Validation of a nanoliquid chromatography-tandem mass spectrometry method for the identification and the accurate quantification by isotopic dilution of glutathionylated and cysteinylated precursors of 3-mercaptohexan-1-ol and 4-mercapto-4-methylpentan-2-one in white grape juices

Journal of Chromatography A

Volumn 1217, Issue 10, 2010, Pages 1626-1635

  Roland, Aurélie ^a,b   Vialaret, Jérôme ^a   Moniatte, Marc ^a   Rigou, Peggy ^b   Razungles, Alain ^b   Schneider, Rémi ^c  

^a EPFL   (Switzerland)

^b MONTPELLIER SUPAGRO   (France)

^c SPO   (France)

Author keywords

Cysteinylated conjugates; Glutathionylated conjugates; grape; LC MS MS; stable isotope dilution assay; thiols

Indexed keywords

ANALYTES; CALIBRATION CURVES; CATION EXCHANGE RESINS; CORRELATION COEFFICIENT; DEUTERATED ANALOGUE; EXTERNAL CALIBRATION; GRAPE JUICE; INTERNATIONAL CONFERENCE ON HARMONIZATIONS; ISOTOPIC DILUTION; LACK-OF-FIT TEST; LC-MS/MS; LIMITS OF QUANTIFICATION; LINEAR MODEL; MATRIX EFFECTS; NANO LIQUID CHROMATOGRAPHY; NANOLC-MS/MS; QUADRATIC MODELS; REPRODUCIBILITIES; REVERSE-PHASE COLUMN; SELECTED REACTION MONITORING; SIMULTANEOUS DETERMINATIONS; STABLE ISOTOPE DILUTION ASSAY; TANDEM MASS SPECTROMETRY;

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; DEUTERIUM; DILUTION; FRUIT JUICES; HOUSING; MASS SPECTROMETERS; MASS SPECTROMETRY; METAL VAPOR LAMPS; RESINS; ULSI CIRCUITS;

CALIBRATION;

3 MERCAPTOHEXAN 1 OL; 4 MERCAPTO 4 METHYLPENTAN 2 ONE; FLAVORING AGENT; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CALCULATION; CALIBRATION; CATION EXCHANGE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; CHROMATOGRAPHY; GRAPE JUICE; ISOTOPE DILUTION ASSAY; NANOLIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY; PRIORITY JOURNAL; PROCESS OPTIMIZATION; PURIFICATION; REPRODUCIBILITY; SEPARATION TECHNIQUE; TANDEM MASS SPECTROMETRY; VALIDITY;

BEVERAGES; CHROMATOGRAPHY, LIQUID; INDICATOR DILUTION TECHNIQUES; ISOTOPES; SULFHYDRYL COMPOUNDS; TANDEM MASS SPECTROMETRY; VITIS;

CUCUMIS; VITACEAE;

EID: 75949108873     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.01.031     Document Type: Article

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