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52949110673
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The ligand 5-aminotetrazole-1-acetic acid (Hatza) was prepared from chloroacetic acid and 5-aminotetrazole in methanolic potassium hydroxide according to a reported procedure [17a].
-
The ligand 5-aminotetrazole-1-acetic acid (Hatza) was prepared from chloroacetic acid and 5-aminotetrazole in methanolic potassium hydroxide according to a reported procedure [17a].
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41
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52949121524
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-1): 3419 (s), 1645 (s), 1616 (s), 1498 (m) 1383 (s), 1290 (m), 1151 (m), 1083 (m), 1028 (m), 825 (s), 613 (m)
-
-1): 3419 (s), 1645 (s), 1616 (s), 1498 (m) 1383 (s), 1290 (m), 1151 (m), 1083 (m), 1028 (m), 825 (s), 613 (m)
-
-
-
-
42
-
-
52949126829
-
-
-1): 3406 (m), 1642 (s), 1618 (s), 1569 (m), 1452 (s), 1384 (m), 1369 (m), 1263 (m), 1166 (m), 1134 (m), 1060 (m), 1024 (m), 802 (s), 761(s), 719 (m), 601(s).
-
-1): 3406 (m), 1642 (s), 1618 (s), 1569 (m), 1452 (s), 1384 (m), 1369 (m), 1263 (m), 1166 (m), 1134 (m), 1060 (m), 1024 (m), 802 (s), 761(s), 719 (m), 601(s).
-
-
-
-
43
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52949115405
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-
note
-
2 by full-matrix leastsquares using SHELXL-97 program. All non-H atoms were refined anisotropically while all H atoms were placed in geometrically idealized positions.
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