Characterization of self-healing glassy composites by high-temperature environmental scanning electron microscopy (HT-ESEM)

Journal of Electron Microscopy

Volumn 59, Issue 5, 2010, Pages 359-366

  Coillot, Daniel ^a,b   Podor, Renaud ^c   Méar, François O ^a   Montagne, Lionel ^a  

^a UNIV LILLE   (France)

^b UNITÉ DE CATALYSE ET DE CHIMIE DU SOLIDE   (France)

^c DIF   (France)

Author keywords

composite; environmental scanning electron microscopy (ESEM); self healing; solid oxide fuel cell (SOFC); temperature

Indexed keywords

CRACKS; GLASS; SELF-HEALING MATERIALS; SOLID OXIDE FUEL CELLS (SOFC);

ENVIRONMENTAL SCANNING; ENVIRONMENTAL SCANNING ELECTRON MICROSCOPES; ENVIRONMENTAL SCANNING ELECTRON MICROSCOPY; HEALING OF CRACKS; HIGHEST TEMPERATURE; SELF-HEALING; SELF-HEALING PROPERTIES; SOLID OXIDE FUEL CELL; SOLID-OXIDE FUEL CELL; TEMPERATURE CHAMBER;

SCANNING ELECTRON MICROSCOPY;

EID: 77957995894     PISSN: 00220744     EISSN: 14779986     Source Type: Journal    
DOI: 10.1093/jmicro/dfq018     Document Type: Article

References (60)

1. Li V C, Lim Y M, and Chan Y W (1998) Feasibility study of a passive smart self-healing cementitious composite. Compos. B Eng. 29: 819-827.
2. Dry C (1992) Passive tuneable fibers and matrices. Int. J. Mod. Phys. B 6: 2763-2771.
3. Bleay S M, Loader C B, Hawyes V J, Humberstone L, and Curtis P T (2001) A smart repair system for polymer matrix composites. Compos. Appl. Sci. Manuf. 32: 1767-1776.
4. Dry C (1997) Self-repairing reinforced matrix materials US005660624.
5. Pang J W C and Bond I P (2005) A hollow fibre reinforced polymer composite encompassing self-healing and enhanced damage visibility. Compos. Sci. Technol. 65: 1791-1799.
6. Brown E N, White S R, and Sottos N R (2004) Microcapsule induced toughening in a self-healing polymer composite. J. Mater. Sci. 39: 1703-1710.
7. Cho S H, White S R, and Braun P V (2009) Self-healing polymer coatings. Adv. Mater. 21: 645-649.
8. White S R, Sottos N R, Geubelle P H, Moore J S, Kessler M R, Sriram S R, Brown E N, and Viswanathan S (2001) Autonomic healing of polymer composites. Nature 409: 794-797.
9. Chen X, Wudl X, Mal A K, Shen H, and Nutt S R (2003) New thermally remendable highly cross-linked polymeric materials. Macromolecules 36: 1802-1807.
10. Naslain R, Guette A, Rebillat F, Pailler R, Langlais F, and Bourrat X (2004) Boron-bearing species in ceramic matrix composites for longterm aerospace applications. J. Solid State Chem. 177: 449-456.
11. Osada T, Nakao W, Takahashi K, and Ando K (2009) Kinetics of selfcrack- healing of alumina/silicon carbide composite including oxygen partial pressure effect. J. Am. Ceram. Soc. 92: 864-869.
12. Quemard L, Rebillat F, Guette A, Tawil H, and Louchet-Pouillerie C (2007) Self-healing mechanisms of a SiC fiber reinforced multilayered ceramic matrix composite in high pressure steam environments. J. Eur. Ceram. Soc. 27: 2085-2094. (Pubitemid 44848195)
13. Viricelle J P, Goursat P, and Bahloul-Hourlier D (2001) Oxidation behaviour of multi-layered ceramic-matrix (SiC)f/C/(SiBC)m. Compos. Sci. Technol. 61: 607-614.
14. Yang Z H, Jia D C, Zhou Z, Shi P Y, Song C B, and Lin L (2008) Oxidation resistance of hot-pressed SiC-BN composites. Ceram. Int. 34: 317-321.
15. 2-SiC ceramic composite. J. Am. Ceram. Soc. 91: 4068-4073.
16. Kessler M R, Sottos N R, and White S R (2003) Self-healing structural composite materials. Compos. Appl. Sci. Manuf. 34: 743-753.
17. Govindaraju N, Liu W N, Sun X, Singh P, and Singh R N (2009) A modeling study on the thermomechanical behavior of glass-ceramic and self-healing glass seals at elevated temperatures. J. Power Sources 190: 476-484.
18. Liu W, Sun X, and Khaleel M A (2008) Predicting Young's modulus of glass/ceramic sealant for solid oxide fuel cell considering the combined effects of aging, micro-voids and self-healing. J. Power Sources 185: 1193-1200.
19. Singh N R (2007) Sealing technology for solid oxide fuel cells (SOFC). Int. J. Appl. Ceram. Tech. 4: 134-144.
20. Moreira Jorge Jr A, Inoue A, and Yavari A R (2008) Surface self-healing of metallic glasses in the super-cooled liquid region δT = Tx - Tg. Rev. Adv. Mater. Sci. 18: 193-196.
21. Deng X, Duquette J, and Petric A (2007) Silver-glass composite for high temperature sealing. Int. J. Appl. Ceram. Tech. 4: 145-151.
22. Coillot D, Méar F O and Montagne L (2009) Composition vitreuse autocicatrisante, procédé de préparation et utilisations. Patent submitted.
23. Coillot D, Méar F O, Podor R, and Montagne L (2010) Autonomic self-repairing glassy materials. Adv. Funct. Mater. Submitted.
24. Knowles R W and Hardt T A (1997) High temperature specimen stage and detector for an environmental scanning electron microscope. Patent no. WO 97/07526.
25. Schmid B, Aas N, Grong Ø, and ØDegard R (2001) High-temperature oxidation of nickel and chromium studied with an in-situ environmental scanning electron microscope. Scanning 23: 255-266.
26. Schmid B, Aas N, Grong Ø, and ØDegard R (2001) In situ environmental scanning electron microscope observations of catalytic processes encountered in metal dusting corrosion on iron and nickel. Appl. Catal. A Gen. 215: 257-270.
27. Schmid B, Aas N, Grong Ø, and ØDegard R (2002) High-temperature oxidation of iron and the decay of Wüstite studied with in situ ESEM. Oxid. Met. 57: 115-130.
28. Oquab D and Monceau D (2001) In-situ SEM study of cavity growth during high temperature oxidation of β-(Ni, Pd)Al. Scr. Mater. 44: 2741-2746.
29. Srinivasan N S (2002) Dynamic study of changes in structure and morphology during the heating and sintering of iron powder. Powder Technol. 124: 40-44.
30. Maroni V A, Teplitsky M, and Rupich M W (1999) An environmental scanning electron microscope study of the Ag/Bi-2223 composite conductor from 25 to 840°C. Phys. C Supercond. 313: 169-174.
31. 3 powder bed. J. Electron Microsc. 53: 393-396.
32. 2S attack on the protective oxide on an Ni-Fe alloy. Scanning 18: 497-499.
33. Gregori G, Kleebe H J, Siegelin F, and Ziegler G (2002) In situ SEM imaging at temperatures as high as 1450°C. J. Electron Microsc. 51: 347-352.
34. Abolhassani S, Dadras M, Leboeuf M, and Gavillet D (2003) In situ study of the oxidation of Zircaloy-4 by ESEM. J. Nucl. Mater. 321: 70-77.
35. Reichmann A, Poelt P, Brandl C, Chernev B, and Wilhelm P (2008) High-temperature corrosion of steel in an ESEM with subsequent scale characterisation by Raman microscopy. Oxid. Met. 70: 257-266.
36. 2O on iron oxidation at 500°C. Corros. Sci. 51: 1914-1924.
37. Marzagui H and Cutard T (2004) Characterisation of microstructural evolutions in refractory castables by in situ high temperature ESEM. J. Mater. Process. Tech. 155-156: 1474-1481.
38. Smith A J, Atkinson H V, Hainsworth S V, and Cocks A C F (2006) Use of a micromanipulator at high temperature in an environmental scanning electron microscope to apply force during the sintering of copper particles. Scr. Mater. 55: 707-710.
39. Sample D R, Brown P W, and Dougherty J P (1996) Microstructural evolution of copper thick films observed by environmental scanning electron microscopy. J. Am. Ceram Soc. 79: 1303-1306.
40. Subramaniam S (2006) In Situ High Temperature Environmental Scanning Electron Microscopic Investigations of Sintering Behavior in Barium Titanate. PhD thesis, University of Cincinnati, Engineering: Materials Science, 194 p.
41. Bondioli F, Bonamartini Corradi A, Ferrari A M, and Manfredini T (2000) Environmental scanning electron microscopy (ESEM) investigation of the reaction mechanism in praseodymium-doped zircon. J. Am. Ceram. Soc. 83: 1518-1520.
42. Blanford C F, Carter C B, and Stein A (2008) In situ high-temperature electron microscopy of 3DOM cobalt, iron oxide, and nickel. J. Mater. Sci. 43: 3539-3552.
43. Imaizumi K, Matsuda N, and Otsuka M (2003) Coagulation/phase separation process in the silica/inorganic salt systems (1) observation of state transformation. J. Mater. Sci. 38: 2979-2986.
44. Jacobsson L, Persson C, and Melin S (2008) In-situ ESEM study of thermo-mechanical fatigue crack propagation. Mater. Sci. Eng. A 496: 200-208.
45. Celik E and Hascicek Y S (2002) In situ hot-stage ESEM evaluation of CeO2 buffer layers on Ni tapes for YBCO coated conductors. Mater. Sci. Eng. A 94: 176-180.
46. Biallas G and Maier H J (2007) In-situ fatigue in an environmental scanning electron microscope-potential and current limitations. Int. J. Fatigue 29: 1413-1425.
47. Hillers M, Matzen G, Veron E, Dutreilh-Colas M, and Douy A (2007) Application of in situ high-temperature techniques to investigate the effect of B2O3 on the crystallization behavior of aluminosilicate Eglass. J. Am. Ceram. Soc. 90: 720-726.
48. Gualtieri A F, Lassinantti Gualtieri M, and Tonelli M (2008) In situ ESEM study of the thermal decomposition of chrysotile asbestos in view of safe recycling of the transformation product. J. Hazard. Mater. 156: 260-266.
49. 4 by in situ heating in an ESEM. Int. J. Hydrogen Energy 34: 9151-9156.
50. 2-2LiH monitored by environmental scanning microscopy. Int. J. Hydrogen Energy 34: 376-379.
51. Atkinson H V, Hainsworth S V, Stevenson T, Samara-Ratna P, Sykes J, Smith A J. GR/S97910/01 Final Report Feasibility Study: High Temperature Micro-Manipulation System for ESEM.
52. Samara-Ratna P, Atkinson H V, Stevenson T, Hainsworth S V, and Sykes J (2007) Design of a micromanipulation system for high temperature operation in an environmental scanning electron microscope (ESEM). J. Micromechanics Microengineering 17: 104-114.
53. Subramaniam S and Roseman R D (2005) Control and optimization of parameters in the ESEM at high temperatures. Microsc. Microanal. 11: 1514-1515.
54. Wang L, Ji Y, Wei B, Zhang Y, FuJ Xu X, and Han X (2009) Charge compensation by in-situ heating for insulating ceramics in scanning electron microscope. Ultramicroscopy 109: 1326-1332.
55. Klemenso T, Appel C C, and Mogensen M (2006) In situ observations of microstructural changes in SOFC anodes during redox cycling. Electrochem. Solid-State Lett. 9: 403-407.
56. Nakagawa Y, Yashiro K, Sato K, Kawada T, and Mizusaki J (2007) Microstructural changes of Ni/YSZ cermet under repeated redox reaction in environmental scanning electron microscope (ESEM). Solid oxide fuel cells 10 (SOFC-X), parts 1 & 2 book series. ECS Transactions 7: 1373-1380.
57. Wilson B A and Case E D (1999) Effect of humidity on crack healing in glass from in-situ investigations using an ESEM. J. Mater. Sci. 34: 247-250.
58. Air solubility in water. http://www.engineeringtoolbox.com/airsolubility- water-d-639.html.
59. Khedim H, Podor R, Rapin C, and Vilasi M (2008) Redox-control solubility of chromium in soda-silicate melts. J. Am. Ceram. Soc. 91: 3571-3579.
60. Weast R C and Astle M J (1981-1982) CRC Handbook of Chemistry and Physics (Boca Raton, FL, CRC Press, Inc.).