Application of a high resolution benchtop quadrupole-Orbitrap mass spectrometry for the rapid screening, confirmation and quantification of illegal adulterated phosphodiesterase-5 inhibitors in herbal medicines and dietary supplements

Journal of Chromatography A

Volumn 1344, Issue , 2014, Pages 91-98

  Shi, Feng ^a   Guo, Changchuan ^a   Gong, Liping ^a   Li, Jun ^a   Dong, Peng ^a   Zhang, Jinling ^b   Cui, Ping ^c   Jiang, Shuyin ^a   Zhao, Yanxia ^a   Zeng, Su ^d  

^a SHANDONG INSTITUTE FOR FOOD AND DRUG CONTROL   (China)

^b People's Hospital of Linyi City   (China)

^c Thermo Fisher Scientific   (United States)

^d ZHEJIANG UNIVERSITY   (China)

Author keywords

Illegal adulteration; Orbitrap; Phosphodiesterase 5 inhibitors; Qualitation; Quantitation; Screening

Indexed keywords

CHEMICAL ANALYSIS; CRIME; DIETARY SUPPLEMENTS; ESTERS; MASS SPECTROMETRY; MEDICINE; NUTRITION; PLANT EXTRACTS; SCREENING; VITAMINS;

ILLEGAL ADULTERATION; ORBITRAP; PHOSPHODIESTERASE 5 INHIBITORS; QUALITATION; QUANTITATION;

FOOD ADDITIVES;

ACETILDENAFIL; AMINOTADALAFIL; HOMOSILDENAFIL; HYDROXYHOMOSILDENAFIL; NORACETILDENAFIL; NORNEOSILDENAFIL; PHOSPHODIESTERASE V INHIBITOR; PIPERIDENAFIL; SILDENAFIL; TADALAFIL; THIOAILDENAFIL; UNCLASSIFIED DRUG; VARDENAFIL;

ANALYTIC METHOD; ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DIET SUPPLEMENTATION; HERBAL MEDICINE; LIMIT OF DETECTION; MASS SPECTROMETER; MASS SPECTROMETRY; MEASUREMENT ACCURACY; MEASUREMENT PRECISION; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; SIGNAL NOISE RATIO; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY;

ILLEGAL ADULTERATION; ORBITRAP; PHOSPHODIESTERASE-5 INHIBITORS; QUALITATION; QUANTITATION; SCREENING;

DIETARY SUPPLEMENTS; DRUG CONTAMINATION; HERBAL MEDICINE; MASS SPECTROMETRY; PHOSPHODIESTERASE 5 INHIBITORS; PIPERAZINES; PLANT EXTRACTS; PURINES; SULFONES;

EID: 84899896620     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.12.030     Document Type: Article

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