Synthesis, structures and luminescent properties of Ca(II), Sr(II) and Pb(II) coordination compounds based on new flexible ligand 5-(2-pyrazinyl) tetrazole-2-acetic acid

Inorganic Chemistry Communications

Volumn 14, Issue 6, 2011, Pages 843-847

  Li, Qiao Yun ^a   Zhou, Feng ^a   Zhai, Chun ^a   Shen, Lei ^a   Tang, Xiao Yan ^a   Yang, Jie ^a   Yang, Gao Wen ^a   Miao, Zhu Feng ^a   Jin, Jian Ning ^a   Shen, Wei ^a  

^a CHANGSHU INSTITUTE OF TECHNOLOGY   (China)

Author keywords

5 (2 pyrazinyl)tetrazole 2 acetic acid; Ca(II); Crystal structure; Luminescence; Pb(II); Sr(II)

Indexed keywords

EID: 79955835557     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2011.03.004     Document Type: Article

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59. 2: C, 40.78; H, 2.93; N, 40.76%. Found: C, 40.49; H, 2.75; N, 40.61%. IR (KBr, cm-1): 3426 (s), 1730 (s), 1449 (s), 1420 (s), 1347 (s) 1257 (s), 1209 (m), 1146 (m), 1064 (m), 1018 (m), 905 (m), 868 (s), 830 (m), 666 (m).
60. -1): 3424 (s), 1631 (s), 1596 (s), 1580 (s), 1424 (m), 1394 (s), 1318 (w), 1296 (w), 1174 (w), 1155 (w), 1045 (w), 821 (w), 710 (w), 679 (w).
61. 5Pb, Mr=635.56, colorless crystal, triclinic, space group Pī, a=7.2085(14) Å, b=8.3093 (17) Å, c=16.711 (3) Å, α=99.92(3) ° β=98.13(3) ° γ =97.58(3) ° V=963.5(3) Å3, Z=2, T=293(2) K, Dcalcd. = 9.191 g.cm-3, μ=8.815mm-1, R (wR)=0.0610 (0.1347) and GOF=0.885 for 3386 reflectionswith I>2.00r(I). The crystal structures of 1-3 were solved by directmethods using SHELXS-97 programand refined onF2 by full-matrix leastsquares using SHELXL-97 program. All non-H atoms were refined anisotropically while all H atoms were placed in geometrically idealized positions.
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