Preparation of graphene oxide and characterisation using electron spectroscopy

Journal of Electron Spectroscopy and Related Phenomena

Volumn 193, Issue , 2014, Pages 92-99

  Lesiak, B ^a   Stobinski, L ^a   Malolepszy, A ^b   Mazurkiewicz, M ^b   Kover L ^c   Toth J ^c  

^a INSTITUTE OF PHYSICAL CHEMISTRY   (Poland)

^b WARSAW UNIVERSITY OF TECHNOLOGY   (Poland)

^c INSTITUTE OF NUCLEAR RESEARCH ATOMKI   (Hungary)

Author keywords

Graphene; Graphene oxidation; Graphene oxide; REELS; XPS

Indexed keywords

ELECTRON ENERGY ANALYZERS; ELECTRON ENERGY LOSS SPECTROSCOPY; ENERGY DISSIPATION; FUNCTIONAL GROUPS; INTERCALATION; OXIDATION; OZONE; OZONE WATER TREATMENT; OZONIZATION; PHOTOELECTRONS; PLASMAS; PLATELETS; REELS; X RAY PHOTOELECTRON SPECTROSCOPY;

AVERAGE NUMBERS; CHEMICAL METHOD; GRAPHENE OXIDES; GRAPHENE PLATELETS; INTENSITY RATIO; OXYGEN FUNCTIONAL GROUPS; QUANTITATIVE INFORMATION; REFLECTION ELECTRON ENERGY LOSS SPECTROSCOPIES;

GRAPHENE;

EID: 84899036155     PISSN: 03682048     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.elspec.2014.03.015     Document Type: Article

References (45)

1. K.S. Novoselov, A.K. Geim, S.V. Morozov, D. Jiang, Y. Zhang, S.V. Dubonos, I.V. Grigorieva, and A.A. Firsov Electric field effect in atomically thin carbon films Science 306 2004 666 669
2. J. Campos-Delgado, J.M. Romo-Herrera, X. Jia, D.A. Cullen, H. Muramatsu, Y.A. Kim, T. Hayashi, Zh. Ren, D.J. Smith, Y. Okuno, T. Ohba, H. Kanoh, K. Kaneko, M. Endo, H. Terrones, M.S. Dresselhaus, and M. Terrones Bulk production of a new form of sp2 carbon: crystalline graphene nanoribbons Nano Lett. 8 2008 2773 2778
3. D.V. Kosynkin, A.L. Higginbotham, A. Sinitskii, J.R. Lomeda, A. Dimiev, B.K. Price, and J.M. Tour Longitudinal unzipping of carbon nanotubes to form graphene nanoribbons Nature 458 2009 872 876
4. A. Yu, P. Ramesh, M.E. Itkis, E. Bekyarova, and R.C. Haddon Graphite nanoplatelet-epoxy composite thermal interface materials J. Phys. Chem. C 111 2007 7565 7569
5. B.C. Brodie Sur le poids atomique du graphite Ann. Chim. Phys. 59 1860 466 471
6. L. Staudenmaier Verfahren zur Darstellung der Graphitsäure Ber. Dtsch. Chem. Ges. 31 1898 1481 1487
7. U. Hofmann, and E. Konig Untersuchungen über Graphitoxyd Z. Anorg. Allg. Chem. 234 1937 311 336
8. U. Hofmann, and R. Hoist Über die Säurenatur und die Methylierung von Graphitoxyd Ber. Dtsch. Chem. Ges. 72 1939 754 771
9. W.S. Hummers, and R.E. Offeman Preparation of graphitic oxide J. Am. Chem. Soc. 80 1958 1339
10. B. Dai, L. Fu, L. Liao, N. Liu, K. Yan, Y. Chen, and Zh. Liu High-quality single-layer graphene via reparative reduction of graphene oxide Nano Res. 4 2011 434 439
11. O. Fellahi, M.R. Das, Y. Coffinier, S. Szunerits, T. Hadjersi, M. Maamachee, and R. Boukherroub Silicon nanowire arrays-induced graphene oxide reduction under UV irradiation Nanoscale 3 2011 4662 4669
12. I. Kaminska, M.R. Das, Y. Coffinier, J. Niedziolka-Jonsson, P. Woisel, M. Opallo, S. Szunerits, and R. Boukherroub Preparation of graphene/ tetrathiafulvalene nanocomposite switchable surfaces Chem. Commun. 48 2012 1221 1223
13. L.-Q. Xu, Y.-L. Liu, K.-G. Neoh, E.-T. Kang, and G.-D. Fu Reduction of graphene oxide by aniline with its concomitant oxidative polymerisation Macromol. Rapid Commun. 32 2011 684 688
14. T. Eberlein, U. Bangert, R.R. Nair, R. Jones, M. Gass, A.L. Bleloch, K.S. Novoselov, A. Geim, and P.R. Briddon Plasmon spectroscopy of free-standing graphene films Phys. Rev. B 77 2008 233406 233414
15. P. Johari, and V.B. Shenoy Modulating optical properties of graphene oxide: role of prominent functional groups ACS Nano 5 2011 7640 7647
16. H.L. Poh, F. Šaněk, A. Ambrosi, G. Zhao, Z. Soferb, and M. Pumera Graphenes prepared by Staudenmaier, Hofmann and Hummers methods with consequent thermal exfoliation exhibit very different electrochemical properties Nanoscale 4 2012 3515 3522
17. S.-J. Park, J.-H. An, J.R. Potts, A. Velamakanni, Sh. Murali, and R.S. Ruoff Hydrazine-reduction of graphite and graphene oxide Carbon 49 2011 3019 3023
18. R.-F. Nie, J.-H. Wang, L. Wang, Y. Qin, P. Chen, and Zh.-Y. Hou Platinum supported on reduced graphene oxide as a catalyst for hydrogenation of nitroarenes Carbon 50 2012 586 596
19. L. Calliari, S. Fanchenko, and M. Filippi Plasmon features in electron energy loss spectra from carbon materials Carbon 45 2007 1410 1418
20. L. Stobinski, H.-M. Lin, and P. Tomasik Peaks of the tips removal of well-aligned carbon nanotubes with the glow air plasma Synth. Met. 135-136 2003 741 742
21. Ch.-Y. Lii, Ch.-D. Liao, L. Stobinski, and P. Tomasik Behaviour of granular starches in low-pressure glow plasma Carbohydr. Polym. 49 2002 499 507
22. L. Kövér, D. Varga, I. Cserny, J. Tóth, and K. Tokési Some applications of high-energy, high-resolution Auger electron spectrosocopy using bremsstrahlung radiation Surf. Interface Anal. 19 1992 9 15
23. S. Tougaard, Background analysis of XPS/AES. QUASES Simple Background, Ver. 2.2, Copyright 1994-2001; http://www.tougaard.com.
24. M. Mohai XPS multiquant. Multimodel XPS quantification software Surf. Interface Anal. 36 2004 828 832 M. Mohai, Multimodel X-ray photoelectron spectroscopy quantification program for 32-bit Windows, XPS MultiQuant, ver. 7, 1999-2001
25. J.H. Scofield Hatree-Fock subshell photoionization cross-section at 1254 and 1487 eV J. Electron Spectrosc. Relat. Phenom. 8 1976 129 137
26. A. Jablonski, and J. Zemek Overlayer thickness determination by XPS using the multiline approach Surf. Interface Anal. 41 2009 193 204
27. R.W.M. Kwok XPS Peak Fitting Program for WIN95/98 XPSPEAK Version 4.1 2000 Department of Chemistry, The Chinese University of Hong Kong http://www.uksaf.org/software.html, XPSPEAK4.1
28. R. Hesse, P. Streubel, and R. Szargan Product or sum: comparative test of Voigt, and product or sum of Gaussian and Lorentzian functions in the fitting of synthetic Voigt-based X-ray photoelectron spectra Surf. Interface Anal. 39 2007 381 391
29. S. Rey, and F. Le Normand Surface transformations of carbon (graphene, graphite, diamond, carbide), deposited on polycrystalline nickel by hot filaments chemical vapour deposition Thin Solid Films 519 2011 4426 4428
30. Yu. V. Butenko, A.K. Krishnamurthy, V.L. Chakraborty, V.L. Kuznetsov, V.R. Dhanak, M.R.C. Hunt, and L. Šiller Photoemission study of onionlike carbons produced by annealing nanodiamonds Phys. Rev. B 71 2005 075420 75510
31. S.H. Shim, K.T. Kim, J.U. Lee, and W.H. Jo Facile method to functionalize graphene oxide and its application to poly(ethylene terephthalate)/graphene composite ACS Appl. Mater. Interfaces 4 2012 4184 4191
32. P. Solís-Fernández, J.I. Paredes, A. Cosío, A. Martínez-Alonso, and J.M.D. Tascón A comparison between physically and chemically driven etching in the oxidation of graphite surfaces J. Colloid Interface Sci. 344 2010 451 459
33. M.R. Cuervoa, E. Asedegbega-Nietoa, E. Díaz, S. Ordóñez, A. Vega, A.B. Dongil, and I. Rodríguez-Ramos Modification of the adsorption properties of high surface area graphites by oxygen functional groups Carbon 46 2008 2096 2106
34. X. Liu, Ch. Yang, and Y. Lu Contrastive study of anodic oxidation on carbon fibers and graphite fibers Appl. Surf. Sci. 258 2012 4268 4275
35. P. Krawczyk Effect of ozone treatment on properties of expanded graphite Chem. Eng. J. 172 2011 1096 1102
36. Sh. Kundu, Y.-M. Wang, W. Xia, and M. Muhler Thermal stability and reducibility of oxygen-containing functional groups on multiwalled carbon nanotube surfaces: a quantitative high-resolution XPS and TPD/TPR study J. Phys. Chem. C 112 2008 16869 16878
37. W.G. Hong, B.H. Kim, S. Moon Lee, H.Y. Yu, Y.J. Yun, Y.-S. Jun, J.B. Lee, and H.J. Kim Agent-free synthesis of graphene oxide/transition metal oxide composites and its application for hydrogen storage Int. J. Hydrogen Energy 37 2012 7594 7599
38. C.D. Wagner, A.V. Naumkin, A. Kraut-Vass, J.W. Allison, C.J. Powell, and J.R. Rumble Jr. NIST X-ray photoelectron database, NIST SRD 20, ver. 4.1, online PC 2003
39. H.A.E. Hagelin-Weaver, J.F. Weaver, G.B. Hoflund, and G.N. Salaita Electron energy loss spectroscopic investigation of polycrystalline Au, Pd and a Pd-Au alloy J. Alloys Compd. 393 2005 93 99
40. S. Tanuma, C.J. Powell, and D.R. Penn Calculations of electron inelastic mean free paths. IX. Data for 41 elemental solids over the 50 eV to 30 keV range Surf. Interface Anal. 43 2011 689 713
41. A. Jablonski, and C.J. Powell Practical expressions for the mean escape depth, the information depth, and the effective attenuation length in Auger-electron spectroscopy and X-ray photoelectron spectroscopy J. Vac. Sci. Technol. A 27 2009 253 261
42. A. Jablonski, and C.J. Powell Information depth for elastic-peak electron spectroscopy Surf. Sci. 551 2004 106 124
43. J. Zemek, K. Olejnik, and P. Klapetek Photoelectron spectroscopy from randomly corrugated surfaces Surf. Sci. 602 2008 1440 1446
44. A. Jablonski, K. Olejnik, and J. Zemek Elastic electron backscattering from flat and rough Si surfaces J. Electron Spectrosc. Relat. Phenom. 152 2006 100 106
45. B. Strawbridge, R.K. Singh, C. Beach, A. Mahajan, and N. Newman Effect of surface topography on reflection electron energy loss plasmon spectra of group III metals J. Vac. Sci. Technol. A 24 2006 1776 1781