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For transformation of 3E,6R,7R-laurediol to deacetyl-laurencin by LPO, see
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In vitro studies have shown that laureatin and isolaureatin are derived from Z-prelaureatin by LPO and that laurallene is derived from E-prelaureatin by bromoperoxidase (BPO), see
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In vitro studies have shown that laureatin and isolaureatin are derived from Z-prelaureatin by LPO and that laurallene is derived from E-prelaureatin by bromoperoxidase (BPO), see. Ishihara J., Shimada Y., Kanoh N., Takasugi Y., Fukuzawa A., and Murai A. Tetrahedron 53 (1997) 8371
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For a review of the construction of medium-ring ethers, see. For total syntheses of (+)-prelaureatin, see
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For a review of the construction of medium-ring ethers, see. Elliott M.C. For total syntheses of (+)-prelaureatin, see. Contemp. Org. Synth. 1 (1994) 457
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For total syntheses of (+)-laurallene, see
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Also see reference 10b. For a total synthesis of natural (+)-laurenyne, see
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Also see reference 10b. For a total synthesis of natural (+)-laurenyne, see. Saitoh T., Suzuki T., Sugimoto M., Hagiwara H., and Hoshi T. Tetrahedron Lett. 44 (2003) 3175
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For representative examples of total syntheses of (+)-laurencin, see:
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The Schrock molybdenum complex is commercially available (Strem) and can be prepared according to the reported procedure with consistent purity and reactivity, see
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The Schrock molybdenum complex is commercially available (Strem) and can be prepared according to the reported procedure with consistent purity and reactivity, see. Fox H.H., Yap K.B., Robbins J., Cai S., and Schrock R.R. Inorg. Chem. 31 (1992) 2287
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To the best of our knowledge, the ring opening of a 1,3-dioxolanone with bis(trimethylsilyl)acetylene is unpreccedented. Ring opening of acetal templates with silylacetylenic compounds promoted by Lewis acid have been reported, see
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To the best of our knowledge, the ring opening of a 1,3-dioxolanone with bis(trimethylsilyl)acetylene is unpreccedented. Ring opening of acetal templates with silylacetylenic compounds promoted by Lewis acid have been reported, see. Johnson W.S., Elliott R., and Elliott J.D. J. Am. Chem. Soc. 105 (1983) 2904
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For some representative examples of ring opening of acetal templates, see. Mori A., Ishihara K., Arai I., and Yamamoto H. Tetrahedron 43 (1987) 755
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For examples using acetylenic organometallic reagents, see reference 18. For mechanism studies, see
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