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iPrOH, 0.1 mmol) under nitrogen. The resulting brown solution was stirred at room temperature for 10 min. The mixture was then heated at 80 °C. The mixture turned pale yellowish after the reaction was complete. The yields were determined by GC analysis with n-undecane as internal standard, and the identities of the hydrogenation products were confirmed by comparison to authentic samples.
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79958814168
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2 = 0.0435 [I > 2σ(I)]. Structural data for was collected on a Bruker Smart Apex CCD with graphite-monochromated Mo-Kα radiation (λ = 0.71073 Å) at 153 K. The structure was solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 programs.
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