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Volumn 4, Issue 6, 2002, Pages 1007-1010

Capture-ROMP - Release: Application for the synthesis of O-alkylhydroxylamines

Author keywords

[No Author keywords available]

Indexed keywords

HYDROXYLAMINE; N HYDROXYSUCCINIMIDE; N-HYDROXYSUCCINIMIDE; POLYMER; SUCCINIMIDE DERIVATIVE;

EID: 0037149703     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol025577v     Document Type: Article
Times cited : (30)

References (64)
  • 33
    • 0000809126 scopus 로고    scopus 로고
    • For use of ROM polymers as organic soluble supports for radical reactions, see: (a) Enholm, E. J.; Gallagher, M. E. Org. Lett. 2001, 3, 3397-3399.
    • (2001) Org. Lett. , vol.3 , pp. 3397-3399
    • Enholm, E.J.1    Gallagher, M.E.2
  • 37
    • 0042041857 scopus 로고
    • For other methods on the production of O-alkylhydroxylamines, see: (a) Theilacker, W.; Ebke, K. Angew. Chem. 1956, 68, 303.
    • (1956) Angew. Chem. , vol.68 , pp. 303
    • Theilacker, W.1    Ebke, K.2
  • 46
    • 0041540557 scopus 로고    scopus 로고
    • note
    • 2 = 1,3-dimesityl-4,5-dihydroimidazol-2-ylidene.
  • 48
    • 0041540612 scopus 로고    scopus 로고
    • note
    • 1H NMR spectra of crude 5a-h in the Supporting Information.
  • 56
    • 0043043534 scopus 로고    scopus 로고
    • note
    • (d) Bis(5-norbornenyl-2-methyl) azodicarboxylate (DNAD). see ref 8.
  • 57
    • 0043043535 scopus 로고    scopus 로고
    • note
    • Barrett has previously shown that 3 can be used to construct a ROMPgel acylating agent, see ref 9c.
  • 58
    • 0043043533 scopus 로고    scopus 로고
    • note
    • When the polymerization was performed at ambient temperature, a reaction time of 3 h was required for complete consumption of monomer.
  • 62
    • 0043043532 scopus 로고    scopus 로고
    • note
    • When 1 was employed, the polymerization required refluxing for multiple hours, while 2 only required 45 min at reflux.
  • 63
    • 0026931032 scopus 로고
    • 1H NMR assignments were made according to the reported shifts of poly(7-oxabicyclo[2.2.1]hept-2-ene) derivatives. See: Benedicto, A. D.; Novak, B. M.; Grubbs, R. H. Macromolecules 1992, 25, 5893-5900.
    • (1992) Macromolecules , vol.25 , pp. 5893-5900
    • Benedicto, A.D.1    Novak, B.M.2    Grubbs, R.H.3
  • 64
    • 0033515856 scopus 로고    scopus 로고
    • For an example of Mitsunobu reactions with menthol and other hindered alcohols, see: Sammakia, T.; Jacobs, J. S. Tetrahedron Lett. 1999, 40, 2685-2688.
    • (1999) Tetrahedron Lett. , vol.40 , pp. 2685-2688
    • Sammakia, T.1    Jacobs, J.S.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.