메뉴 건너뛰기




Volumn 2, Issue 6, 2010, Pages 915-921

Evolution of solid-state NMR in pharmaceutical analysis

Author keywords

[No Author keywords available]

Indexed keywords

CARBON 13; CRYSTALLIN;

EID: 77953644733     PISSN: 17568919     EISSN: None     Source Type: Journal    
DOI: 10.4155/fmc.10.200     Document Type: Note
Times cited : (56)

References (60)
  • 1
    • 77953146976 scopus 로고    scopus 로고
    • Significance of drug substance physiochemical properties in regulatory quality by design
    • (Preformulation in Solid Dosage Form Development). Informa Healthcare, NY, USA
    • Lee SL, Raw AS, Yu L. Significance of drug substance physiochemical properties in regulatory quality by design. In: Drugs and the Pharmaceutical Sciences 178 (Preformulation in Solid Dosage Form Development). Informa Healthcare, NY, USA, 571-583 (2008).
    • (2008) Drugs and the Pharmaceutical Sciences , vol.178 , pp. 571-583
    • Lee, S.L.1    Raw, A.S.2    Yu, L.3
  • 2
    • 43349088601 scopus 로고    scopus 로고
    • Pharmaceutical quality by design: Product and process development, understanding and control
    • Yu L. Pharmaceutical quality by design: product and process development, understanding and control. Pharm. Res. 25(4), 781-791 (2008).
    • (2008) Pharm. Res. , vol.25 , Issue.4 , pp. 781-791
    • Yu, L.1
  • 5
    • 33644613761 scopus 로고    scopus 로고
    • NMR studies of organic polymorphs and solvates
    • Harris RK. NMR studies of organic polymorphs and solvates. Analyst 131(3), 351-373 (2006).
    • (2006) Analyst , vol.131 , Issue.3 , pp. 351-373
    • Harris, R.K.1
  • 9
    • 34548383799 scopus 로고    scopus 로고
    • Solid state effects on NMR chemical shifts
    • Orendt AM, Facelli JC. Solid state effects on NMR chemical shifts. Ann. Rep. NMR Spectr. 62, 115-178 (2007).
    • (2007) Ann. Rep. NMR Spectr. , vol.62 , pp. 115-178
    • Orendt, A.M.1    Facelli, J.C.2
  • 10
    • 84994944706 scopus 로고
    • Carbon-13 NMR investigations of three fluorinated steroids
    • Carss SA, Harris RK, Fletton RA. Carbon-13 NMR investigations of three fluorinated steroids. Magn. Reson. Chem. 33(7), 501-505 (1995).
    • (1995) Magn. Reson. Chem. , vol.33 , Issue.7 , pp. 501-505
    • Carss, S.A.1    Harris, R.K.2    Fletton, R.A.3
  • 11
    • 0344583871 scopus 로고    scopus 로고
    • Anhydrates and hydrates of olanzapine: Crystallization, solid-state characterization, and structural relationships
    • Reutzel-Edens SM, Bush JK, Magee PA, Stephenson GA, Byrn SR. Anhydrates and hydrates of olanzapine: crystallization, solid-state characterization, and structural relationships. Cryst. Growth Des. 3(6), 897-907 (2003).
    • (2003) Cryst. Growth Des. , vol.3 , Issue.6 , pp. 897-907
    • Reutzel-Edens, S.M.1    Bush, J.K.2    Magee, P.A.3    Stephenson, G.A.4    Byrn, S.R.5
  • 13
    • 0033780730 scopus 로고    scopus 로고
    • A spectroscopic and crystallographic study of polymorphism in an aza-steroid
    • Wenslow RM, Baum MW, Ball RG, McCauley JA, Varsolona RJ. A spectroscopic and crystallographic study of polymorphism in an aza-steroid. J. Pharm. Sci. 89(10), 1271-1285 (2000).
    • (2000) J. Pharm. Sci. , vol.89 , Issue.10 , pp. 1271-1285
    • Wenslow, R.M.1    Baum, M.W.2    Ball, R.G.3    McCauley, J.A.4    Varsolona, R.J.5
  • 15
    • 3042560483 scopus 로고    scopus 로고
    • Effects of polymorphic differences for sulfanilamide, as seen through 13C and 15N solid-state NMR, together with shielding calculations
    • Portieri A, Harris RK, Fletton RA, Lancaster RW, Threlfall TL. Effects of polymorphic differences for sulfanilamide, as seen through 13C and 15N solid-state NMR, together with shielding calculations. Magn. Reson. Chem. 42(3), 313-320 (2004).
    • (2004) Magn. Reson. Chem. , vol.42 , Issue.3 , pp. 313-320
    • Portieri, A.1    Harris, R.K.2    Fletton, R.A.3    Lancaster, R.W.4    Threlfall, T.L.5
  • 16
    • 20144387515 scopus 로고    scopus 로고
    • Structural analysis of polymorphism and solvation in tranilast
    • Vogt FG, Cohen DE, Bowman JD et al. Structural analysis of polymorphism and solvation in tranilast. J. Pharm. Sci. 94(3), 651-665 (2005).
    • (2005) J. Pharm. Sci. , vol.94 , Issue.3 , pp. 651-665
    • Vogt, F.G.1    De, C.2    Bowman, J.D.3
  • 17
    • 18744374968 scopus 로고    scopus 로고
    • Mechanochromism of piroxicam accompanied by intermolecular proton transfer probed by spectroscopic methods and solid-phase changes
    • Sheth AR, Lubach JW, Munson EJ, Muller FX, Grant DJW. Mechanochromism of piroxicam accompanied by intermolecular proton transfer probed by spectroscopic methods and solid-phase changes. J. Am. Chem. Soc. 127(18), 6641-6651 (2005).
    • (2005) J. Am. Chem. Soc. , vol.127 , Issue.18 , pp. 6641-6651
    • Sheth, A.R.1    Lubach, J.W.2    Munson, E.J.3    Muller, F.X.4    Grant, D.J.W.5
  • 18
    • 33745660776 scopus 로고    scopus 로고
    • Solid-state acid-base interactions in complexes of heterocyclic bases with dicarboxylic acids: Crystallography, hydrogen bond analysis, and 15N NMR spectroscopy
    • Li ZJ, Abramov Y, Bordner J, Leonard J, Medek A, Trask AV. Solid-state acid-base interactions in complexes of heterocyclic bases with dicarboxylic acids: crystallography, hydrogen bond analysis, and 15N NMR spectroscopy. J. Am. Chem. Soc. 128(25), 8199-8210 (2006).
    • (2006) J. Am. Chem. Soc. , vol.128 , Issue.25 , pp. 8199-8210
    • Li, Z.J.1    Abramov, Y.2    Bordner, J.3    Leonard, J.4    Medek, A.5    Trask, A.V.6
  • 20
    • 33144460221 scopus 로고    scopus 로고
    • Quantitation of crystalline and amorphous forms of anhydrous neotame using 13C CPMAS NMR spectroscopy
    • Offerdahl TJ, Salsbury JS, Dong Z et al. Quantitation of crystalline and amorphous forms of anhydrous neotame using 13C CPMAS NMR spectroscopy. J. Pharm. Sci. 94(12), 2591-2605 (2005).
    • (2005) J. Pharm. Sci. , vol.94 , Issue.12 , pp. 2591-2605
    • Offerdahl, T.J.1    Salsbury, J.S.2    Dong, Z.3
  • 21
    • 4444355871 scopus 로고    scopus 로고
    • Fluorine in medicinal chemistry
    • Böhm HJ, Banner D, Bendels S et al. Fluorine in medicinal chemistry. ChemBioChem 5(5), 637-643 (2004).
    • (2004) ChemBioChem , vol.5 , Issue.5 , pp. 637-643
    • Böhm, H.J.1    Banner, D.2    Bendels, S.3
  • 22
    • 34848848499 scopus 로고    scopus 로고
    • Flourine in pharmaceuticals: Looking beyond intuition
    • Müller K, Faeh C, Diederich F. Flourine in pharmaceuticals: looking beyond intuition. Science 317(5846), 1881-1886 (2007).
    • (2007) Science , vol.317 , Issue.5846 , pp. 1881-1886
    • Müller, K.1    Faeh, C.2    Diederich, F.3
  • 23
    • 0038664748 scopus 로고    scopus 로고
    • Methods for the analysis and design of a solid-state nuclear magnetic resonance probe
    • Stringer JA, Drobny GP. Methods for the analysis and design of a solid-state nuclear magnetic resonance probe. J. Chem. Phys. 69(9), 3384-3391 (1998).
    • (1998) J. Chem. Phys. , vol.69 , Issue.9 , pp. 3384-3391
    • Stringer, J.A.1    Drobny, G.P.2
  • 24
    • 0035999082 scopus 로고    scopus 로고
    • 19F solid-state NMR spectroscopic investigation of crystalline and amorphous forms of a selective muscarinic M3 receptor antagonist, in both bulk and pharmaceutical dosage form samples
    • Wenslow RM. 19F solid-state NMR spectroscopic investigation of crystalline and amorphous forms of a selective muscarinic M3 receptor antagonist, in both bulk and pharmaceutical dosage form samples. Drug Dev. Ind. Pharm. 28(5), 555-561 (2002).
    • (2002) Drug Dev. Ind. Pharm. , vol.28 , Issue.5 , pp. 555-561
    • Wenslow, R.M.1
  • 25
    • 33847610330 scopus 로고    scopus 로고
    • Quantitation of crystalline material within a liquid vehicle using 1H/19F CP/MAS NMR
    • Farrer BT, Peresypkin A, Wenslow RM. Quantitation of crystalline material within a liquid vehicle using 1H/19F CP/MAS NMR. J. Pharm. Sci. 96(2), 264-267 (2007).
    • (2007) J. Pharm. Sci. , vol.96 , Issue.2 , pp. 264-267
    • Farrer, B.T.1    Peresypkin, A.2    Wenslow, R.M.3
  • 26
    • 57849156179 scopus 로고    scopus 로고
    • Characterization, selection, and development of an orally-dosed drug polymorph from an enantiotropically-related system
    • Katrincic LM, Sun YT, Carlton RA, Diederich AM, Mueller RL, Vogt FG. Characterization, selection, and development of an orally-dosed drug polymorph from an enantiotropically-related system. Int. J. Pharm. 366(1-2), 1-13 (2009).
    • (2009) Int. J. Pharm. , vol.366 , Issue.1-2 , pp. 1-13
    • Katrincic, L.M.1    Sun, Y.T.2    Carlton, R.A.3    Diederich, A.M.4    Mueller, R.L.5    Vogt, F.G.6
  • 27
    • 34247488844 scopus 로고    scopus 로고
    • Investigation of the effects of pharmaceutical processing upon solid-state NMR relaxation times and implications to solid-state formulation stability
    • Lubach JW, Xu D, Segmuller BE, Munson EJ. Investigation of the effects of pharmaceutical processing upon solid-state NMR relaxation times and implications to solid-state formulation stability. J. Pharm. Sci. 96(4), 777-787 (2007).
    • (2007) J. Pharm. Sci. , vol.96 , Issue.4 , pp. 777-787
    • Lubach, J.W.1    Xu, D.2    Segmuller, B.E.3    Munson, E.J.4
  • 29
    • 23644454677 scopus 로고    scopus 로고
    • Quantification of bambuterol hydrochloride in a formulated product using solid-state NMR
    • Harris RK, Hodgkinson P, Larsson T, Muruganantham A. Quantification of bambuterol hydrochloride in a formulated product using solid-state NMR. J. Pharm. Biomed. Anal. 38(5), 858-864 (2005).
    • (2005) J. Pharm. Biomed. Anal. , vol.38 , Issue.5 , pp. 858-864
    • Harris, R.K.1    Hodgkinson, P.2    Larsson, T.3    Muruganantham, A.4
  • 30
    • 33750582144 scopus 로고    scopus 로고
    • Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance
    • Mollica G, Geppi M, Pignatello R, Veracini CA. Molecular properties of flurbiprofen and its solid dispersions with Eudragit RL100 studied by high- and low-resolution solid-state nuclear magnetic resonance. Pharm. Res. 23(9), 2129-2140 (2006).
    • (2006) Pharm. Res. , vol.23 , Issue.9 , pp. 2129-2140
    • Mollica, G.1    Geppi, M.2    Pignatello, R.3    Veracini, C.A.4
  • 31
    • 0036066542 scopus 로고    scopus 로고
    • Solid-state NMR spectroscopy of small molecules: From NMR crystallography to the characterization of solid oral dosage forms
    • Reutzel-Edens SM, Bush JK. Solid-state NMR spectroscopy of small molecules: from NMR crystallography to the characterization of solid oral dosage forms. Am. Pharm. Rev. 5(2), 112-115 (2002).
    • (2002) Am. Pharm. Rev. , vol.5 , Issue.2 , pp. 112-115
    • Reutzel-Edens, S.M.1    Bush, J.K.2
  • 32
    • 55849083074 scopus 로고    scopus 로고
    • A multi-disciplinary approach to the solid-state analysis of pharmaceuticals
    • Vogt FG. A multi-disciplinary approach to the solid-state analysis of pharmaceuticals. Am. Pharm. Rev. 11(5), 50-57 (2008).
    • (2008) Am. Pharm. Rev. , vol.11 , Issue.5 , pp. 50-57
    • Vogt, F.G.1
  • 34
    • 0346938543 scopus 로고    scopus 로고
    • High-field and high-speed CP-MAS 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling
    • van Rossum BJ, Förster H, de Groot HJM. High-field and high-speed CP-MAS 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling. J. Magn. Reson. 124, 516-519. (1997).
    • (1997) J. Magn. Reson. , vol.124 , pp. 516-519
    • Van Rossum, B.J.1    Förster, H.2    De Groot, H.J.M.3
  • 35
    • 33750364928 scopus 로고    scopus 로고
    • Physical, crystallographic, and spectroscopic characterization of a crystalline pharmaceutical hydrate: Understanding the role of water
    • Vogt FG, Brum J, Katrincic LM et al. Physical, crystallographic, and spectroscopic characterization of a crystalline pharmaceutical hydrate: understanding the role of water. Cryst. Growth Des. 6(1), 2333-2354 (2006).
    • (2006) Cryst. Growth Des. , vol.6 , Issue.1 , pp. 2333-2354
    • Vogt, F.G.1    Brum, J.2    Katrincic, L.M.3
  • 36
    • 53249113784 scopus 로고    scopus 로고
    • Rapid analysis of organic compounds by proton-detected heteronuclear correlation NMR spectroscopy with 40 kHz magic-angle spinning
    • Zhou DH, Rienstra CM. Rapid analysis of organic compounds by proton-detected heteronuclear correlation NMR spectroscopy with 40 kHz magic-angle spinning. Angew. Chem. Int. Ed. 47(38), 7328-7331 (2008).
    • (2008) Angew. Chem. Int. Ed. , vol.47 , Issue.38 , pp. 7328-7331
    • Zhou, D.H.1    Rienstra, C.M.2
  • 37
    • 35648929928 scopus 로고    scopus 로고
    • Distinguishing anhydrous and hydrous forms of an active pharmaceutical ingredient in a tablet formulation using solid-state NMR spectroscopy
    • Griffin JM, Martin DR, Brown SP. Distinguishing anhydrous and hydrous forms of an active pharmaceutical ingredient in a tablet formulation using solid-state NMR spectroscopy. Angew. Chem. Int. Ed. 46, 8036-8038 (2007).
    • (2007) Angew. Chem. Int. Ed. , vol.46 , pp. 8036-8038
    • Griffin, J.M.1    Martin, D.R.2    Brown, S.P.3
  • 38
    • 21244479996 scopus 로고    scopus 로고
    • Powder crystallography by proton solid-state NMR
    • Elena B, Emsley L. Powder crystallography by proton solid-state NMR. J. Am. Chem. Soc. 127(25), 9140-9146 (2005).
    • (2005) J. Am. Chem. Soc. , vol.127 , Issue.25 , pp. 9140-9146
    • Elena, B.1    Emsley, L.2
  • 39
    • 33746356891 scopus 로고    scopus 로고
    • Molecular structure determination in powders by NMR crystallography from proton spin diffusion
    • Elena B, Pintacuda G, Mifsud N, Emsley L. Molecular structure determination in powders by NMR crystallography from proton spin diffusion. J. Am. Chem. Soc. 128(29), 9555-9560 (2006).
    • (2006) J. Am. Chem. Soc. , vol.128 , Issue.29 , pp. 9555-9560
    • Elena, B.1    Pintacuda, G.2    Mifsud, N.3    Emsley, L.4
  • 40
    • 34547469091 scopus 로고    scopus 로고
    • Resolving structures from powders by NMR crystallography using combined proton spin diffusion and plane wave DFT calculations
    • Pickard CJ, Salager E, Pintacuda G, Elena B, Emsley L. Resolving structures from powders by NMR crystallography using combined proton spin diffusion and plane wave DFT calculations. J. Am. Chem. Soc. 129(29), 8932-8933 (2007).
    • (2007) J. Am. Chem. Soc. , vol.129 , Issue.29 , pp. 8932-8933
    • Pickard, C.J.1    Salager, E.2    Pintacuda, G.3    Elena, B.4    Emsley, L.5
  • 41
    • 55749115595 scopus 로고    scopus 로고
    • Enantiotropically-related polymorphs of {4-(4-chloro-3-fluorophenyl)-2- [4- (methyloxy)phenyl] -1,3-thiazol-5-yl} acetic acid. Crystal structures and multinuclear solid-state NMR
    • Vogt FG, Katrincic LM, Long ST et al. Enantiotropically-related polymorphs of {4-(4-chloro-3-fluorophenyl)-2-[4- (methyloxy)phenyl]-1,3-thiazol- 5-yl} acetic acid. Crystal structures and multinuclear solid-state NMR. J. Pharm. Sci. 97(11), 4756-4782 (2008).
    • (2008) J. Pharm. Sci. , vol.97 , Issue.11 , pp. 4756-4782
    • Vogt, F.G.1    Katrincic, L.M.2    Long, S.T.3
  • 45
    • 67649134796 scopus 로고    scopus 로고
    • Pharmaceutical co-crystals - An opportunity for drug product enhancement
    • Miroshnyk I, Mirza S, Sandler N. Pharmaceutical co-crystals - an opportunity for drug product enhancement. Exp. Opin. Drug Delivery 6(4), 333-341 (2009).
    • (2009) Exp. Opin. Drug Delivery , vol.6 , Issue.4 , pp. 333-341
    • Miroshnyk, I.1    Mirza, S.2    Sandler, N.3
  • 46
    • 61449224880 scopus 로고    scopus 로고
    • Formation and characterization of crystals containing a pleuromutilin derivative, succinic acid and water
    • Clawson JS, Vogt FG, Brum J et al. Formation and characterization of crystals containing a pleuromutilin derivative, succinic acid and water. Cryst. Growth Des. 8(11), 4120-4131 (2008).
    • (2008) Cryst. Growth Des. , vol.8 , Issue.11 , pp. 4120-4131
    • Clawson, J.S.1    Vogt, F.G.2    Brum, J.3
  • 48
    • 77953151209 scopus 로고    scopus 로고
    • Isomorphism, disorder and hydration in the crystal structures of racemic and single-enantiomer carvedilol phosphate
    • In press
    • Vogt FG, Copley RCB, Mueller RL et al. Isomorphism, disorder and hydration in the crystal structures of racemic and single-enantiomer carvedilol phosphate. Cryst. Growth Des. In press (2010).
    • (2010) Cryst. Growth des
    • Vogt, F.G.1    Copley, R.C.B.2    Mueller, R.L.3
  • 49
    • 50249132472 scopus 로고    scopus 로고
    • Application of solid-state 35Cl NMR to structural characterization of hydrochloride pharmaceuticals and their polymorphs
    • Hamaed H, Pawlowski JM, Cooper BFT, Fu RQ, Eichhorn SH, Schurko RW. Application of solid-state 35Cl NMR to structural characterization of hydrochloride pharmaceuticals and their polymorphs. J. Am. Chem. Soc. 130(33), 11056-11065 (2008).
    • (2008) J. Am. Chem. Soc. , vol.130 , Issue.33 , pp. 11056-11065
    • Hamaed, H.1    Pawlowski, J.M.2    Cooper, B.F.T.3    Fu, R.Q.4    Eichhorn, S.H.5    Schurko, R.W.6
  • 50
    • 70349632845 scopus 로고    scopus 로고
    • Low temperature 65Cu NMR spectroscopy of the Cu+ site in azurin
    • Lipton AS, Heck RW, de Jong WA et al. Low temperature 65Cu NMR spectroscopy of the Cu+ site in azurin, J. Am. Chem. Soc. 131(39), 13992-13999 (2009).
    • (2009) J. Am. Chem. Soc. , vol.131 , Issue.39 , pp. 13992-13999
    • Lipton, A.S.1    Heck, R.W.2    De Jong, W.A.3
  • 51
    • 32644460308 scopus 로고    scopus 로고
    • A study of variable hydration states in topotecan hydrochloride
    • Vogt FG, Dell'Orco PC, Diederich AM et al. A study of variable hydration states in topotecan hydrochloride. J. Pharm. Biomed. Anal. 40(5), 1080-1088 (2006).
    • (2006) J. Pharm. Biomed. Anal. , vol.40 , Issue.5 , pp. 1080-1088
    • Vogt, F.G.1    Dell'Orco, P.C.2    Diederich, A.M.3
  • 52
    • 38849108169 scopus 로고    scopus 로고
    • Solid-state NMR spectroscopy of amyloid proteins
    • Heise H. Solid-state NMR spectroscopy of amyloid proteins, ChemBioChem 9(2), 179-189 (2008).
    • (2008) ChemBioChem , vol.9 , Issue.2 , pp. 179-189
    • Heise, H.1
  • 53
    • 33846027490 scopus 로고    scopus 로고
    • NMR methods for characterising ligand-receptor and drug-membrane interactions in pharmaceutical research
    • Middleton DA. NMR methods for characterising ligand-receptor and drug-membrane interactions in pharmaceutical research. Ann. Rep. NMR Spectros. 60, 39-75 (2006).
    • (2006) Ann. Rep. NMR Spectros. , vol.60 , pp. 39-75
    • Middleton, D.A.1
  • 54
    • 33749049148 scopus 로고    scopus 로고
    • Molecular interactions investigated by multi-dimensional solid-state NMR
    • DOI 10.1016/j.sbi.2006.08.003, PII S0959440X06001382, Carbohydrates and Glycoconjugates / Biophysical Methods
    • Baldus M. Molecular interactions investigated by multi-dimensional solid-state NMR. Curr. Opin. Struct. Biol. 16(5), 618-623 (2006). (Pubitemid 44466405)
    • (2006) Current Opinion in Structural Biology , vol.16 , Issue.5 , pp. 618-623
    • Baldus, M.1
  • 55
    • 67649399085 scopus 로고    scopus 로고
    • Solid-state NMR for the analysis of high-affinity ligand/receptor interactions
    • Williamson PTF. Solid-state NMR for the analysis of high-affinity ligand/receptor interactions. Concepts Magn. Reson. 34A(3), 144-172 (2009).
    • (2009) Concepts Magn. Reson. , vol.34 A , Issue.3 , pp. 144-172
    • Williamson, P.T.F.1
  • 56
    • 34848898190 scopus 로고    scopus 로고
    • Backbone assignments in solid-state proteins using J-based 3D heteronuclear correlation spectroscopy
    • Chen L, Kaiser JM, Polenova T, Yang J, Rienstra CM, Mueller LJ. Backbone assignments in solid-state proteins using J-based 3D heteronuclear correlation spectroscopy. J. Am. Chem. Soc. 129(35), 10650-10651 (2007).
    • (2007) J. Am. Chem. Soc. , vol.129 , Issue.35 , pp. 10650-10651
    • Chen, L.1    Kaiser, J.M.2    Polenova, T.3    Yang, J.4    Rienstra, C.M.5    Mueller, L.J.6
  • 57
    • 33846422346 scopus 로고    scopus 로고
    • Proton-detected 14N MAS NMR using homonuclear decoupled rotary resonance
    • Gan Z, Amoureux JP, Trebosc J. Proton-detected 14N MAS NMR using homonuclear decoupled rotary resonance. Chem. Phys. Lett. 435(1-3), 163-169 (2007).
    • (2007) Chem. Phys. Lett. , vol.435 , Issue.1-3 , pp. 163-169
    • Gan, Z.1    Amoureux, J.P.2    Trebosc, J.3
  • 58
    • 67650564613 scopus 로고    scopus 로고
    • Fast and simple acquisition of solid-state 14N NMR spectra with signal enhancement via population transfer
    • O'Dell LA, Schurko RW. Fast and simple acquisition of solid-state 14N NMR spectra with signal enhancement via population transfer. J. Am. Chem. Soc. 131(19), 6658-6659 (2009).
    • (2009) J. Am. Chem. Soc. , vol.131 , Issue.19 , pp. 6658-6659
    • O'Dell, L.A.1    Schurko, R.W.2
  • 59
    • 76249124885 scopus 로고    scopus 로고
    • Homogeneous nanoparticles to enhance the efficiency of a hydrophobic drug, antihyperlipidemic probucol, characterized by solid-state NMR
    • Io T, Fukami T, Yamamoto K et al. Homogeneous nanoparticles to enhance the efficiency of a hydrophobic drug, antihyperlipidemic probucol, characterized by solid-state NMR. Mol. Pharm. 7(1), 299-305 (2010).
    • (2010) Mol. Pharm. , vol.7 , Issue.1 , pp. 299-305
    • Io, T.1    Fukami, T.2    Yamamoto, K.3
  • 60
    • 57349122408 scopus 로고    scopus 로고
    • Storage stability of freeze-dried human growth hormone (hGH) with structure and dynamics in the glassy solid
    • Pikal MJ, Rigsbee D, Roy ML et al. Storage stability of freeze-dried human growth hormone (hGH) with structure and dynamics in the glassy solid. J. Pharm. Sci. 97, 5106-5121 (2008).
    • (2008) J. Pharm. Sci. , vol.97 , pp. 5106-5121
    • Pikal, M.J.1    Rigsbee, D.2    Roy, M.L.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.