Combined application of analytical techniques for the characterization of polymer supported species

Journal of Combinatorial Chemistry

Volumn 2, Issue 5, 2000, Pages 491-495

  Grice, P ^a   Leach, A G ^a   Ley, S V ^a   Massi, A ^a   Mynett, D M ^a  

^a UNIVERSITY OF CAMBRIDGE   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001508050     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc000021p     Document Type: Article

References (52)

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48. IR spectra were obtained on a Perkin-Elmer Spectrum 1000 IR spectrometer in conjunction with a Perkin-Elmer Autoimage IR/ visible microscope. Beads were flattened in a Specac diamond compression cell.
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50. 3 (internal) taken as 77.0 ppm.
51. 13C may also be recorded without inserts to give a sample volume of ~60 μL. (21) CPMG spectra were obtained using the standard Bruker pulse program. The loop counter was set to between 16 or 128 depending on the level of suppression required.
52. DQF-COSY spectra were obtained using the standard Bruker pulse program.