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0041872473
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See the Supporting Information for details
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See the Supporting Information for details.
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19
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0042373481
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note
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Abbreviations: DEPBT = 3-(diethyloxyphosphoryloxy)-1,2,3-benzotriazin-4(3H)-one, EDC = 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide, HATU = 2-(1-H-7-azabenzotriazol)-1,1,3,3-methyluronium hexafluorophosphate, HOAt = 1-hydroxy-7-azabenzotriazole.
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20
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0041872471
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note
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Details will be disclosed later in the full account of this work.
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21
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0033526392
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Hoveyda, A.H.7
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0042373479
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note
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A significant byproduct in the Cu-mediated reaction relates to formation of phenol derived from the boronic acid; none of the corresponding methyl ether is detected, however. This observation is in contrast to a previous hypothesis (ref 17a) that phenol formation arises from reaction of adventitious water.
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32
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85008070422
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and references therein
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34
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0041371718
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note
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1H NMR (see the Supporting Information).
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