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Inorganic Chemistry Communications

Volumn 13, Issue 8, 2010, Pages 976-980

Four coordination polymers derived from 4-amino-3,5-bis(3-pyridyl)-1,2,4-triazole and copper sulfate

(5) Liu, Kui a Zhu, Xia a Wang, Ju a Li, Baolong a Zhang, Yong a

a SOOCHOW UNIVERSITY (China)

Author keywords

4 amino 3,5 bis(3 pyridyl) 1,2,4 triazole; Coordination polymer; Copper sulfate complex; Solvent controlled assembly

Indexed keywords

EID: 77953871256 PISSN: 13877003 EISSN: None Source Type: Journal
DOI: 10.1016/j.inoche.2010.05.011 Document Type: Article

Times cited : (12)

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- Synthesis of 1: A 5 mL aqueous solution of CuSO4·5H2O (0.025 g, 0.1 mmol) was added to an aqueous solution (5 mL) of 3-bpt (0.024 g, 0.1 mmol) with stirring. The light blue single crystals 1 were obtained after the mixture was allowed to stand at room temperature for two weeks in 78% yield (0.038 g, Anal. Calc. for C12H20CuN6O9S: C, 29.54; H, 4.13; N, 17.23. Found: C, 29.47; H, 4.16; N, 17.15, Synthesis of 2: A 5 mL aqueous solution of CuSO4·5H2O (0.025 g, 0.1 mmol) was added to a 7 mL mixture solution (2 mL EtOH and 5 mL H2O) of 3-bpt (0.024 g, 0.1 mmol) with stirring. The light blue single crystals 2 were obtained after the mixture was allowed to stand at room temperature for two weeks in 64% yield 0.034 g, Anal. Calc. for C24H48Cu2N12O22S2: C, 27.51; H, 4.62; N, 16.04. Found: C, 27.39; H, 4.58; N, 15.96, Synthesi
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- X-ray single crystal difraction data collection for 1-4 were performed on a Rigaku Mercury CCD diffractometer. The structures were solved by direct methods and refined with full-matrix least-squares technique (SHELXTL-97, 38, Crystal data for C12H20CuN6O9S (1, Mr, 487.94, monoclinic, P21/c, a, 10.408(4, b, 17.120(6, c, 11.582(4) Å, β, 114.531(4)o, V, 1877.4(12) Å3, Z, 4, Dc, 1.726 g/cm3, μ, 1.336 mm- 1, F(000, 1004, S, 0.993, R, 0.0403, wR, 0.1022. Crystal data for C24H48Cu2N12O22S2 (2, Mr, 1047.94, monoclinic, P21/c, a, 27.9184(12, b, 10.8607(2, c, 30.3935(13) Å, β, 114.969(2)o, V, 8354.4(5) Å3, Z, 8, Dc, 1.666 g/cm3, μ, 1.214 mm- 1, F000, 4336, S, 1.029, R, 0.0369, wR, 0.1039. Crystal data for C12H20CuN6O9
- - 1, F(000) = 844, S = 1.071, R = 0.0417, wR = 0.0990.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.