Development and validation of a pre-column reversed phase liquid chromatographic method with fluorescence detection for the determination of primary phenethylamines in dietary supplements and phytoextracts

Journal of Chromatography A

Volumn 1218, Issue 28, 2011, Pages 4468-4473

  Gatti, Rita ^a   Lotti, Cinzia ^a  

^a UNIVERSITY OF BOLOGNA   (Italy)

Author keywords

Dietary supplements; Fluorescence detection; Method validation; O Phthaldialdehyde; Phenethylamines; Pre column derivatization; Reversed phase liquid chromatography

Indexed keywords

DIETARY SUPPLEMENTS; FLUORESCENCE DETECTION; METHOD VALIDATIONS; O-PHTHALDIALDEHYDE; PHENETHYLAMINES; PRECOLUMN DERIVATIZATIONS; REVERSED-PHASE LIQUID CHROMATOGRAPHY;

ACETONITRILE; AMINO ACIDS; CHROMATOGRAPHIC ANALYSIS; COLUMN CHROMATOGRAPHY; FLUORESCENCE; FOOD ADDITIVES; HIGH PRESSURE LIQUID CHROMATOGRAPHY; METHANOL; NUTRITION; SODIUM; VITAMINS;

LIQUIDS;

ACETIC ACID; ACETONITRILE; HORDENINE; METHANOL; N METHYLTYRAMINE; OCTOPAMINE; OXEDRINE; PHENETHYLAMINE; PHTHALALDEHYDE; SODIUM 1 HEPTANE SULFONIC ACID; SOUR ORANGE EXTRACT; SULFONIC ACID DERIVATIVE; TYRAMINE; TYROSINE; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CHEMICAL COMPOSITION; CONTROLLED STUDY; DERIVATIZATION; DIET SUPPLEMENTATION; DRUG ISOLATION; ELUTION; FLUORESCENCE ANALYSIS; FLUOROMETRY; INTERMETHOD COMPARISON; LIMIT OF DETECTION; LIMIT OF QUANTITATION; PH; PRIORITY JOURNAL; REPRODUCIBILITY; REVERSED PHASE LIQUID CHROMATOGRAPHY; ROOM TEMPERATURE; SENSITIVITY ANALYSIS; SOUR ORANGE;

ACETONITRILES; CHROMATOGRAPHY, REVERSE-PHASE; CITRUS; DIETARY SUPPLEMENTS; HYDROGEN-ION CONCENTRATION; O-PHTHALALDEHYDE; PHENETHYLAMINES; PLANT EXTRACTS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPECTROMETRY, FLUORESCENCE;

CITRUS AURANTIUM;

EID: 79959380630     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.05.044     Document Type: Article

References (37)

1. Tang W., Eisenbrand G. Chinese Materia Medica 1998, CRC Press LLC, Boca Raton, FL.
2. Carpéné C., Galitzky J., Fontana E., Atgie C., Lafontan M., Berlan M. Naunyn-Schmiedebergs Arch. Pharm 1999, 359:310.
3. Airriess C.N., Rudling J.E., Midgley J.M., Evans P.D. Brit. J. Pharm. 1997, 122:191.
4. Fugh-Berman A., Myers A. Exp. Biol. Med. 2004, 229:698.
5. Putzbach K., Rimmer C.A., Sharpless K.E., Sander L.C. J. Chromatogr. A 2007, 1156:304.
6. Dallas C., Gerbi A., Tenca G., Juchaux F. Phytomed 2008, 15:783.
7. Ganzera M., Lanser C., Stuppner H. Talanta 2005, 66:889.
8. Blumenthal M. WholeFoods. Part 1 2004, ®American Botanical Council.
9. Blumenthal M. WholeFoods. Part 2 2005, ®American Botanical Council.
10. The World Anti-Doping Code; The 2006 Prohibited List International Standard. http://www.wadaama.org/en/WorldAntiDopingProgram/SportsandAntiDopingOrga nizations/Intenational-Standards/Prohibited-List/.
11. Pellati F., Benvenuti S. J. Chromatogr. A 2007, 1161:71.
12. Vieira S.M., Theodoro K.H., Gloria M.B.A. Food Chem. 2007, 100:895.
13. Roman M.C., Betz J.M., Hildreth J. J. AOAC Int. 2007, 90:68.
14. Hashimoto K., Yasuda T., Ohsawa K. J. Chromatogr. 1992, 623:386.
15. Pellati F., Benvenuti S., Melegari M., Firenzuoli F. Phytochem. Anal. 2002, 29:1113.
16. Pellati F., Benvenuti S. J. Chromatogr. A 2007, 1165:58.
17. Avula B., Upparapalli S.K., Navarrete A., Khan I.A. J. AOAC Int. 2005, 88:1593.
18. Tang F., Tao L., Luo X., Ding L., Guo M., Nie L., Yao S. J. Chromatogr. A 2006, 1125:182.
19. Niemann R.A., Gay M.L. J. Agric. Food Chem. 2003, 51:5630.
20. Percy D.W., Adcock J.L., Conlan X.A., Barnett N.W., Gange M.E., Noonan L.K., Henderson L.C., Francis P.S. Talanta 2010, 80:2191.
21. Vidal-Carou M.C., Lahoz-Portolés F., Bover-Cid S., Mariné-Font A. J. Chromatogr. A 2003, 998:235.
22. Önal A. Food Chem. 2007, 103:1475.
23. Seiler in: N., Blau K., Halket J.M. Handbook of Derivatives for Chromatography 1993, John Wiley & Sons, New York, (Chapter IX).
24. Lunn G., Hellwig L.C. Handbook of Derivatization Reactions for HPLC 1998, John Wiley and Sons, New York, N.Y, pp. 253.
25. Mao H.-M., Chen B.-G., Qian X.-M., Liu Z. Microchem. J. 2009, 91:176.
26. Ruan G.H., Zheng L.X., Wu Q.E., Zhou Z.J. J. Hyg. Res. 2006, 35:146.
27. Gatti R., Gioia M.G., Andreatta P., Pentassuglia G. J. Pharm. Biomed. Anal. 2004, 35:339.
28. Pereira V., Pontes M., Câmara J.S., Marques J.C. J. Chromatogr. A 2008, 1189:435.
29. Antoine F.R., Wei C.I., Littell R.C., Marshall M.R. J. Agric. Food Chem. 1999, 47:5100.
30. Mell L.D., Carpenter D.O. Neurochem. Res. 1980, 5:1089.
31. Gatti R., Andreatta P., Gioia M.G., Boschetti S. J. Liq. Chrom. Related Technol. 2010, 33:1760.
32. Qureshi G.A., Fohlin L., Bergström J. J. Chromatogr. 1984, 297:91-100.
33. United States Pharmacopeia XXVIII The National Formulary XXIII 2005, Pharmacopeial Convention, Inc., Rockville, MD, p. 2855.
34. Farmacopea Ufficiale della Repubblica Italiana XII, Roma, Italy 2008, p. 660.
35. Okamura N., Miki H., Harada T., Yamshita S., Masaoka Y., Nakamoto Y., Tsuguma M., Yoshitomi H., Yagi A. J. Pharm. Biomed. Anal. 1999, 20:363.
36. International Conference on Harmonization of Technical Requirements for the Registration of Pharmaceuticals for Human Use (ICH), Guideline Q2(R1)-Validation of Analytical Procedures: Text and Methodology 2005.
37. Van Loco J., Elskens M., Croux C., Beernaert H. Accred. Qual. Assur. 2002, 7:281.