Continuous vs. segmented second-dimension system gradients for comprehensive two-dimensional liquid chromatography of sugarcane (Saccharum spp.)

Analytical and Bioanalytical Chemistry

Volumn 406, Issue 18, 2014, Pages 4315-4324

  Leme, Gabriel Mazzi ^a,b   Cacciola, Francesco ^a   Donato, Paola ^a,c   Cavalheiro, Alberto José ^b   Dugo, Paola ^a,c   Mondello, Luigi ^a,c  

^a UNIVERSITY OF MESSINA   (Italy)

^b SÃO PAULO STATE UNIVERSITY UNESP   (Brazil)

^c UNIVERSITY CAMPUS BIO MEDICO   (Italy)

Author keywords

Comprehensive two dimensional liquid chromatography; Cyano column; Mass spectrometry; Polyphenols; Sugarcane

Indexed keywords

CHROMATOGRAPHY; INDUCTIVELY COUPLED PLASMA; ISOTOPES; MASS SPECTROMETRY; PHOTODIODES; SUGAR CANE; TWO DIMENSIONAL;

COMPLEMENTARY DATA; COMPREHENSIVE TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY; CYANO COLUMNS; GRADIENT ELUTION MODE; IN-HOUSE DATABASE; POLYPHENOLS; REVERSED-PHASE COLUMNS; SATISFACTORY DEGREE;

HIGH PRESSURE LIQUID CHROMATOGRAPHY;

SACCHARUM;

PLANT EXTRACT; POLYPHENOL;

CHEMISTRY; DEVICES; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PLANT LEAF; PROCEDURES; SUGARCANE;

CHROMATOGRAPHY, LIQUID; MASS SPECTROMETRY; PLANT EXTRACTS; PLANT LEAVES; POLYPHENOLS; SACCHARUM;

EID: 84903766951     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-014-7786-8     Document Type: Article

References (43)

1. CONAB Companhia Nacional de Abastecimento (2013). Conab - Companhia Nacional de Abastecimento. http://www.conab.gov.br/. Accessed 29 Nov 2013
2. Li X, Shun Y, Bin T, Xue L, Chunmei J, Hang S (2010) Determination and comparison of flavonoids and anthocyanins in Chinese sugarcane tips, stems, roots and leaves. J Sep Sci 33:1216-1223
3. Colombo R, Yariwake JH, Queiroz EF, Ndjoko K, Hostettmann K (2005) On-line identification of sugarcane (Saccharum officinarum L.) methoxyflavones by liquid chromatography-UV detection using post-column derivatization and liquid chromatography-mass spectrometry. J Chromatogr A 1082:51-59
4. Colombo R, Yariwake JH, Queiroz EF, Ndjoko K, Hostettmann K (2006) On-line identification of further flavone C- and O-glycosides from Sugarcane (Saccharum officinarum L., Gramineae) by HPLC-UV-MS. Phytochem Anal 17:337-343
5. Colombo R, Yariwake JH, Mccullaghb M (2008) Study of C- and O-glycosylflavones in sugarcane extracts using liquid chromatography-exact mass measurement mass spectrometry. J Braz Chem Soc 19:483-490
6. Cavalheiro AJ, Coutinho ID, Leme GM, Silva AA, Silva APD (2012) In: Stradiotto NR, Lemos EG (eds) Bioenergia: pesquisa, desenvolvimento e inovação. São Paulo, Cultura Acadêmica
7. Uysal UD, Aturki Z, Raggi MA, Fanali S (2009) Separation of catechins and methylxanthines in tea samples by capillary electrochromatography. J Sep Sci 32:1002-1010
8. Iacopini P, Baldi M, Storchi P, Sebastian L (2008) Catechin, epicatechin, quercetin, rutin and resveratrol in red grape: content, in vitro antioxidant activity and interactions. J Food Compos Anal 21:589-598
9. Dugo P, Cacciola F, Kumm T, Dugo G, Mondello L (2008) Comprehensive multidimensional liquid chromatography: theory and applications. J Chromatogr A 1184:353-368
10. Stoll DR (2010) Recent progress in online, comprehensive two-dimensional high-performance liquid chromatography for non-proteomic applications. Anal Bional Chem 397:979-986
11. François I, Sandra K, Sandra P (2009) Comprehensive liquid chromatography: fundamental aspects and practical considerations - a review. Anal Chim Acta 641:14-31
12. Donato P, Cacciola F, Tranchida PQ, Dugo P, Mondello L (2012) Mass spectrometry detection in comprehensive liquid chromatography: Basic concepts, instrumental aspects, applications and trends. Mass Spectrom Rev 31:523-559
13. Blahovà E, Jandera P, Cacciola F, Mondello L (2006) Two-dimensional and serial column reversed-phase separation of phenolic antioxidants on octadecyl-, polyethyleneglycol-, and pentafluorophenylpropyl- silica columns. J Sep Sci 29:555-566
14. Cacciola F, Jandera P, Blahovà E, Mondello L (2006) Development of different comprehensive two dimensional systems for the separation of phenolic antioxidants. J Sep Sci 29:2500-2513
15. François I, de Villers A, Sandra P (2006) Considerations on the possibilities and limitations of comprehensive normal phase-reversed phase liquid chromatography (NPLC×RPLC). J Sep Sci 29:492-498
16. Cacciola F, Jandera P, Mondello L (2007) Temperature effects on separation on zirconia columns: Applications to one- and two-dimensional LC separations of phenolic antioxidants. J Sep Sci 30:462-474
17. Cacciola F, Jandera P, Mondello L (2007) Comparison of high-temperature gradient heart-cutting and comprehensive LC×LC systems for the separation of phenolic antioxidants. Chromatographia 66:661-667
18. Cacciola F, Jandera P, Hajdù Z, Česla P, Mondello L (2007) Comprehensive two-dimensional liquid chromatography with parallel gradients for separation of phenolic and flavone antioxidants. J Chromatogr A 1149:73-87
19. Montero L, Herrero M, Prodanov M, Ibanàñez E, Cifuentes A (2013) Characterization of grape seed procyanidins by comprehensive two-dimensional hydrophilic interaction×reversed phase liquid chromatography coupled to diode array detection and tandem mass spectrometry. Anal Bioanal Chem 405:4627-4638
20. Kivilompolo M, Hyötyläinen T (2007) Comprehensive two-dimensional liquid chromatography in analysis of Lamiaceae herbs: characterisation and quantification of antioxidant phenolic acids. J Chromatogr A 1145:155-164
21. Dugo P, Cacciola F, Herrero M, Donato P, Mondello L (2008) Use of partially porous column as second dimension in comprehensive two-dimensional system for analysis of polyphenolic antioxidants. J Sep Sci 31:3297-3308
22. Hájek T, Škeříková V, Česla P, Vyňuchalová K, Jandera P (2008) Multidimensional LC×LC analysis of phenolic and flavone natural antioxidants with UV-electrochemical coulometric and MS detection. J Sep Sci 31:3309-3328
23. Kivilompolo M, Obůrka V, Hyötyläinen T (2008) Comprehensive two-dimensional liquid chromatography in the analysis of antioxidant phenolic compounds in wines and juices. Anal Bioanal Chem 391:373-380
24. François I, de Villiers A, Tienpont B, David F, Sandra P (2008) Comprehensive two-dimensional liquid chromatography applying two parallel columns in the second dimension. J Chromatogr A 1178:33-42
25. Dugo P, Cacciola F, Donato P, Airado-Rodriguez D, Herrero M, Mondello L (2009) Comprehensive two-dimensional liquid chromatography to quantify polyphenols in red wines. J Chromatogr A 1216:7483-7487
26. Dugo P, Cacciola F, Donato F, Jacques RA, Caramao EB, Mondello L (2009) High efficiency liquid chromatography techniques coupled to mass spectrometry for the characterization of mate extracts. J Chromatogr A 1216:7213-7221
27. Česla P, Hájek T, Jandera P (2009) Optimization of two-dimensional gradient liquid chromatography separations. J Chromatogr A 1216:3443-3457
28. Kalili KM, de Villiers A (2009) Off-line comprehensive 2-dimensional hydrophilic interaction×reversed phase liquid chromatography analysis of procyanidins. J Chromatogr A 1216:6274-6284
29. Jandera P, Hájek T, Česla P (2010) Comparison of various second-dimension gradient types in comprehensive two-dimensional liquid chromatography. J Sep Sci 33:1382-1397
30. Mnatsakanyan M, Stevenson PG, Shock D, Conlan XA, Goodie TA, Spencer KN, Barnett NW, Francis PS, Shalliker RA (2010) The assessment of π-π selective stationary phases for two-dimensional HPLC analysis of foods: application to the analysis of coffee. Talanta 82:1349-1347
31. Kalili KM, de Villiers A (2010) Off-line comprehensive two-dimensional hydrophilic interaction×reversed phase liquid chromatographic analysis of green tea phenolics. J Sep Sci 33:853-863
32. Russo M, Cacciola F, Bonaccorsi I, Dugo P, Mondello L (2011) Determination of flavanones in CITRUS juices by means of one-and two-dimensional liquid chromatography. J Sep Sci 34:681-687
33. Scoparo CT, Souza LM, Dartora N, Sassaki GL, Gorin PAJ, Iacomini M (2012) Analysis of Camellia sinensis green and black teas via ultra high performance liquid chromatography assisted by liquid-liquid partition and two-dimensional liquid chromatography (size exclusion×reversed phase). J Chromatogr A 1222:29-37
34. Beelders T, Kalili KM, Joubert E, Beer D, de Villiers A (2012) Comprehensive two-dimensional liquid chromatographic analysis of rooibos (Aspalathus linearis) phenolics. J Sep Sci 35:1808-1820
35. Pòl J, Hohnovà B, Hyötyläinen T (2007) Characterisation of Stevia rebaudiana by comprehensive two-dimensional liquid chromatography time-of-flight mass spectrometry. J Chromatogr A 1150:85-92
36. Cacciola F, Delmonte P, Jaworska K, Dugo P, Mondello L (2011) Employing ultra high pressure liquid chromatography as the second dimension in a comprehensive two-dimensional system for analysis of Stevia rebaudiana extracts. J Chromatogr A 1218:2012-2018
37. Funari CS, Carneiro RL, Andrade AM, Hilder EF, Cavalheiro AJ (2013) Green chromatographic fingerprinting: an environmentally friendly approach for the development of separation methods for fingerprinting complex matrices. J Sep Sci 37:37-44
38. Murphy RE, Schure MR, Foley JP (1998) Effect of sampling rate on resolution in comprehensive two-dimensional liquid chromatography. Anal Chem 70:1585-1594
39. Snyder LR, Kirkland JJ, Loyd JW (2010) Introduction to modern liquid chromatography. Wiley, Totowa
40. Jandera P (2012) Programmed elution in comprehensive two-dimensional liquid chromatography. J Chromatogr A 1255:112-129
41. Neue UW (2005) Theory of peak capacity in gradient elution. J Chromatogr A 1079:153-161
42. Gu H, Huang Y, Carr PW (2011) Peak capacity optimization in comprehensive two dimensional liquid chromatography: a practical approach. J Chromatogr A 1218:64-73
43. Liu Z, Patterson DG, Lee ML (1995) Geometric approach to factor analysis for the estimation of orthogonality and practical peak capacity in comprehensive two-dimensional separations. Anal Chem 67:3840-3845