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85034476104
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note
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1H NMR.
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19
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85034462554
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note
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tert-Butylethane (tba) was identified and quantified by GC analyses performed on a temperature-programmed (45°C isothermal for 1 min, 5°C/min to 75°C) Hewlett-Packard 5890 gas Chromatograph using a 250 μm × 25 m OV-1 capillary column.
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20
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85034476506
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note
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2H NMR (60.4 MHz) spectroscopic analysis of the reaction mixtures.
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21
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85034465600
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Ph.D. Thesis, University of Hawaii
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Belli, J. Ph.D. Thesis, University of Hawaii, 1997.
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Belli, J.1
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22
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85034476524
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note
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12) δ 70.6 (s).
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23
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15444364712
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Cooper, A. C.; Folting, K.; Huffman, J. C.; Caulton, K. C. Organometallics 1997, 16, 505.
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Caulton, K.C.4
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24
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85034459275
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note
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4: C, 48.07; H, 7.23; N, 2.33. Found: C, 47.95; H, 7.33; N, 2.40.
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-
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25
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85034474821
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note
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w) = 4.85% (11.88%), GOF = 1.073. The finding of the unusual cyclohexane solvate in the crystals was unexpected and noteworthy.
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28
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0001104050
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Yoshida, T.; Okano, T.; Thorn, D. L.; Tulip, T. H.; Otsuka, S.; Ibers, J. A. J. Organomet. Chem. 1979, 181, 183.
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Yoshida, T.1
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Ibers, J.A.6
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29
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33947092184
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Chart, J.; Dilworth, J. R.; Richards, R. L. Chem. Rev. 1978, 78, 589.
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