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Volumn 13, Issue 11, 2010, Pages 1259-1262

A 3D pillared-layer porous framework with rare magnetic corner-sharing a-chain and unprecedented pentadentate 5-(4-pyridyl)tetrazolate ligand

Author keywords

Chain; Cobalt(II); Pillared layer framework; Pyridyl tetrazolate; Spin frustration

Indexed keywords


EID: 77956913110     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.07.010     Document Type: Article
Times cited : (25)

References (52)
  • 21
    • 77956911368 scopus 로고    scopus 로고
    • note
    • - 1): 3319(br), 1622(vs), 1566(vs), 1530(vs), 1452(vs), 1422(vs), 1354(vs), 1220(w), 1199(w), 1083(w), 1019(m), 923(w), 841(s), 780(s), 737(s), 726(s), 706(s), 568(m), 538(w).
  • 28
    • 77956918485 scopus 로고    scopus 로고
    • note
    • max = 0.8970/0.7685). X-ray data collection was carried out using a Bruker APEX II diffractometer with a CCD area detector. There was no evidence of crystal decay during data collection. Semiempirical multi-scan absorption corrections were applied (SADABS), and the program SAINT was used for integration of the diffraction profiles. The structure was solved by direct methods and refined with the full-matrix least-squares technique using the SHELXS-97 and SHELXL-97 progranms. All nonhydrogen atoms were treated anisotropically. C-bound H atoms of the ligands were placed geometrically refined as riding atoms. The staring position of H attached to oxygen atom were located in differences Fourier synthesis and then fixed geometrically as riding atoms. CCDC-764132 contains the supplementary crystallographic data for this paper.
  • 29
    • 12344290845 scopus 로고    scopus 로고
    • Bruker AXS Madison, WI
    • G.M. Sheldrick SAINT 1998 Bruker AXS Madison, WI
    • (1998) SAINT
    • Sheldrick, G.M.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.