Quechers methodologies as an alternative to solid phase extraction (SPE) for the determination and characterization of residues of cephalosporins in beef muscle using LC-MS/MS

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 899, Issue , 2012, Pages 57-65

  Perez Burgos R ^a   Grzelak, E M ^b   Gokce, G ^c   Saurina, J ^a   Barbosa, J ^a   Barron D ^a  

^a UNIVERSITY OF BARCELONA   (Spain)

^b MARIA CURIE SK ODOWSKA UNIVERSITY   (Poland)

^c CUMHURIYET UNIVERSITY   (Turkey)

Author keywords

Beef tissues; Cephalosporins; Experimental design; LC MS MS; QuEChERS; SPE; Validation according 2002 657 EC

Indexed keywords

2002/657/EC; CEPHALOSPORINS; LC-MS/MS; QUECHERS; SPE;

DESIGN OF EXPERIMENTS; MUSCLE; RECOVERY; STATISTICS;

ANTIBIOTICS;

CEFALEXIN; CEFALONIUM; CEFAPIRIN; CEFAZOLIN; CEFOPERAZONE; CEFQUINOME; CEFTIOFUR; CEPHALOSPORIN; UNCLASSIFIED DRUG;

ACCURACY; ANALYTICAL PARAMETERS; ARTICLE; BEEF; DISPERSIVE SOLID PHASE EXTRACTION; DRUG DETERMINATION; DRUG MUSCLE LEVEL; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIQUID CHROMATOGRAPHY; MAXIMUM RESIDUE LIMIT; PRIORITY JOURNAL; PROCESS OPTIMIZATION; QUECHERS METHODOLOGY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS;

ANIMALS; ANTI-BACTERIAL AGENTS; CATTLE; CEPHALOSPORINS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DRUG RESIDUES; MEAT; MUSCLES; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

EID: 84862147303     PISSN: 15700232     EISSN: 1873376X     Source Type: Journal    
DOI: 10.1016/j.jchromb.2012.05.002     Document Type: Article

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