphyrins: Isolation, spectroscopy, and X-ray crystal structures of ruthenium and osmium porphyrins binding phenyl-Or diphenylphosphane

Chemistry - A European Journal

Volumn 11, Issue 8, 2005, Pages 2405-2416

  Xie, Jin ^a   Huang, Jie Sheng ^a   Zhu, Nianyong ^a   Zhou, Zhong Yuan ^b   Che, Chi Ming ^a  

^a UNIVERSITY OF HONG KONG   (Hong Kong)

^b HONG KONG POLYTECHNIC UNIVERSITY   (Hong Kong)

Author keywords

Osmium; P ligands porphyrinoids; Ruthenium; Structure elucidation

Indexed keywords

CATALYSIS; COMPLEXATION; CRYSTAL STRUCTURE; CYCLIC VOLTAMMETRY; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; OSMIUM; OXIDATION; RUTHENIUM; SYNTHESIS (CHEMICAL); X RAY CRYSTALLOGRAPHY;

P LIGANDS; PORPHYRINOIDS; STRUCTURE ELUCIDATION;

TRANSITION METALS;

METALLOPORPHYRIN; OSMIUM; PHENOL; PHOSPHINE; PHOSPHINE DERIVATIVE; RUTHENIUM;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; ELECTROCHEMISTRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; X RAY CRYSTALLOGRAPHY;

CRYSTALLOGRAPHY, X-RAY; ELECTROCHEMISTRY; MAGNETIC RESONANCE SPECTROSCOPY; METALLOPORPHYRINS; MODELS, MOLECULAR; MOLECULAR STRUCTURE; OSMIUM; PHENOL; PHOSPHINES; RUTHENIUM;

EID: 17444373967     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/chem.200400996     Document Type: Article

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29. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
30. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
31. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
32. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
33. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
34. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
35. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
36. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
37. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
38. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
39. Selected examples: a) H. J. Callot, C. Piechocki, Tetrahedron Lett. 1980, 21, 3489; b) K. C. Brown, T. Kodadek, J. Am. Chem. Soc. 1992, 114, 8336; c) D. W. Bartley, T. Kodadek, J. Am. Chem. Soc. 1993, 115, 1656; d) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; e) J. R. Wolf, C. G. Hamaker, J.-P. Djukic, T. Kodadek, L. K. Woo, J. Am. Chem. Soc. 1995, 117, 9194; f) E. Galardon, P. Le Maux, G. Simonneaux, Chem. Commun. 1997, 927; g) W.-C. Lo, C.-M. Che, K.-F. Cheng, T. C. W. Mak, Chem. Commun. 1997, 1205; h) M. Frauenkron, A. Berkessel, Tetrahedron Lett. 1997, 38, 7175; i) Z. Gross, N. Galili, L. Simkhovich, Tetrahedron Lett. 1999, 40, 1571; j) E. Galardon, P. Le Maux, G. Simonneaux, Tetrahedron 2000, 56, 615; k) C.-M. Che, J.-S. Huang, F.-W. Lee, Y. Li, T.-S. Lai, H.-L. Kwong, P.-F. Teng, W.-S. Lee, W.-C. Lo, S.-M. Peng, Z.-Y. Zhou, J. Am. Chem. Soc. 2001, 123, 4119; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, J. Am. Chem. Soc. 2001, 123, 4843: m) A. Berkcssel, P. Kaiser, J. Lex, Chem. Eur. J. 2003, 9, 4746.
40. Selected examples: a) R. Breslow, S. H. Gellman. J. Chem. Soc. Chem. Commun. 1982, 1400;
41. b) R. Breslow, S. H. Gellman, J. Am. Chem. Soc. 1983, 105, 6728;
42. D. Mansuy, J.-P. Mahy, A. Durcault, G. Bedi, P. Battioni, J. Chem. Soc. Chem. Commun. 1984, 1161;
43. J. P. Mahy, G. Bedi, P. Battioni, D. Mansuy, Tetrahedron Lett. 1988, 29, 1927;
44. e) T.-S. Lai, H.-L. Kwong, C.-M. Che, S.-M. Peng, Chem. Commun. 1997, 2373;
45. f) X.-G. Zhou, X.-Q. Yu, J.-S. Huang, C.-M. Che, Chem. Commun. 1999, 2377;
46. g) X.-Q. Yu, J.-S. Huang, X.-G. Zhou, C.-M. Che, Org. Lett. 2000, 2, 2233;
47. h) J.-L. Liang, S.-X. Yuan, J.-S. Huang, W.-Y. Yu, C.-M. Che. Angew. Chem. 2002, 114, 3615; Angew. Chem. Int. Ed. 2002, 41, 3465.
48. h) J.-L. Liang, S.-X. Yuan, J.-S. Huang, W.-Y. Yu, C.-M. Che. Angew. Chem. 2002, 114, 3615; Angew. Chem. Int. Ed. 2002, 41, 3465.
49. K. B. Dillon, F. Mathey, J. F. Nixon, Phosphorus: the Carbon Copy: from Organophosphorus to Phospha-Organic Chemistry, Wiley, New York. 1998.
50. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
51. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
52. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
53. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
54. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
55. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
56. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
57. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
58. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
59. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
60. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
61. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
62. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
63. Selected examples: a) D. Mansuy, M. Lange, J.-C Chottard, P. Guerin, P. Morliere, D. Brault, M. Rougee, J. Chem. Soc. Chem. Commun. 1977, 648; b) D. Mansuy, M. Lange, J.-C. Chottard, J. F. Bartoli, B. Chevrier, R. Weiss, Angew. Chem. 1978, 90, 828; Angew. Chem. Int. Ed. Engl. 1978, 17, 781; c) J. P. Collman, P. J. Brothers, L. McElwee-White, E. Rose, L. J. Wright, J. Am. Chem. Soc. 1985, 107, 4570, d) J. P. Collman, P. J. Brothers. L. McElwee-White, E. Rose, J. Am. Chem. Soc. 1985, 107, 6110; e) I. Artaud, N. Gregoire, J.-P. Battioni, D. Dupre, D. Mansuy, J. Am. Chem. Soc. 1988, 110, 8714; f) T. Boschi, S. Licoccia, R. Paolesse, P. Tagliatesta, G. Pelizzi, F. Vitali, Organometallics 1989, 8, 330; g) I. Artaud, N. Gregoire, P. Leduc, D. Mansuy, J. Am. Chem. Soc. 1990, 112, 6899; h) D. A. Smith, D. N. Reynolds, L. K. Woo, J. Am. Chem. Soc. 1993, 115, 2511; i) E. Galardon, P. Le Maux, L. Toupet, G. Simonneaux, Organometallics 1998, 17, 565; j) C. G. Hamaker, J.-P. Djukic, D. A. Smith, L. K. Woo, Organometallics 2001, 20, 5189; k) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, X.-Z. You, J. Am. Chem. Soc. 2002, 124, 13 185; l) Y. Li, J.-S. Huang, Z.-Y. Zhou, C.-M. Che, Chem. Commun. 2003, 1362; m) Y. Li, J.-S. Huang, G.-B. Xu, N. Zhu, Z.-Y. Zhou, C.-M. Che, K.-Y. Wong, Chem. Eur. J. 2004,1 0, 3486.
64. a) J. W. Buchler, S. Pfeifer, Z. Naturforsch. B 1985, 40, 1362;
65. b) R. L. Elliott, P. J. Nichols, B. O. West, Polyhedron 1987, 6, 2191;
66. C.-M. Che, J.-S. Huang, Z.-Y. Li, C.-K. Poon, Inorg. Chim. Acta 1991, 190, 161;
67. J.-S. Huang, C.-M. Che, C.-K. Poon, J. Chem. Soc. Chem. Commun. 1992, 161;
68. e) J. A. Smieja, K. M. Omberg, G. L. Breneman, Inorg. Chem. 1994, 33, 614;
69. f) L. M. Berreau, V. G. Young, Jr., L. K. Woo, Inorg. Chem. 1995, 34, 527;
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72. Z.-Y. Li, J.-S Huang, M. C.-W. Chan, K.-K. Cheung, C.-M. Che, Inorg. Chem. 1997, 36, 3064;
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76. S.-M. Au, J.-S. Huang, W.-Y. Yu, W.-H. Fung, C.-M. Che, J. Am. Chem. Soc. 1999, 121, 9120;
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93. C.-M. Che, T.-F. Lai, W.-C. Chung, W. P. Schaefer, H. B. Gray, Inorg. Chem. 1987, 26, 3907.
94. 3): δ=-83.39, -84.13, -84.44, -84.78, -85.52, -86.25, -86.59, -86.91, -87.64 ppm.
95. +.
96. R. G. Ball, G. Domazetis, D. Dolphin, R R. James, J. Trotter, Inorg. Chem. 1981, 20, 1556.
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109. a) D. P. Rillema. J. K. Nagle, L. F. Barringer, Jr., T. J. Meyer, J. Am. Chem. Soc. 1981, 103, 56 ;
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