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2442531435
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note
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(a) A typical synthesis of these materials is exemplified by that of IRMOF-18: 2,3,5,6-tetramethylbenzene-1,4-dicarboxylic acid (1.2 g, Chem Service) and zinc nitrate hexahydrate (12 g, Aldrich) dissolved in N,N-diethylformamide (600 mL. BASF) and heated for 48 h at 70 °C. Details are provided in the Supporting Information.
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2442531434
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note
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(b) A Cahn C-1000 microgravimetric balance was operated within a gas manifold system in contact with a liquid nitrogen bath (vacuum level < 10-3 Torr) to measure the nitrogen and hydrogen isotherms from 0 to 1 atm. Volumetric measurements were performed using a Micromeritics Co. sorption apparatus (model 2010). Experimental details are described in ref 2a and the Supporting Information.
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14
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2442619936
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note
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An exception occurs for IRMOF-18, where the sterics of the TMBDC methyl groups orient the phenylene planes perpendicular to the carboxylate planes, exposing alternate faces of the Zn40 clusters.
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