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The X-ray crystal structure of complex 1 was determined; see:
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The X-ray crystal structure of complex 1 was determined; see: Feller, M.; Ben-Ari, E.; Tarkeshwar, G.; Shimon, L. J.W.; Leitus, G.; Diskin-Posner, Y.; Weiner, L.; Milstein, D. Inorg. Chem. 2007, 46, 10479
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79956155944
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3a has been prepared previously by reaction of (PNP)Rh(OTf) with diphenylzinc, as described in ref 10
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3a has been prepared previously by reaction of (PNP)Rh(OTf) with diphenylzinc, as described in ref 10.
-
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43
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2 at -35 °C under dry argon resulted in the formation of a mixture of products.
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46
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0001346445
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I fragment, probably as a result of steric hindrance; see
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For preparation and characterization of complex 9 see ref 11b.
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79956118570
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Complex 1 was also formed in the reaction as a byproduct, apparently as a result of reprotonation of 2 with adventitious water
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Complex 1 was also formed in the reaction as a byproduct, apparently as a result of reprotonation of 2 with adventitious water.
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