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CCDC 928824 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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CCDC 928824 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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1H NMR experiments at high temprature showed that the coupling products 2b-i are atropoconfigurationnaly stable up to at least 100 8C.
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1H NMR experiments at high temprature showed that the coupling products 2b-i are atropoconfigurationnaly stable up to at least 100 8C.
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