메뉴 건너뛰기




Volumn 3, Issue 4, 2001, Pages 387-396

Solid-phase development of a 1-hydroxybenzotriazole linker for heterocycle synthesis using analytical constructs

Author keywords

[No Author keywords available]

Indexed keywords


EID: 0001160658     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc0100114     Document Type: Article
Times cited : (20)

References (44)
  • 32
    • 0042728284 scopus 로고    scopus 로고
    • note
    • The yields of the solid-phase steps in the synthesis were determined gravimetrically.
  • 34
    • 0030869889 scopus 로고    scopus 로고
    • An impurity (up to a maximum of 6%) was formed during the Mitsunobu reaction. The level of the impurity increased when the cleavage of the o-nitrobenzenesulfonamide was carried out using sodium thiophenolate in dimethylformamide. Buffering the cleavage solution with thiophenol prevented further byproduct formation. The structure of the byproduct was tentatively assigned as the Stevens rearrangement product by analogy with literature precedent. Bowman, W. R.; Coghlan, D. R. Tetrahedron 1997, 46, 15787-15798.
    • (1997) Tetrahedron , vol.46 , pp. 15787-15798
    • Bowman, W.R.1    Coghlan, D.R.2
  • 35
    • 0043229557 scopus 로고    scopus 로고
    • note
    • Now commercially available from Novabiochem.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.