Determination of organophosphorus pesticide residues in food. A review;Revisión de los métodos de determinación de residuos de plaguicidas organofosforados en alimentos

Revista de Toxicologia

Volumn 20, Issue 3, 2003, Pages 166-175

  Juan, A ^a   Pico Y ^a   Font, G ^a  

^a UNIVERSITY OF VALENCIA   (Spain)

Author keywords

Chromatographic techniques; Food; Organophosphorus pesticides; Sample preparation

Indexed keywords

ORGANOPHOSPHATE PESTICIDE;

ACCURACY; AGRICULTURE; CHEMICAL ANALYSIS; COST EFFECTIVENESS ANALYSIS; CROP; EXTRACTION; FOOD; GAS CHROMATOGRAPHY; HEALTH HAZARD; HUMAN; INTERMETHOD COMPARISON; RELIABILITY; REVIEW; SAMPLING; SOLID; TECHNOLOGY; TIME;

EID: 0347762678     PISSN: 02127113     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Review

References (88)

1. Saunders DS, Harper C (1994) Pesticides. En: Hayes AW (ed) Principles and methods of toxicology. Raven Press, Nueva York, NY, 389-415.
2. Repetto M (1995) Toxicologia avanzada, Diaz de Santos, Madrid, 571-583.
3. Hajslová J, Holadova K, Kocourek V, Poustka J, Godula M, Cuhra P, Kempn_ M (1998) Matrix-induced effects: a critical point in the gas chromathographic analysis of pesticide residues. J Chromatogr A 800: 283-295.
4. Hogendoorn EA, Ossendrijver FM, Dijkman E, Baumann RA (1999) Rapid determination of glyphosate in cereal samples by means of pre-columns derivatisation with 9-fluorenylmethyl chloroformate and coupled-column liquid chromatography with fluorescence detection. J Chromatogr A 833: 67-73.
5. Fernández M, Picó Y, Mañes J (2001) Pesticide Residues in oranges from Valencia (Spain). Food Add Contam 18: 615-624.
6. Fernández M, Picó Y, Mañes J (2001) Comparison of gas and liquid chromatography coupled to mass spectrometry for the residue analysis of pesticide in oranges. Chromatographia 54: 302-308.
7. Dogheim SM, Gad Alla SA, El-Syes SMA, Almaz MM, Salama EY (1996) Organochlorine and organophosphorus pesticide residues in food from egyptian local markets. J AOAC Int 79: 949-952.
8. Dogheim SM, Mohamed E, Gad Alla SA, El-Saied S, Emel SY, Mohsen MA (1996) Monitoring of pesticide residues in human milk, soil water and food samples collected from Karf El-Zayat Governorate. J AOAC Int 79: 111-116.
9. Uygun U (1997) Determination of organophosphorus pesticide residues in carrot using gel permeation chromatography. J Liq Chrom Rel Technol 20: 771-777.
10. Kocourek V, Hajslová J, Holadova K, Poustka J (1998) Stability of pesticides in plant extracts used as calibrants in the gas chromatography analysis of residues. J Chromatogr A 800: 297-304.
11. Yamazaki Y, Ninomiya T (1999) Determination of benomyl, difenyl, o-phenylphenol, thiabendazole, chlorpyriphos, methidathion, and methyl parathion in oranges by solid-phase extraction, liquid chromatography and gas chromatography. J AOAC Int 82: 1474-1478.
12. Molinari GP, Cavanna S, Ferroni B (1998) Multiresidue method for determination of organophosphorus pesticides in vegetables. Food Add Contam 15: 510-517.
13. Dorea HS, Tadeo JL, Sanchez C (1996) Determination of organophosphorus pesticide residues in fruits bygas chromatography with ITD and NPD detection. Chromatographia 43: 380-386.
14. Obana H, Akutsu K, Okihashi M, Hori S (2001) Multiresidue analysis of pesticides in vegetables and fruits using two-layered column with graphitized carbon and water absorbent polymer. Analyst 126: 1529-1534.
15. Mergnat T, Fritsch P, Saint-Joly C, Truchot E, Saint-Blanquat G (1995) Reduction in phosalone residue levels during industrial dehydration of apples. Food Add Contam 12: 759-767.
16. Schaterle S, Feigel C (1996) Pesticide residue analysis in fresh produce by gas chromatography-tandem mass spectrometry. J Chromatogr A 754: 411-422.
17. Ahmad N, Bugueno G, Guo L, Marolt R (1999) Determination of organochlorine and organophosphate pesticide residues in fruits, vegetables and sediments. J Environ Sci Health 34: 829-848.
18. Oliva J, Navarro S, Barba A, Navarro G (1999) Determination of chlorpyrifos, penconazole, fenarimol, vinclozolin and metalaxyl in grapes, must and wine by on-line microextraction and gas chromatography. J Chromatogr A 833: 43-51.
19. Johnson PD, Rimmer DA, Braun RH (1997) Adaptation in application of a multi-residue method for the determination of a range of pesticides, including phenoxy acid herbicides in vegetation, ased on high-resolution gel permeation chromatographic clean-up and gas chromatographic analysis with mass-selective detection. J Chromatogr A 765: 3-11.
20. Lacassie E, Dreyfuss MF, Daguet JL, Vignaud M, Marquet P, Lachâtre G (1998) Multiresidue determination of pesticides in apples and pears by gas chromatography-mass spectrometry. J Chromatogr A 805: 319-326.
21. Lacassie E, Dreyfuss MF, Daguet JL, Vignaud M, Marquet P, Lachâtre G (1999) Liquid chromotography-electrospray mass spectrometry multiresidue determination of pesticides in apple and pears. J Chromatogr A 830: 135-143.
22. Bouaid A, Martin-Esteban A, Fernández P, Contreras M (2000) Microwave-assisted extraction method for the determination of atrazine and four organophosphorus pesticides in oranges by gas chromatography. Fresenius J Anal Chem 367: 291-294.
23. Gazea F, Calvarano Y (1998) Determination of organophosphorus pesticide residues in fruits. Fresenius Envir Bull 7: 710-715.
24. Bicchi C, D'Amato A, Binello A (1996) Identification of pesticide residues in real matrices by combining retention indices and specific multidetcction responses. J High Rcsol Chromatogr 19: 80-84.
25. Sojo LE, Broke A, Fillion J, Price SM (1997) Application of activated carbon membranes for on-line cleanup of vegetable and fruit extracts in the determination of pesticide multiresidues by gas chromatography with mass selective detection. J Chromatogr A 788: 141-154.
26. Fillion J, Sauvé F, Selwyn J (2000) Multiresidue method for the determination of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromathography with fluorescence detection. J AOAC Int 83: 698-713.
27. Sheridan RS, Meola JR (1999) Analysis of pesticide residues in fruits, vegetables and milk by gas chromatography/tandem mass spectrometry. J AOAC Int 82: 982-990.
28. Dogheim SM, Gad Alla SA, El-Marsafy AM (1999) Monitoring pesticide residues in egyptian fruits and vegetables in 1995. J AOAC Int 82: 948-955.
29. Gelsomino A, Petrovicová B, Tiburtini S, Magnani E, Felici M (1997) Multiresidue analysis of pesticides in fruits and vegetables by gel permeation chromatography followed by gas chromatography with electron-capture and mass spectrometric detection. J Chromatogr A 782: 105-122.
30. Szymczyk S, Malczewska M (1998) Gas chromatography analysis of organophosphorus pesticides in plant samples. Chromatographia 48: 156-157.
31. Richter BE, Hoefler FLM (2001) Determination of organophosphorus pesticides in food using accelerated solvent extraction with large sample sizes. LC-GC Int 19: 408-412.
32. Obana H, Kikuchi K, Okihashi M, Hori S (1997) Determination of organophosphorus pesticides in foods using an accelerated solvent extraction system. Analyst 122: 217-220.
33. Ramesh A, Balasubramanian M (1999) The impact of household preparations on the residues of pesticides in selected agricultural food commodities available in India. J AOAC Int 82: 725-737.
34. Abou-Arab AAK, Abou Donia MA (2001) Pesticide residues in some Egyptian spices and medicinal plants as affected by processing. Food Chem 72: 439-445.
35. Armishaw P, Millar R (2001) A natural matrix (pureed tomato) candidate reference material containing residue concetrations of pesticide chemicals. Fresenius J Anal Chem 370: 291-296.
36. Sampedro MC, Gómez de Balugera Z, Goicolea A, Barrio RJ (1998) Determination of the insecticide pyridafenthion in river water, soils and wine by adsorptive stripping voltammetry. Food Add Contam 15: 793-800.
37. Stan HJ, Linkerhägner M (1996) Pesticide residues analysis in foodstuffs applying capillary gas chromatography with atomic emission detection. State-of-the-art use of modified multimethod S19 of Deutsche Forschugsgemeinschaft and automated large-volume injection with programmed-temperature vaporization and solvent venting. J Chromatogr A 750: 369-390.
38. Lentza-Rizos Ch, Avramides EJ, Cherasco F (2001) Low-temperature clean-up method for the determination of organophosphorus insecticides in olive oil. J Chromatogr A 912: 135-142.
39. Hiskia AE, Atmajidou MD, Tsipi DF (1998) Determination of organophosphorus pesticide residues in Greek virgin olive oil by capillary gas chromatography. J Agric Food Chem 46: 570-574.
40. Jongenotter B, Janssen H-G (2002) On-Line GPC-CG analysis of organophosphorus pesticides in edible oils. LC-GC Eur 15: 338-357.
41. Juhler RK (1997) Optiomized method for the determination of organophosphorus pesticide in meat and fatty matrices. J Chromatogr A 786: 145-153.
42. Schenck FJ, Donoghue DJ (2000) Determination of organochlorine and organophosphorus pesticide residues in eggs using a solid phase extraction cleanup. J Agric Food Chem 48: 6412-6415.
43. Bennett D, Chung AC, Lee SM (1997) Multiresidue method for analysis of pesticides in liquid whole milk. J AOAC Int 80: 1065-1077.
44. Ronald D, Pawloski TM (1997) Matrix-induced enhancement of pesticides in gas chromatography: is there a solution?. J High Resolut Chromatogr 20: 375-378.
45. 14C] methyl parathion during milk processing. Bull Envirom Contam Toxicol 65: 207-214.
46. Hernández F, Serrano R, Beltrán J, López FJ (1996) Comparison of cleanup techniques for simple method for analysis of selected organophosphorus pesticide residue in molluscs. J AOAC Int 79: 123-131.
47. Hernández F, Serrano R, Pitarch E, López FJ (1998) Automated sample clean-up procedure for organophosphorus pesticides in several aquatic organisms using normal phase liquid chromatography. Anal Chim Acta 374: 215-229.
48. Serrano R, López FJ, Hernández F (2002) Multiresidue determination of persistent organochlorine and organophosphorus compounds in wale tissues using automated liquid chromatographic clean up and gas chromatographic-mass spectrometric detection. J Chromatogr A 855: 633-643.
49. Agüera A, Piedra L, Hernando MD, Fernández-Alba AR, Contreras M (2000) Splitless large-volume GC-MS injection for the analysis of organophosphorus and organochlorine pesticides in vegetables using a miniaturised ethyl acetate extraction. Analyst 125: 1397-1402.
50. di Muccio A, Pelosi P, Camoni I, Barbini DA, Dommarco R, Generali T, Ausili A (1996) Selective, solid-matrix dispersion extraction of organophosphate pesticide residues from milk. J Chromatogr A 754: 497-506.
51. Bushway RJ, Fan Z (1998) Determination of chlorpyrifos in fruits and vegetables by ELISA and confirmation by GC-AED. Food Agric Immunol 10: 215-221.
52. 18 and graphitized carbon black solid phase extraction cleanup. J Environ Sci Health 34: 349-362.
53. Casanova JA (1996) Use of solid-phase extraction disks for analysis of moderately polar and non-polar pesticides in high-moisture foods. J AOAC Int 79: 936-940.
54. Jiménez JJ, Bernal JL, del Nozal MJ, Toribio L, Martin MT (1998) Gas chromatography with electron capture and nitrogen-phosphorus detection in the analysis of pesticides in honey after the elution with florisil column. J Chromatogr A 823: 381-387.
55. Niessner G, Buchberger W, Bonn GK (1996) Rapid multiresidue screening method for the determination of pesticide in plant materials. J Chromatogr A 737: 215-222.
56. Lagana A, D'Ascenzo G, Fago G, Marino A (1997) Determination of organophosphorus pesticides and metabolites in crops by solid-phase extraction followed by liquid chromatography-diode-array detection. Chromatographia 46: 256-264.
57. Torres CM, Picó Y, Redondo MJ, Mañes J (1996) Matrix solid-phase dispersion extraction procedure for multiresidue pesticide analysis in oranges. J Chromatogr A 719: 95-103.
58. Allender WJ (1991) Column extraction of chlorpyrifos from contaminated fish. J Anal Toxicol 15: 141-143.
59. Abou-Arab AAK (1999) Behavior of pesticide in tomatoes during commercial and home preparation. Food Chem 65: 509-514.
60. Dórea H, Langas FM (1999) Matrix solid-phase dispersion extraction of organphosphorus and synthetic pyrethroid pesticides in cashew nut and passion fruit. J Microcol Sep 11: 367-375.
61. Schenck FJ, Wagner R (1995) Screening procedure for organochlorine and organophosphorus pesticide residues in milk using matrix solid phase dispersion (MSPD) extraction and gas chromatographic determination. Food Add Contam 12: 535-541.
62. Kristenson EM, Haverkate EGJ, Slooten CJ, Ramos L, Vreuls RJJ, Brinkman UATh (2001) Miniaturized automated matrix solid-phase dispersion extraction of pesticides in fruit followed by gas chromatography-mass spectrometric analysis. J Chromatogr A 917: 277-286.
63. Torres CM, Picó Y, Mañes J (1995) Analysis of pesticide residues in fruit and vegetables by matrix solid-phase dispersion and different gas chromatographic element-selective detectors. Chromatographia 41: 685-692.
64. Bicchi C, D'Amato A, Bal C (1997) Multiresidue method for quantitative gas chromatographic determination of pesticide residues in sweet cherries. J AOAC Int 80: 1281-1286.
65. Viana E, Moltó JC, Font G (1996) Optimization of matrix solid-phase dispersion method for the analysis of pesticide residues in vegetables. J Chromatogr A 754: 437-444.
66. Blasco C, Font G, Picó Y (2002) Comparison of microextraction procedures to determine pesticides in oranges by liquid chromatography-mass spectrometry. J Chromatogr A 970: 201-212.
67. Simplicio AL, Boas LV (1999) Validation of a solid-phase microextraction method for the determination of organophosphorus pesticides in fruits and fruit juice. J Chromatogr A 833: 35-42.
68. Vitali M, Guidotti M, Giovinazzo R, Cedrone O (1998) Determination of pesticide residues in wine by solid phase microextraction and gas chromatography/mass spectrometry for consumer risk assessment. Food Add Contam 15: 280-287.
69. Barker A (2000) Applications of matrix solid-phase dispersion in food analysis. J Chromatogr A 880: 63-68.
70. Batlle R, Sanchez C, Nerin C (1999) A systematic approach to optimize solid-phase microextraction. Determination of pesticides in ethanol/water mixtures used as food simulants. Anal Chem 71: 2417-2422.
71. Chen W, Poon KF, Lam MHW (1998) The application of solid-phase microextraction in the analysis of organophosphorus pesticides in a food plant. Environ Sci Technol 32: 3816-3820.
72. Hu R, Hennion B, Urruti R, Montury M (2002) Solid phase microextraction of pesticide residues from strawberries. Food Add Contam 16: 111-117.
73. Normal KNT, Panton SHW (2001) Supercritical fluid extraction and quantitative determination of organophosphorus pesticide residues in wheat and maize using gas chromatography with flame photometric and mass spectrometric detection. J Chromatogr A 907: 247-255.
74. Kim DA, Heo GS, Lee DW (1998) Determination of organophosphorus pesticides in wheat flour by supercritical fluid extraction and gas chromatography with nitrogen-phosphorus detection. J Chromatogr A 824: 63-70.
75. Faugeron J, Tourte J, Gros P, Charabel S, Cooper JF (1997) Extraction par fluide supercritique de résidus de pesticides. Développement et validation d'une méthode appliquée aux céréales et à leurs dérivés. Analusis 25: 192-196.
76. Stefani R, Buzzi M, Grazzi R (1997) Supercritical fluid extraction of pesticide residues in fortified apple matrices. J Chromatogr A 782: 123-132.
77. Lehotay S, Valverde-Garcia A (1997) Evaluation of different solid-phase traps for automated collection and clean-up in the analyis of multiple pesticides in fruits and vegetables after supecritical fluid extraction. J Chromatogr A 765: 69-84.
78. Nerin C, Batlle R, Cacho J (1998) Determination of pesticde in high-water-content samples by off-line supercritical fluid extraction-gas chromatography-electron-capture detection. J Chromatogr A 795: 117-124.
79. Valverde-Garcia A, Fernández-Alba AR, Contreras M, Agüera A (1996) Supercritical fluid extraction of pesticides from vegetables using anhydrous magnesium sulfate for sample preparation. J Agric Food Chem 44: 1780-1784.
80. Pearce KL, Trenerry VC, Were S (1997) Supercritical fluid extraction of pesticides residues from strawberries. J Agric Food Chem 45: 153-157.
81. Juhler RK (1998) Supercritical fluid extraction of pesticides from meat: a systematic approach for optimisation. Analyst 123: 1551-1556.
82. Hopper ML (1997) Extraction and cleanup of organochlorine and organophosphorus pesticide residues in fats by supercritical fluid techniques. J of AOAC Int 80: 639-646.
83. Hopper ML (1999) Automated one-step supercritical fluid extraction and clean-up system for the analysis of pesticide residues in fatty matrices. J Chromatogr A 840: 93-105.
84. Ranalli A, Cabras P, lannucci E, Contreras M (2001) Lipochromes, vitamins, aromas and other components of virgin olive oil are affected by processing technology. Food Chem 73: 445-451.
85. Cabras P, Angioni A, Melis M, Minelli EV, Pirisi FP (1997) Simplified muyltiresidue method for the determination of OPPS insecticides in olive oil. J Chromatogr A 761: 327-331.
86. Hooijschuur EWJ, Kientz ChE, Dijksman J, Brinkman UATh (2001) Potential of microcolumn liquid chromatography and capillary electrophoresis with flame photometric detection for determination of polar phosphorus-containing pesticides. Chromatographia 54: 295-301.
87. Zhu W, Wu F, Raushel FM, Vigh G (2000) Capillary electrophoretic separation of the enantiomers of organophosphates with a phosphorus esterogenic center using the sodium salt of octakis (2,3-diacetyl-6-sulfo)-gamma-cyclodextrin as resolving agent. J Chromatogr A 895: 247-254.
88. Wang J, Chatrathi MP, Mulchandani A, Chen W (2001) Capillary electrophoresis microchips for separation and detection of organophosphate nerve agents. Anal Chem 73: 1804-1808.