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77956939396
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note
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- 1): 3122 (m), 2975 (w), 1511 (s), 1487 (s), 1385 (m), 1325 (s), 1276 (s), 1244 (s), 1224 (s), 1145 (s), 1090 (m), 1050 (m), 986 (m), 957 (m), 869 (m), 805 (s), 672 (s).
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20
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77956936543
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note
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-1 region.
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77956929448
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note
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- 3. 7060 reflections collected, 1646 unique (R(int) = 0.0230) which were used in all calculations. R1 = 0.0568 (I > 2r(I)), wR2 = 0.1526 (all data). Data were collected on a Bruker ApexII CCD diffractometer with graphitemonochromated Mo-Kα radiation (λ = 0.71073 Å). The structures were solved with direct methods and refined with full-matrix least squares (SHELX-97)
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