메뉴 건너뛰기




Volumn 89, Issue 7, 2012, Pages 1211-1222

Development and validation of an HPLC-DAD method for analysis of the six major isoflavones in extracts from soybean processing

Author keywords

HPLC; Isoflavones; Quantification; Soy; Soy molasses; Soybean; Soybean meal

Indexed keywords

HPLC; ISOFLAVONES; QUANTIFICATION; SOY; SOYBEAN; SOYBEAN MEAL;

EID: 84863776205     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11746-012-2030-1     Document Type: Article
Times cited : (13)

References (48)
  • 1
    • 0036211515 scopus 로고    scopus 로고
    • Effects of processing on the content and composition of isoflavones during manufacturing of soy beverage and tofu
    • Jackson C-JC, Dini JP, Lavandier C, Rupasinghe HPV, Faulkner H, Poysa V, Buzzell D, DeGrandis S (2002) Effects of processing on the content and composition of isoflavones during manufacturing of soy beverage and tofu. Process Biochem 37:1117-1123
    • (2002) Process Biochem , vol.37 , pp. 1117-1123
    • C-Jc, J.1    Dini, J.P.2    Lavandier, C.3    Hpv, R.4    Faulkner, H.5    Poysa, V.6    Buzzell, D.7    Degrandis, S.8
  • 2
    • 0028815434 scopus 로고
    • Effect of genistein on in vitro and in vivo models of cancer
    • Barnes S (1995) Effect of genistein on in vitro and in vivo models of cancer. J Nutr 125:777-783
    • (1995) J Nutr , vol.125 , pp. 777-783
    • Barnes, S.1
  • 5
    • 0015093318 scopus 로고
    • Separation of soybean isoflavones from their 5-hydroxy derivatives by thin-layer chromatography
    • Wang LC (1971) Separation of soybean isoflavones from their 5-hydroxy derivatives by thin-layer chromatography. Anal Biochem 42:296-298
    • (1971) Anal Biochem , vol.42 , pp. 296-298
    • Wang, L.C.1
  • 6
    • 38949158452 scopus 로고    scopus 로고
    • Rfeti Determinação de daidzeína, genisteína e gliciteína em cápsulas de isoflavonas por Cromatografia em Camada Delgada (CCD) e Cromatografia Líquida de Alta Eficiência (CLAE)
    • Cesar IC, Braga FC, Vianna-Soares CD, Nunan EA, Barbosa TAF, Moreira-Campos LM (2007) Determinação de daidzeína, genisteína e gliciteína em cápsulas de isoflavonas por Cromatografia em Camada Delgada (CCD) e Cromatografia Líquida de Alta Eficiência (CLAE). Braz J Pharmacogn 17:616-625
    • (2007) Braz J Pharmacogn , vol.17 , pp. 616-625
    • Cesar, I.C.1    Braga, F.C.2    Vianna-Soares, C.D.3    Nunan, E.A.4    Taf, B.5    Moreira-Campos, L.M.6
  • 7
    • 84863774721 scopus 로고    scopus 로고
    • TLC and HPLC analysis of soy isoflavones in semen sojae praeparatum
    • Yuana D, Chena Y, Baia X, Pana Y, Kanob Y (2006) TLC and HPLC analysis of soy isoflavones in Semen Sojae Praeparatum. Asian J Trad Med 1:3-4
    • (2006) Asian J Trad Med , vol.1 , pp. 3-4
    • Yuana, D.1    Chena, Y.2    Baia, X.3    Pana, Y.4    Kanob, Y.5
  • 8
    • 84863775308 scopus 로고    scopus 로고
    • Determinação de genisteína e genistina por espectrofotometria de UV-Visível em extratos secos de soja utilizados como matéria-prima em farmácias de manipulação
    • Nissola C, Hess B, de Francisco TMG, Gasparetto JC, Campos FR, Pontarolo R (2011) Determinação de genisteína e genistina por espectrofotometria de UV-Visível em extratos secos de soja utilizados como matéria-prima em farmácias de manipulação. Visão Acadêmica 11:35-41
    • (2011) Visão Acadêmica , vol.11 , pp. 35-41
    • Nissola, C.1    Hess, B.2    De Francisco Tmg3    Gasparetto, J.C.4    Campos, F.R.5    Pontarolo, R.6
  • 9
    • 1942542356 scopus 로고    scopus 로고
    • Determination of isoflavones in soy products by capillary electrophoresis with electrochemical detection
    • Peng Y, Chu Q, Liu F, Ye J (2004) Determination of isoflavones in soy products by capillary electrophoresis with electrochemical detection. Food Chem 87:135-139
    • (2004) Food Chem , vol.87 , pp. 135-139
    • Peng, Y.1    Chu, Q.2    Liu, F.3    Ye, J.4
  • 10
    • 0016110006 scopus 로고
    • Soybean isoflavones. Characterization, determination, and antifungal activity
    • Naim M, Gestetner B, Zilkah S, Birk Y, Bondi A (1974) Soybean isoflavones. Characterization, determination, and antifungal activity. J Agric Food Chem 22:806-810
    • (1974) J Agric Food Chem , vol.22 , pp. 806-810
    • Naim, M.1    Gestetner, B.2    Zilkah, S.3    Birk, Y.4    Bondi, A.5
  • 11
    • 77955867875 scopus 로고    scopus 로고
    • Analysis of soy isoflavones in foods and biological fluids: An overview
    • Hsu B, Inbaraj BS, Chen BH (2010) Analysis of soy isoflavones in foods and biological fluids: an overview. J Food Drug Anal 18: 141-154
    • (2010) J Food Drug Anal , vol.18 , pp. 141-154
    • Hsu, B.1    Inbaraj, B.S.2    Chen, B.H.3
  • 12
    • 0000352284 scopus 로고
    • Size exclusion chromatography of soybean proteins and isoflavones
    • Cole KD, Cousin SL Jr (1994) Size exclusion chromatography of soybean proteins and isoflavones. J Agric Food Chem 42: 2713-2720
    • (1994) J Agric Food Chem , vol.42 , pp. 2713-2720
    • Cole, K.D.1    Cousin Jr., S.L.2
  • 14
    • 0017873404 scopus 로고
    • Separation of the isomeric isoflavones from soybeans by high-performance liquid chromatography
    • West LG, Birac PM, Pratt DE (1978) Separation of the isomeric isoflavones from soybeans by high-performance liquid chromatography. J Chromatogr 150:266-268
    • (1978) J Chromatogr , vol.150 , pp. 266-268
    • West, L.G.1    Birac, P.M.2    Pratt, D.E.3
  • 15
    • 33751554020 scopus 로고
    • A simplified HPLC method for the determination of phytoestrogens in soybean and its processed products
    • Wang G, Kuan SS, Francis OJ, Ware GM, Carman AS (1990) A simplified HPLC method for the determination of phytoestrogens in soybean and its processed products. J Agric Food Chem 38: 185-190
    • (1990) J Agric Food Chem , vol.38 , pp. 185-190
    • Wang, G.1    Kuan, S.S.2    Francis, O.J.3    Ware, G.M.4    Carman, A.S.5
  • 18
    • 33645799944 scopus 로고    scopus 로고
    • Quantification of soy isoflavones in meat products by HPLC
    • Vranová D (2005) Quantification of soy isoflavones in meat products by HPLC. Scripta Medica 78:235-242
    • (2005) Scripta Medica , vol.78 , pp. 235-242
    • Vranová, D.1
  • 19
    • 78651438188 scopus 로고    scopus 로고
    • Simultaneous determination four isoflavones in soybean extraction
    • Han GM, Zhang YY, Wang YZ (2007) Simultaneous determination four isoflavones in soybean extraction. J US-China Med Sci 4:53-60
    • (2007) J US-China Med Sci , vol.4 , pp. 53-60
    • Han, G.M.1    Zhang, Y.Y.2    Wang, Y.Z.3
  • 20
    • 84863782661 scopus 로고    scopus 로고
    • HPLC analysis coupled with diode array detector used in determination of isoflavone aglycones from different Romanian varieties of soybeans
    • Neacsu M, Vicas S, Socaciu C (2008) HPLC analysis coupled with diode array detector used in determination of isoflavone aglycones from different Romanian varieties of soybeans. Bulletin UASVM Agriculture 65:310-315
    • (2008) Bulletin UASVM Agriculture , vol.65 , pp. 310-315
    • Neacsu, M.1    Vicas, S.2    Socaciu, C.3
  • 21
    • 40649107466 scopus 로고    scopus 로고
    • Quantification of daidzein, genistein and fatty acids in soybeans and soy sprouts, and some bioactivity studies
    • Orhan I, Ozçelik B, Kartal M, Aslan S, Sene B, Ozguven M (2007) Quantification of daidzein, genistein and fatty acids in soybeans and soy sprouts, and some bioactivity studies. Acta Biol Cracov 49:61-68
    • (2007) Acta Biol Cracov , vol.49 , pp. 61-68
    • Orhan, I.1    Ozçelik, B.2    Kartal, M.3    Aslan, S.4    Sene, B.5    Ozguven, M.6
  • 23
    • 21144450085 scopus 로고    scopus 로고
    • Determination of isoflavones in commercial soy products by HPLC and coulometric electrode array detection
    • Preinerstorfer B, Sontag G (2004) Determination of isoflavones in commercial soy products by HPLC and coulometric electrode array detection. Eur Food Res Technol 219:305-310
    • (2004) Eur Food Res Technol , vol.219 , pp. 305-310
    • Preinerstorfer, B.1    Sontag, G.2
  • 24
    • 33646266945 scopus 로고    scopus 로고
    • Development and validation of a RP-HPLC method for quantification of isoflavone aglycones in hydrolyzed soy dry extracts
    • César IC, Braga FC, Soares CDV, Nunan EA, Pianetti GA, Condessa FA, Barbosa TAF, Campos LMM (2006) Development and validation of a RP-HPLC method for quantification of isoflavone aglycones in hydrolyzed soy dry extracts. J Chromatogr B 836:74-78
    • (2006) J Chromatogr B , vol.836 , pp. 74-78
    • César, I.C.1    Braga, F.C.2    Cdv, S.3    Nunan, E.A.4    Pianetti, G.A.5    Condessa, F.A.6    Taf, B.7    Lmm, C.8
  • 26
    • 0002441297 scopus 로고    scopus 로고
    • Determinação de isoflavonas em derivados de soja
    • Genovese MI, Lajolo FM (2001) Determinação de isoflavonas em derivados de soja. Cienc Tecnol Aliment 21:86-93
    • (2001) Cienc Tecnol Aliment , vol.21 , pp. 86-93
    • Genovese, M.I.1    Lajolo, F.M.2
  • 27
    • 79959744385 scopus 로고    scopus 로고
    • Isoflavone concentration of soybean in central Europe as determined by HPLC/UV analysis before and after acid hydrolysis
    • Hornig A, Lorbeer E, Vollmann J (2011) Isoflavone concentration of soybean in central Europe as determined by HPLC/UV analysis before and after acid hydrolysis. Acta Alimentaria 40: 247-253
    • (2011) Acta Alimentaria , vol.40 , pp. 247-253
    • Hornig, A.1    Lorbeer, E.2    Vollmann, J.3
  • 28
    • 2342636477 scopus 로고    scopus 로고
    • A simplified HPLC method for total isoflavones in soy products
    • Penalvo JL, Nurmi T, Adlercreutz H (2004) A simplified HPLC method for total isoflavones in soy products. Food Chem 87: 297-305
    • (2004) Food Chem , vol.87 , pp. 297-305
    • Penalvo, J.L.1    Nurmi, T.2    Adlercreutz, H.3
  • 30
    • 80052966314 scopus 로고    scopus 로고
    • Chromatographic fingerprints and quantitative analysis of isoflavones in tofu-type soybeans
    • Shen D, Wu QL, Sciarappa WJ, Simon JE (2012) Chromatographic fingerprints and quantitative analysis of isoflavones in tofu-type soybeans. Food Chem 130:1003-1009
    • (2012) Food Chem , vol.130 , pp. 1003-1009
    • Shen, D.1    Wu, Q.L.2    Sciarappa, W.J.3    Simon, J.E.4
  • 31
    • 84863639233 scopus 로고    scopus 로고
    • A new ultrahigh pressure liquid chromatography method for the determination of total isoflavone aglycones after enzymatic hydrolysis: Application to analyze isoflavone levels in soybean cultivars
    • in press
    • Fiechter G, Opacak I, Raba B, Mayer HK (2011) A new ultrahigh pressure liquid chromatography method for the determination of total isoflavone aglycones after enzymatic hydrolysis: application to analyze isoflavone levels in soybean cultivars. Food Res Inter (in press)
    • (2011) Food Res Inter
    • Fiechter, G.1    Opacak, I.2    Raba, B.3    Mayer, H.K.4
  • 32
    • 34047253206 scopus 로고    scopus 로고
    • Isolation of six isoflavones from Semen sojae praeparatum by preparative HPLC
    • Qu LP, Fan GR, Peng JY, Mi HM (2007) Isolation of six isoflavones from Semen sojae praeparatum by preparative HPLC. Fitoterapia 78:200-204
    • (2007) Fitoterapia , vol.78 , pp. 200-204
    • Qu, L.P.1    Fan, G.R.2    Peng, J.Y.3    Mi, H.M.4
  • 34
    • 20544455259 scopus 로고    scopus 로고
    • Quantitative determination and structural characterization of isoflavones in nutritional supplements by liquid chromatographymass spectrometry
    • Chen LJ, Zhao X, Plummer S, Tang J, Games DE (2005) Quantitative determination and structural characterization of isoflavones in nutritional supplements by liquid chromatographymass spectrometry. J Chromat A 1082:60-70
    • (2005) J Chromat A , vol.1082 , pp. 60-70
    • Chen, L.J.1    Zhao, X.2    Plummer, S.3    Tang, J.4    Games, D.E.5
  • 35
    • 46749116804 scopus 로고    scopus 로고
    • Quantitative determination of isoflavones in soy based nutritional supplements by high-performance liquid chromatography
    • Stürtz M, Lander V, Schmid W, Winterhalter P (2008) Quantitative determination of isoflavones in soy based nutritional supplements by high-performance liquid chromatography. JVL 3: 127-136
    • (2008) JVL , vol.3 , pp. 127-136
    • Stürtz, M.1    Lander, V.2    Schmid, W.3    Winterhalter, P.4
  • 37
    • 78751613026 scopus 로고    scopus 로고
    • Rapid HPLC method for determination of 12 isoflavone components in soybean seeds
    • Sun JM, Sun BL, Han FX, Yan SR, Yang H, Kikuchi A (2011) Rapid HPLC method for determination of 12 isoflavone components in soybean seeds. Agric Sci China 10:70-77
    • (2011) Agric Sci China , vol.10 , pp. 70-77
    • Sun, J.M.1    Sun, B.L.2    Han, F.X.3    Yan, S.R.4    Yang, H.5    Kikuchi, A.6
  • 38
    • 4744375541 scopus 로고    scopus 로고
    • Simultaneous determination of saponins and isoflavones in soybean (Glycine max L.) by reversed-phase liquid chromatography with evaporative lightscattering and ultraviolet detection
    • Ganzera M, Stuppner H (2004) Simultaneous determination of saponins and isoflavones in soybean (Glycine max L.) by reversed-phase liquid chromatography with evaporative lightscattering and ultraviolet detection. J AOAC Int 87:1189-1194
    • (2004) J AOAC Int , vol.87 , pp. 1189-1194
    • Ganzera, M.1    Stuppner, H.2
  • 39
    • 0036801437 scopus 로고    scopus 로고
    • An improved method for determination of isoflavones in soybean powder by liquid chromatography
    • Kao TH, Chen BH (2002) An improved method for determination of isoflavones in soybean powder by liquid chromatography. Chromatographia 56:423-430
    • (2002) Chromatographia , vol.56 , pp. 423-430
    • Kao, T.H.1    Chen, B.H.2
  • 40
    • 77953715122 scopus 로고    scopus 로고
    • Column switching high-performance liquid chromatography with two channels electrochemical detection for highsensitive determination of isoflavones
    • Matsumoto D, Kotani A, Hakamata H, Takahashi K, Kusu F (2010) Column switching high-performance liquid chromatography with two channels electrochemical detection for highsensitive determination of isoflavones. J Chromatogr A 1217: 2986-2989
    • (2010) J Chromatogr A , vol.1217 , pp. 2986-2989
    • Matsumoto, D.1    Kotani, A.2    Hakamata, H.3    Takahashi, K.4    Kusu, F.5
  • 41
    • 0031740985 scopus 로고    scopus 로고
    • Soy isoflavone analysis: Quality control and a new internal standard1-3
    • Song T, Barua K, Buseman G, Murphy P (1998) Soy isoflavone analysis: quality control and a new internal standard1-3. Am J Clin Nutr 68:1474-1479
    • (1998) Am J Clin Nutr , vol.68 , pp. 1474-1479
    • Song, T.1    Barua, K.2    Buseman, G.3    Murphy, P.4
  • 42
    • 0035853633 scopus 로고    scopus 로고
    • Improved methods for the extraction and analysis of isoflavones from soy-containing foods and nutritional supplements by reversed-phase high-performance liquid chromatography and liquid chromatography-mass spectrometry
    • Griffith AP, Collison MW (2001) Improved methods for the extraction and analysis of isoflavones from soy-containing foods and nutritional supplements by reversed-phase high-performance liquid chromatography and liquid chromatography-mass spectrometry. J Chromatogr A 913:397-413
    • (2001) J Chromatogr A , vol.913 , pp. 397-413
    • Griffith, A.P.1    Collison, M.W.2
  • 43
    • 34347403660 scopus 로고    scopus 로고
    • Comparison of extraction solvents and techniques used for the assay of isoflavones from soybean
    • Luthria DL, Biswas R, Natarajan S (2007) Comparison of extraction solvents and techniques used for the assay of isoflavones from soybean. Food Chem 105:325-333
    • (2007) Food Chem , vol.105 , pp. 325-333
    • Luthria, D.L.1    Biswas, R.2    Natarajan, S.3
  • 44
    • 34948815496 scopus 로고    scopus 로고
    • Solvent effects on extraction and HPLC analysis of soybean isoflavones and variations, of Isoflavone compositions as affected by crop season
    • Tsai HS, Huang LJ, Lai YH, Chang JC, Lee RS, Chiou RYY (2007) Solvent effects on extraction and HPLC analysis of soybean isoflavones and variations, of Isoflavone compositions as affected by crop season. J Agric Food Chem 55:7712-7715
    • (2007) J Agric Food Chem , vol.55 , pp. 7712-7715
    • Tsai, H.S.1    Huang, L.J.2    Lai, Y.H.3    Chang, J.C.4    Lee, R.S.5    Ryy, C.6
  • 46
    • 33845738697 scopus 로고    scopus 로고
    • Fast analysis of soy isoflavones by high-performance liquid chromatography with monolithic columns
    • Rostagno MA, Palma M, Barroso CG (2007) Fast analysis of soy isoflavones by high-performance liquid chromatography with monolithic columns. Anal Chim Acta 582:243-249
    • (2007) Anal Chim Acta , vol.582 , pp. 243-249
    • Rostagno, M.A.1    Palma, M.2    Barroso, C.G.3
  • 47
    • 84863154701 scopus 로고    scopus 로고
    • Preparative separation of isoflavones from Korean soybean by HPLC
    • Lee KJ, Row KH, Jun I (2008) Preparative separation of isoflavones from Korean soybean by HPLC. Asian J Sci Res 1: 288-292
    • (2008) Asian J Sci Res , vol.1 , pp. 288-292
    • Lee, K.J.1    Row, K.H.2    Jun, I.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.