Evaporation behaviour of DMS in an aqueous solution at infinite dilution - a review

Journal of the Institute of Brewing

Volumn 122, Issue 1, 2016, Pages 181-190

  Scheuren, H ^a   Baldus, M ^b   Methner, F J ^b   Dillenburger, M ^c  

^a Fachgebiet Brauwesen ^*  (Germany)

^b TECHNISCHE UNIVERSITÄT BERLIN   (Germany)

^c Dillenburger und Hertel GmbH   (Germany)

Author keywords

Calculation; Dimethyl sulfide (DMS); Evaporation; Vaporization

Indexed keywords

CALCULATIONS; SULFUR COMPOUNDS; VAPORIZATION;

DIMETHYL SULFIDE; FUNCTION SETS; INFINITE DILUTION;

EVAPORATION;

EID: 84958773574     PISSN: 00469750     EISSN: 20500416     Source Type: Journal    
DOI: 10.1002/jib.301     Document Type: Article

References (84)

1. Scheuren, H., Dillenburger, M., Tippmann, J., Feilner, R., Methner, F.-J., and Sommer, K. (2014) Stripping DMS in the brew house Part 1, Brauwelt Int. 32(4), 217-219.
2. Narziß, L., and Back, W. (2008) Die Technologie der Würzebereitung, 8th ed., pp. 512-592, Fachverlag Hans Carl, Nürnberg.
3. DIN 8777 (2009) Sudhausanlagen in Brauereien, Deutsches Institut für Normung, Berlin.
4. Scheuren, H., Sommer, K., and Dillenburger, M. (2015) Explanation for the increase of free DMS during mashing, J. Inst. Brew. 122(2).
5. Scheuren, H., Sommer, K., and Hertel, M. (2008) Vaporisation of aromatic components during the beer production, BrewingScience - Monatsschrift für Brauwissenschaft 62, 162-169.
6. Hyde, W. R., and Brookes, P. A. (1978) Malt quality in relation to beer quality, J. Inst. Brew. 84, 167-174.
7. Forster, C., Miedaner, H., Narziß, L., and Back, W. (1995) influence of kilning technology on the formation of volatile aroma compounds in malt, wort and beer, in Proc. Eur. Brew. Conv. Congr. Brussels, pp. 475-482, IRL Press, Oxford.
8. Brookes, P. A., and Dickenson, J. C. (1983) The relationship between malting process conditions and the potential of malt to give dimethyl sulphide in beer, in Proc. Eur. Brew. Conv. Congr. Brussels, pp. 393-400, IRL Press, Oxford.
9. Schwill-Miedaner, A. (2003) Wort boiling today - Are there alternatives?, Brauwelt Int. 1, 42-45.
10. Rübsam, H., Becker, T., and Krottenthaler, M. (2010) Optimizing brewhouse technology with reference to dimethyl sulfide, Brauwelt Int. 3, 138-145.
11. Wilson, R. J., and Booer, C. D. (1979) Control of the dimethyl sulphide content of beer by regulation of the copper boil, J. Inst. Brew. 85, 144-148.
12. De Rouck, G., Flores-Gonzales, A. G., De Clippeleer, J., De Cock, J., De Cooman, L., and Aerts, G. (2010) Sufficient formation and removal of dimethyl sulfide (DMS) without classic wort boiling, Brewing Science - Monatsschrift für Brauwissenschaft 63(1/2), 31-40.
13. Dickenson, J. C. (1979) The relationship of dimethyl sulphide levels in malt, wort and beer, J. Inst. Brew. 85, 235-239.
14. Annes, B. J., and Bamforth, C. W. (1982) Dimethyl sulphide - A review, J. Inst. Brew. 88, 244-252.
15. Zürcher, C., Gruss, R., and Kleber, R. (1979) Technologische Maßnahmen zur Reduzierung des Dimethylsulfidgehaltes im Bier, in Proc. Eur. Brew. Conv. Congr. Berlin-West, pp. 175-187, IRL Press, Oxford.
16. White, F. H., and Wainright, T. (1977) The presence of two dimethyl sulphide precursors in malt, their control by malt kilning conditions and their effect on beer DMS levels, J. Inst. Brew. 83, 224-230.
17. Feilner, R., Rehmann, D., Methner, F.-J., Baldus, M., Kunz, T., and Scheuren, H. (2013) Wort stripping-thermodynamic considerations on the evaporation of aroma substances in continuous desorption processes, BrewingScience - Monatsschrift für Brauwissenschaft 66(5/6), 65-74.
18. Hertel, M., Dauth, H., Scheuren, H., and Sommer, K. (2007) Die Würzekochung: Ausdampfvorgänge korrekt betrachtet Teil 2: Bestätigung der Theorie durch Praxisversuche, Brauwelt 147(3), 48-50.
19. Hertel, M., and Sommer, K. (2009) Wort boiling by batch rectification-possibilities for reducing required evaporation, Tech. Q. Master Brew. Assoc. Am. DOI:10.1094/TQ-46-1-0208-01.
20. Scheuren, H., Heinemann, S., Hertel, M., Voigt, J., Dauth, H., and Sommer, K. (2008) Vorhersage und experimentelle Bestätigung des Ausdampfverhaltens gängiger Würzekochsysteme, Brauwelt 148(14), 380-384.
21. Hertel, M., Dauth, H., Scheuren, H., and Sommer, K. (2007) Die Würzekochung: Ausdampfvorgänge korrekt betrachtet Teil 4: Entwicklungs eines effizienteren Kochverfahrens, Brauwelt Nr. 29-30, 810-841.
22. Seaton, J. C., Forrst, I. S., and Suggett, A. (1981) High temperature wort boiling - A consequence for beer flavour, in Proc. Eur. Brew. Conv. Congr. Copenhagen, pp. 161-168, IRL Press, Oxford.
23. Mitani, Y., Ishida, F., Akiyama, H., and Tamaki, T. (1997) Rate analysis of dimethyl sulphide volatilization during wort boiling, in Proc. Eur. Brew. Conv. Congr. Maastricht, pp. 315-322, IRL Press, Oxford.
24. Todd, J. D., Rogers, R., Li, Y. G., Wexler, M., Bond, P. L., Sun, L., Curson, A. R. J., Malin, G., Steinke, M., and Johnston, A. W. B. (2007) Structural and regulatory genes required to make the gas dimethyl sulfide in bacteria, Science 315(5812), 666-669.
25. Nevitt, G. A., Veit, R. R., and Kareiva, P. (1995) Dimethyl sulphide as a foraging cue for Antarctic procellariiform seabirds, Nature 376, 680-682.
26. Talou, T., Gaset, A., Delmas, M., Kulifaj, M., and Montant, C. (1990) Dimethyl sulphide: The secret for black truffle hunting by animals? Mycol. Res. 94(2), 277-278.
27. Herrmann, K. (1992) Vorkommen, Gehalte und Bedeutung von Inhaltsstoffen des Obstes und Gemüses. IX. Carotinoide von grünen Blattgemüsearten, Kohlarten, grünen Bohnen, Erbsen und Gurkengewächsen, Die Industrielle Obst- und Gemüseverwertung 4, 290-294.
28. Meilgaard, M. C. (1975) Flavor chemistry of beer: Part 2: Flavor and threshold of 239 volatiles, Tech. Q. Master Brew. Assoc. Am. 12, 151-168.
29. Kunze, W. (1998) Technologie Brauer und Mälzer, Verlag VLB, Berlin.
30. Back, W. (2006) Technologie und Analytik-Analytische Kontrollmöglichkeiten zur Optimierung technologischer Prozesse, 39, Technologisches Seminar Weihenstephan, München-Weihenstephan.
31. Buttery, R. G., Ling, L. C., and Stern, D. J. (1997) Studies on popcorn aroma and flavor volatiles, J. Agric. Food Chem. 45, 837-843.
32. Bentley, R., and Chasteen, T. G. (2004) Environmental Voscs - formation and degradation of dimethyl sulfide, methanethiol and related materials, Chemosphere 55, 291-317.
33. Yang, B., Schwarz, P., and Horseley, R. (1998) Factors involved in the formation of two precursors of dimethyl sulfoxide during malting, J. Am. Soc. Brew. Chem. 56, 85-90.
34. Dumoulin, M., and Boivin, P. (2001) Industrial kilning technologies and their influence on organoleptic quality of malt, in Proc. Eur. Brew. Conv. Congr. Budapest, pp. 200-209, Fachverlag Hans Carl, Nürnberg.
35. Baldus, M., Kunz, T., and Methner, F.-J. (2013) The analysis of dimethyl sulfoxide in malt, wort and beer using headspace gas chromatography combined with pulsed flame photometric detection (HS-GC-PFPD) - Methodology and applications, BrewingScience -Monatsschrift für Brauwissenschaft 66(9/10), 154-161.
36. Leemans, C., Dupire, S., and Macron, J. (1993) Relation between wort DMSO and DMS concentration in beer, in Proc. Eur. Brew. Conv. Congr. Olso, pp. 709-716, IRL Press, Oxford.
37. Cremer, D. R., and Eichner, K. (2000) Formation of volatile compounds during heating of spice paprika (Capsicum annuum) powder, J. Agric. Food Chem. 48, 2454-2460.
38. Felgentraeger, W. (1994) Numerische Modellierung des Ab-bzw. Aufbaues der wichtigsten Leitsubstanzen des Bieres während der Produktion, Fortschrittsbericht VDI, Düsseldorf.
39. Hertel, M., Tippmann, J., Sommer, K., and Glas, K. (2006) Engineering investigations of the recreating kinetics of flavour-components during the boiling of wort, BrewingScience - Monatsschrift für Brauwissenschaft 59(1/2), 45-55.
40. Mitani, Y., Ishida, F., Akiyama, H., and Tamaki, T. (1997) Rate analysis of dimethyl sulphide volatilization during wort boiling, in Proc. Eur. Brew. Conv. Congr. Maastricht, pp. 315-322, IRL Press, Oxford.
41. Scheuren, H., Tippmann, J., Methner, F.-J., and Sommer, K. (2014) Decomposition kinetics of dimethyl sulphide, J. Inst. Brew. 120(4), 474-476.
42. Gmehling, J., and Kolbe, B. (1988) Thermodynamik, Georg Thieme Verlag, Stuttgart.
43. Scheuren, H. (2015) Die Verfahrenstechnik im Brauprozess-Teil 3: Thermische Verfahrenstechnik, Brauwelt 155(11/12), 310-313.
44. Gmehling, J. (1994) Phasengleichgewichtsmodelle zur Synthese und Auslegung von Trennprozessen, Chemie-Ingenieur-Technik 66(6), 792-808.
45. Krummen, M. (2002) Experimentelle Untersuchung des Aktivitätskoeffizienten bei unendlicher Verdünnung in ausgewählten Lösungsmitteln und Lösungsmittelgemischen als Grundlage für die Synthese thermischer Trennprozesse, dissertation, Carl von Ossietzky Universität Oldenburg, Oldenburg.
46. Alessi, P., Fermeglia, M., and Kikic, I. (1991) Significance of dilute regions, Fluid Phase Equilibria 70, 239-250.
47. Grisher, D. (1999) The determination of activity coefficients at infinite dilution with the help of the dilutor technique (inert gas stripping), Chem. Eng. Technol. 22, 827-831.
48. Atkins, P. W., de Paula, J., and Ludwig, R. (2008) Kurzlehrbuch Physikalische Chemie, Wiley, Weinheim.
49. Lubbers, S., Landy, P., and Voilley, A. (1998) Retention and release of aroma compounds containing proteins, Food Technol. USA 52(68-74), 208-214.
50. Nahon, D. F., Navarro, y., Koren, P. A., Roozen, J. P., and Posthumus, M. A. (1998) Flavor release from mixtures of sodium cyclamate, sucrose, and an orange aroma, J. Agric. Food Chem. 46, 4963-4968.
51. Philippe, E., Seuvre, A., Colas, B., Langendorf, V., Schippa, C., and Voilles, A. (2003) Behaviour of flavour compounds in model food systems: A thermodynamic study, J. Agric. Food Chem. 53, 1393-1398.
52. Hanson, A., Andersson, J., and Leufven, A. (2001) The effect of sugars and pectin on flavour release from a soft drink-related model system, Food Chem. 72, 363.
53. Sorrentino, F., Voilley, A., and Richon, D. (1986) Activity coefficients of aroma compounds in model food systems, AIChE J. 32, 1988-1993.
54. Covarrrubias-Cervantes, M., Champion, F., Debeaufort, F., and Voilley, A. (2004) Aroma volatility from aqueous sucrose solutions at low and subzero temperatures, J. Agric. Food Chem. 52, 7064-7069.
55. Banat, F. A., Abu Al-Rub, F. A., and Simandi, J. (1999) Experimental study of the salt effect in vapor/liquid equlibria using headspace gas chromatography, Chem. Eng. Technol. 22, 761-765.
56. Godshall, M. A. (1997) How carbohydrates influence food flavour, Food Technol. 51, 63-67.
57. O'Neill, T., and Kinsella, J. (1987) Flavor protein interaction: Characterization of 2- nonanone binding to isolated soy protein fractions, J. Food Sci. 52, 98-101.
58. Fischer, N., and Widder, S. (1997) How proteins influence flavor, Food Technol. 51, 68-70.
59. Landy, P., Druaux, C., and Voiley, A. (1995) Retention of aroma compounds by proteins in aqueous solutions, Food Chem. 54, 387-392.
60. Gmehling, J., and Brehm, A. (1996) Grundoperationen-Lehrbuch der Technischen Chemie, Band 2, Georg Thieme, Stuttgart.
61. 61. Hertel, M. (2007) Das Ausdampfverhalten von Aromastoffen während der Würzekochung, dissertation, Technische Universität München, Freising-Weihenstephan.
62. Dohnal, V., Fenclova, D., and Vrbka, P. (2006) Temperature dependence of limiting activity coefficients, Henry's law constants and derivate infinite dilution properties of lower (44 C1-C5) 1-alkanols in water. Critical compilation, correlation and recommended data, J. Phys. Chem. Ref. Data 34, 1621-1651.
63. Osborne, D. W., Doescher, R. N., and Yost, D. M. (1942) The heat capacity, heats of fusion and vaporization, vapor pressure and entropy of dimethyl sulfide, J. Am. Chem. Soc. 64, 169-172.
64. Doering K.-E., and Preuss, H. (1965) FIZ Report 8196, 4121.
65. Aneja, V. (1990) The emission rate of dimethyl sulfide at the atmospheric-oceanic interface, Chem. Eng. Commun. 98, 199-209.
66. Cline, J., and Bates, T. (1983) Dimethyl sulfide in the equatorial pacific ocean: A natural source of sulphur to the atmosphere, Geophys. Res. Lett. 10(10), 949-952.
67. Dacey, J., Wakeham, S., and Howes, B. (1981) Henry's law constants for dimethylsulfide in freshwater and seawater, Geophys. Res. Lett. 11, 991-999.
68. Przyazny, A., Janicki, W., Chrzanowski, W., and Staszewski, R. (1983) Headspace gas chromatographic determination of distribution coefficients of selected organosulphur compounds and their dependence on some parameters, J. Chromatogr. 280, 249-260.
69. Wong, P. K., and Wang, Y. H. (1997) Determination of the Henry's law constant for dimethyl sulfide in seawater, Chemosphere 35(3), 535-544.
70. Iliuta, M., and Larachi, F. (2005) Gas-liquid partition coefficients and Henry's law constants of DMS in aqueous solutions of Fe(II) chelate complexes using the static headspace method, J. Chem. Eng. Data 50, 1700-1705.
71. Coquelet, C., Laurens, S., and Richon, D. (2008) Measurement through a gas stripping technique of Henry's law constants and infinite dilution activity coefficients of propyl mercaptan, butyl mercaptan and dimethyl sulfide in methyldiethanolamine (1)+water (2) with w1=0, 25 and 0, 35, J. Chem. Eng. Data 53, 2540-2543.
72. Bruyn De, W., Swartz, E., Hu, J., Shorter, A., and Davitovits, P. (1995) Henry's law solubilities and Setchenow coefficients for biogenic reduced sulphur species obtained from gas-liquid uptake measurements, J. Geophys. Res. 100(D4), 7245-7251.
73. Hertel, M., Scheuren, H., and Sommer, K. (2007) Limiting separation factors and limiting activity coefficients for hexanal, 2-methylbutanal, 3-methylbutanal, and dimethylsulfide inwater, J. Chem. Eng. Data 52(1), 148-152.
74. Hertel, M., Scheuren, H., and Sommer, K. (2006) Engineering investigations of the vapour-liquid equilibrium of flavour-components at atmospheric wort boiling conditions (98.1 - 99.0°C), BrewingScience - Monatsschrift für Brauwissenschaft 60(11/12), 16-20.
75. Kojima, K., Zhang, S., and Hiaki, T. (1997) Measuring methods of infinite dilution activity coefficients and a database for systems including water, Fluid Phase Equilibria 131, 145-179.
76. Murakami, H., Okada, T., Nitta, T., and Katayama, T. (1987) Gas solubilities of rancid substances in water, Kagaku Kogaku Ronbunshu 13(1), 43-50.
77. Scheuren, H., Dillenburger, M., Tippmann, J., Methner, F.-J., and Sommer, K. (2014) The volatility of dimethyl sulfide in water in infinite dilution measured by Rayleigh distillation and Dohnal method, BrewingScience - Monatsschrift für Brauwissenschaft 67(9/10), 116-119.
78. Scheuren, H., Dillenburger, M., Tippmann, J., Methner, F.-J., and Sommer, K. (2014) The volatility of dimethyl sulfide measured by flash distillation, BrewingScience - Monatsschrift für Brauwissenschaft 67(5/6), 69-71.
79. Vitenberg, A., Ioffe, B., Dimitrova, Z., and Butaeva, I. (1975) Determination of gas-liquid partition coefficients by means of gas chromatographic analysis, J. Chromatogr. 112, 319-327.
80. Williams, I., and Murray, F. (1966) Studies on the gaschromatographic analysis of kraft mill sulphides, Pulp Paper Mag. Canada 347-352.
81. Rayleigh, J. W. S. (1902) On the distillation of binary mixtures, Phil. Mag. 4, 521-537.
82. Emel'yanenko, V. N., Dabrowska, A., Verevkin, S. P., Hertel, M., Scheuren, H., and Sommer, K. (2007) Vapor pressures, enthalpies of vaporization, and limiting activity coefficients in water at 100°C of 2-furanaldehyde, benzaldehyde, phenylethanal, and 2-phenylethanol, J. Chem. Eng. Data 52(2), 468-471.
83. Hertel, M., Scheuren, H., and Sommer, K. (2007) Solubilities of hexanal, benzaldehyde, 2-furfural, 2-phenylethanol, phenylethanal, and γ-nonalactone in water at temperatures between (50 and 100) °C, J. Chem. Eng. Data 52(6), 2143-2145.
84. Hertel, M., and Sommer, K. (2005) Limiting separation factors and limiting activity coefficients for 2-phenylethanol and 2-phenylethanal in water at 100°C, J. Chem. Eng. Data 50(6), 1905-1906.