Demonstration of feasibility of X-ray free electron laser studies of dynamics of nanoparticles in entangled polymer melts

Scientific Reports

Volumn 4, Issue , 2014, Pages

  Carnis, Jerome ^a   Cha, Wonsuk ^a   Wingert, James ^b   Kang, Jinback ^a   Jiang, Zhang ^c   Song, Sanghoon ^d   Sikorski, Marcin ^d   Robert, Aymeric ^d   Gutt, Christian ^e,f,g   Chen, San Wen ^b   Dai, Yeling ^b   Ma, Yicong ^b   Guo, Hongyu ^b   Lurio, Laurence B ^h   Shpyrko, Oleg ^b   Narayanan, Suresh ^c   Cui, Mengmeng ⁱ   Kosif, Irem ⁱ   Emrick, Todd ⁱ   Russell, Thomas P ⁱ   Lee, Hae Cheol ^j   Yu, Chung Jong ^j   Grübel, Gerhard ^e,f   Sinha, Sunil K ^b   Kim, Hyunjung ^a   more..

^a Sogang University   (South Korea)

^b UNIVERSITY OF CALIFORNIA   (United States)

^c ARGONNE NATIONAL LABORATORY   (United States)

^d SLAC NATIONAL ACCELERATOR LABORATORY   (United States)

^e DESY   (Germany)

^f UNIVERSITY OF HAMBURG   (Germany)

^g UNIVERSITY OF SIEGEN   (Germany)

^h NORTHERN ILLINOIS UNIVERSITY   (United States)

ⁱ UNIVERSITY OF MASSACHUSETTS   (United States)

^j Pohang University of Science and Technology (POSTECH)   (South Korea)

more..

Author keywords

[No Author keywords available]

Indexed keywords

EID: 84905911424     PISSN: None     EISSN: 20452322     Source Type: Journal    
DOI: 10.1038/srep06017     Document Type: Article

References (40)

1. Redecke, L. et al. Natively Inhibited Trypanosoma brucei Cathepsin B Structure Determined by Using an X-ray Laser. Science 339, 227-230 (2012).
2. Glover, T. E. et al. X-ray and optical wave mixing. Nature 488, 603-608 (2012).
3. Clark, J. N. et al. Ultrafast Three-Dimensional Imaging of Lattice Dynamics in Individual Gold Nanocrystals. Science 341, 56-59 (2013).
4. Gru?el, G., Stephenson, G. B., Gutt, C., Sinn, H. & Tschentscher, T. XPCS at the European X-Ray free electron laser facility. Nucl. Instrum. Methods Phys. Res. B 262, 357-367 (2007). (Pubitemid 47259546)
5. Saldin, E. L., Schneidmiller, E. A. & Yurkov, M. V. Statistical properties of radiation from VUV and X-ray free electron laser. Opt. Commun. 148, 383-403 (1998). (Pubitemid 128408820)
6. Lee, S. et al. High wavevector temporal speckle correlations at the Linac Coherent Light Source. Opt. Express 20, 9790-9800 (2012).
7. Gutt, C. et al. Single shot Spatial and Temporal Coherence Properties of the SLAC Linac Coherent Light Source in the Hard X-Ray Regime. Phys. Rev. Lett. 108, 024801 (2012).
8. Gutt, C. et al. Measuring temporal speckle correlations at ultrafast X-ray sources. Opt. Express 17, 55-61 (2009).
9. Goodman, J. Speckle Phenomena in Optics: Theory and Application. (Roberts & Company Publishers, Greenwood Village, 2007).
10. Hruszkewycz, S. O. et al.High Contrast X-ray Speckle from Atomic-Scale order in Liquids and Glasses. Phys. Rev. Lett. 109, 185502 (2012).
11. Livet, F. et al. Kinetic evolution of unmixing in an AlLi alloy using X-ray intensity fluctuation spectroscopy. Phys. Rev. E 63, 036108 (2001).
12. Shpyrko, O. G. et al. Direct measurement of antiferromagnetic domain fluctuations. Nature 447, 68-71 (2007). (Pubitemid 46685843)
13. Kim, H. et al. Surface Dynamics of Polymer Films. Phys. Rev. Lett. 90, 068302 (2003).
14. Jiang, Z. et al. Evidence for Viscoelastic Effects in Surface Capillary Waves of Molten Polymer Films. Phys. Rev. Lett. 98, 227801 (2007).
15. Jiang, Z. et al. Entanglement Effects in Capillary Waves on Liquid Polymer Films. Phys. Rev. Lett. 101, 246104 (2008).
16. Stephenson, G. B. et al. LCLS: The First Experiments. www-ssrl.slac.stanford.edu/lcls/papers/lcls-experiments-2.pdf (2000), date of access: 19/07/2014.
17. Roseker, W. et al. Performance of a picosecond X-ray delay line unit at 8.39 keV. Optics Letters 34, 1768-1770 (2009).
18. Roseker, W. et al. Development of a hard X-ray delay line for X-ray photon correlation spectroscopy and jitter-free pump-probe experiments at X-ray freeelectron laser sources. J. Synchrotron Rad. 18, 481-491 (2011).
19. Dixon, P. K.&Durian, D. J. Speckle Visibility Spectroscopy andVariable Granular Fluidization. Phys. Rev. Lett. 90, 184302 (2003).
20. Bandyopadhyay, R., Gittings, A. S., Suh, S. S., Dixon, P. K. & Durian, D. J. Specklevisibility spectroscopy: A tool to study time-varying dynamics. Rev. Sci. Instrum. 76, 093110 (2005).
21. DeCaro, C. et al. X-Ray speckle visibility spectroscopy in the single-photon limit. J. Synchrotron Rad. 20, 332-338 (2012).
22. Robert, A. et al. The X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source. J. Phys.: Conf. Ser. 425, 212009 (2013).
23. Robert, A., Wandersman, E., Dubois, E., Dupuis, V. & Perzynski, R. Glassy dynamics and aging in a dense ferrofluid. Europhy. Lett. 75, 764-770 (2006). (Pubitemid 44369673)
24. Cipelletti, L. & Ramos, L. Slow dynamics in glassy soft matter. J. Phys.: Condens. Matter 17, R253-R285 (2005). (Pubitemid 40296651)
25. Narayanan, S., Lee, D. R., Hagman, A., Li, X. & Wang, J. Particle Dynamics in Polymer-Metal Nanocomposite Thin Films on Nanometer-Length Scales. Phys. Rev. Lett. 98, 185506 (2007).
26. Brown, G., Rikvold, P. A., Sutton, M. & Grant, M. Speckle from phase-ordering systems. Phys. Rev. E 56, 6601-6612 (1997). (Pubitemid 127605701)
27. Malik, A. et al. Coherent X-Ray Study of Fluctuations during Domain Coarsening. Phys. Rev. Lett. 81, 5832-5835 (1998). (Pubitemid 128628272)
28. Solomon, M. J. & Varadan, P. Dynamic structure of thermoreversible colloidal gels of adhesive spheres. Phys. Rev. E 63, 051402 (2001).
29. Bearden, J. A. & Burr, A. F. Reevaluation of X-Ray Atomic Energy Levels. Rev. Mod. Phys. 39, 125-142 (1967).
30. Yeh, J. J. & Lindau, I. Atomic subshell photoionization cross sections and asymmetry parameters: 1 #Z #103. At. Data Nucl. Data Tab. 32, 1-155 (1985).
31. Powell, C. J. & Jablonski, A. Evaluation of Calculated and Measured Electron Inelastic Mean Free Paths Near Solid Surfaces. J. Phys. Chem. Ref. Data 28, 19-62 (1999).
32. Bearden, J. A. X-Ray Wavelengths. Rev. Mod. Phys. 39, 78-142 (1967).
33. Childs, K. D. et al. Handbook of Auger Electron Spectroscopy. [Hedberg, C. L. (ed)] (Physical Electronics, Eden Prairie, 1995).
34. Hubbell et al. A Review, Bibliography, and Tabulation of K, L, and Higher Atomic Shell X-Ray Fluorescence Yields. J. Phys. Chem. Ref. Data 23, 339-364 (1994).
35. Pu, Z. Polymer Data Handbook. [Mark, J. E. (ed)](Oxford University Press, New York, 1999).
36. Plazek, D. J. & O'Rourke, V. M. Viscoelastic Behavior of Low Molecular Weight Polystyrene. J. Polym. Sci. Part A-2 9, 209-243 (1971).
37. Sandy, A. R. L. et al Design and characterization of an undulator beamline optimized for small-angle coherent X-ray scattering at the Advanced Photon Source. J. Synchrotron Rad. 6, 1174-1184 (1999).
38. Amann, J. et al. Demonstration of self-seeding in a hard-X-ray free-electron laser. Nature Photon. 6, 693-698 (2012).
39. Schazel, K. Noise on photon correlation data: I. Autocorrelation functions. Quantum Opt. 2, 287-305 (1990).
40. Sikorski, M., Jiang, Z., Sprung, M., Narayanan, S., Sandy, A. R. & Tieman, B. A graphical user interface for real-time analysis of XPCS using HPC. Nucl. Instrum. Meth Phys. Res. A 649, 234-236 (2011).