Synthesis and reactivity of titanium and zirconium complexes supported by a multidentate monoanionic [N 2 P 2] ligand

Organometallics

Volumn 28, Issue 12, 2009, Pages 3338-3349

  Chomitz, Wayne A ^a   Sutton, Andrew D ^a   Krinsky, Jamin L ^a   Arnold, John ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CATIONIC SPECIES; COORDINATION BEHAVIOR; COORDINATION CHEMISTRY; DEGREE OF REDUCTION; HALIDE COMPLEXES; IMIDO COMPLEXES; MULTIDENTATE; MULTIDENTATE LIGANDS; NMR AND X-RAY; ZIRCONIUM COMPLEXES;

ALKYLATION; DYES; HYDROCARBONS; LIGANDS; SYNTHESIS (CHEMICAL); TITANIUM; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION; ZIRCONIUM; ZIRCONIUM COMPOUNDS;

TITANIUM COMPOUNDS;

EID: 67449111008     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om8011932     Document Type: Article

References (75)

1. Fryzuk, M. D.; Giesbrecht, G.; Rettig, S. J. Organometallics 1996, 15, 3329-3336.
2. Fryzuk, M. D.; Mao, S. S. H.; Zaworotko, M. J.; Macgillivray, L. R. J. Am. Chem. Soc. 1993, 115, 5336-5337.
3. Fryzuk, M. D.; Haddad, T. S.; Rettig, S. J. J. Am. Chem. Soc. 1990, 112, 8185-8186.
4. Bailey, B. C.; Fan, H. J.; Huffman, J. C.; Baik, M. H.; Mindiola, D. J. J. Am. Chem. Soc. 2007, 129, 8781-8793.
5. Kilgore, U. J.; Yang, X. F.; Tomaszewski, J.; Huffman, J. C.; Mindiola, D. J. Inorg. Chem. 2006, 45, 10712-10721.
6. Gerber, L. C. H.; Watson, L. A.; Parkin, S.; Weng, W.; Foxman, B. M.; Ozerov, O. V. Organometallics 2007, 26, 4866-4868.
7. Weng, W.; Yang, L.; Foxman, B. M.; Ozerov, O. V. Organometallics 2004, 23, 4700-4705.
8. Minasian, S. G.; Arnold, J. Dalton Trans. 2009, 1714-1720.
9. Bambirra, S.; Boot, S. J.; van Leusen, D.; Meetsma, A.; Hessen, B. Organometallics 2004, 23, 1891-1898.
10. Chomitz, W. A.; Minasian, S. G.; Sutton, A. D.; Arnold, J. Inorg. Chem. 2007, 46, 7199-7209.
11. Marinescu, S. C.; Agapie, T.; Day, M. W.; Bercaw, J. E. Organometallics 2007, 26, 1178-1190.
12. 31P NMR spectroscopy is a useful diagnostic tool, and a good deal of structural information on the reported compounds is based on these data.
13. Chomitz, W. A.; Arnold, J. Chem. Commun. 2007, 4797-4799.
14. Chomitz, W. A.; Arnod, J. Chem. Eur. J. 2009, 15, 2020-2030.
15. Alaimo, P. J.; Peters, D. W.; Arnold, J.; Bergman, R. G. J. Chem. Educ. 2001, 78, 64-64.
16. Piguet, C. J. Chem. Educ. 1997, 74, 815-816.
17. Chomitz, W. A.; Mickenberg, S. F.; Arnold, J. Inorg. Chem. 2008, 47, 373-380.
18. Manzer, L. E. Inorg. Synth. 1982, 21, 135-140.
19. Crane, F. E. Anal. Chem. 1956, 28, 1794-1797.
20. Jones, N. A.; Liddle, S. T.; Wilson, C.; Arnold, P. L. Organometallics 2007, 26, 755-757.
21. Gavenonis, J.; Tilley, T. D. Organometallics 2002, 21, 5549-5563.
22. Carmalt, C. J.; Newport, A. C.; Parkin, I. P.; White, A. J. P.; Williams, D. J. J. Chem. Soc., Dalton Trans. 2002, 4055-4059.
23. Weber, W. P.; Ugi, I. K.; Gokel, G. W. Angew. Chem., Int. Ed. Engl. 1972, 11, 530.
24. SMART: Area-Detector Software Package; Bruker Analytical X-ray Systems, Inc.: Madison, WI, 1995-1999.
25. SAINT: SAX Area-Detector Integration Program, version 7.06; Siemens Industrial Automation, Inc.: Madison, WI, 2005.
26. XPREP (v6.12): Part of the SHELXTL Crystal Structure Determination Package; Bruker AXS Inc.: Madison, WI, 1995.
27. Sheldrick, G. SADABS (v2.10): Siemens Area Detector ABSorption correction program; Bruker Analytical X-ray Systems Inc.: Madison, WI, 2005.
28. XS: Program for the Refinement of X-ray Crystal Structures, Part of the SHELXTL Crystal Structure Determination Package; Bruker Analytical X-ray Systems Inc.: Madison, WI, 1995-1999.
29. XL: Program for the Refinement of X-ray Crystal Structures, Part of the SHELXT Crystal Structure Determination Package; Bruker Analytical Systems Inc.: Madison, WI: 1995-1999.
30. Ghesner, I.; Fenwick, A.; Stephan, D. W. Organometallics 2006, 25, 4985-4995.
31. Chauvin, Y.; Grubbs, R. H.; Schrock, R. R. "for the development of the metathesis method in organic synthesis".
32. Nugent, W. A.; Mayer, J. M. Metal-ligand multiple bonds; John Wiley & Sons Inc.: New York, 1988.
33. Walsh, P. J.; Hollander, F. J.; Bergman, R. G. J. Am. Chem. Soc. 1988, 110, 8729-8731.
34. Bart, S. C.; Lobkovsky, E.; Bill, E.; Chirik, P. J. J. Am. Chem. Soc. 2006, 128, 5302-5303.
35. Dewith, J.; Horton, A. D. Angew. Chem., Int. Ed. Engl. 1993, 32, 903-905.
36. Jenkins, D. M.; Betley, T. A.; Peters, J. C. J. Am. Chem. Soc. 2002, 124, 11238-11239.
37. Kogut, E.; Wiencko, H. L.; Zhang, L. B.; Cordeau, D. E.; Warren, T. H. J. Am. Chem. Soc. 2005, 127, 11248-11249.
38. Mindiola, D. J.; Hillhouse, G. L. Chem. Commun. 2002, 1840-1841.
39. Shay, D. T.; Yap, G. P. A.; Zakharov, L. N.; Rheingold, A. L.; Theopold, K. H. Angew. Chem., Int. Ed. 2005, 44, 1508-1510.
40. Shay, D. T.; Yap, G. P. A.; Zakharov, L. N.; Rheingold, A. L.; Theopold, K. H. Angew. Chem., Int. Ed. 2006, 45, 7870-7870.
41. Cummins, C. C.; Baxter, S. M.; Wolczanski, P. T. J. Am. Chem. Soc. 1988, 110, 8731-8733.
42. MacLachlan, E. A.; Fryzuk, M. D. Organometallics 2006, 25, 1530-1543.
43. Hirotsu, M.; Fontaine, P. P.; Zavalij, P. Y.; Sita, L. R. J. Am. Chem. Soc. 2007, 129, 12690-12692.
44. Fryzuk, M. D.; Love, J. B.; Rettig, S. J.; Young, V. G. Science 1997, 275, 1445-1447.
45. Pool, J. A.; Lobkovsky, E.; Chirik, P. J. Nature 2004, 427, 527-530.
46. Morello, L.; Yu, P. H.; Carmichael, C. D.; Patrick, B. O.; Fryzuk, M. D. J. Am. Chem. Soc. 2005, 127, 12796-12797.
47. Cambridge Structural Database: Allen, F. H. Acta Crystallogr. 2002, B58, 380-388.
48. Cotton, F. A.; Diebold, M. P.; Kibala, P. A. Inorg. Chem. 1988, 27, 799-804.
49. Hoffman, D. M.; Lee, S. Inorg. Chem. 1992, 31, 2676-2677.
50. Wengrovius, J. H.; Schrock, R. R.; Day, C. S. Inorg. Chem. 1981, 20, 1844-1849.
51. Stephens, P. J.; Devlin, F. J.; Chabalowski, C. F.; Frisch, M. J. J. Phys. Chem. 1994, 98, 11623-11627.
52. Francl, M. M.; Pietro, W. J.; Hehre, W. J.; Binkley, J. S.; Gordon, M. S.; DeFrees, D. J.; Pople, J. A. J. Phys. Chem. 1982, 77, 3654-3665.
53. Hay, P. J.; Wadt, W. R. J. Phys. Chem. 1985, 82, 299-310.
54. Ditchfield, R.; Hehre, W. J.; Pople, J. A. J. Phys. Chem. 1971, 54, 724-728.
55. Hehre, W. J.; Ditchfield, R.; Pople, J. A. J. Phys. Chem. 1972, 56, 2257-2261.
56. Hariharan, P. C.; Pople, J. A. Theor. Chim. Acta 1973, 28, 213-222.
57. Jaguar, version 6.5;Schrodinger, LLC: New York, 2005.
58. Maestro, version 7.5; Schrondinger, LLC: New York, 2005.
59. For recent work with terphenylisocyanides, see: Fox, B. J.; Sun, Q. Y.; DiPasquale, A. G.; Fox, A. R.; Rheingold, A. L.; Figueroa, J. S. Inorg. Chem. 2008, 47, 9010-9020.
60. Galan, B. R.; Gembicky, M.; Dominiak, P. M.; Keister, J. B.; Diver, S. T. J. Am. Chem. Soc. 2005, 127, 15702-15703.
61. Boyer, J. H.; Jong, J. D. J. Am. Chem. Soc. 1969, 91, 5929-5930.
62. Pinkas, J.; Lukesova, L.; Gyepes, R.; Cisarova, I.; Lonnecke, P.; Kubista, J.; Horacek, M.; Mach, K. Organometallics 2007, 26, 3100-3110.
63. Hagadorn, J. R.; Arnold, J. J. Am. Chem. Soc. 1996, 118, 893-894.
64. Budzelaar, P. H. M.; van Oort, A. B.; Orpen, A. G. Eur. J. Inorg. Chem. 1998, 1485-1494.
65. Cohen, J. D.; Fryzuk, M. D.; Loehr, T. M.; Mylvaganam, M.; Rettig, S. J. Inorg. Chem. 1998, 37, 112-119.
66. Beydoun, N.; Duchateau, R.; Gambarotta, S. J. Chem. Soc., Chem. Commun. 1992, 244-246.
67. Studt, F.; Lehnert, N.; Wiesler, B. E.; Scherer, A.; Beckhaus, R.; Tuczek, F. Eur. J. Inorg. Chem. 2006, 291-297.
68. Haskel, A.; Straub, T.; Eisen, M. S. Organometallics 1996, 15, 3773-3775.
69. Kilgore, U. J.; Basuli, F.; Huffman, J. C.; Mindiola, D. J. Inorg. Chem. 2006, 45, 487-489.
70. Boyd, C. L.; Clot, E.; Guiducci, A. E.; Mountford, P. Organometallics 2005, 24, 2347-2367.
71. Guiducci, A. E.; Boyd, C. L.; Mountford, P. Organometallics 2006, 25, 1167-1187.
72. Boyd, C. L.; Toupance, T.; Tyrrell, B. R.; Ward, B. D.; Wilson, C. R.; Cowley, A. R.; Mountford, P. Organometallics 2005, 24, 309-330.
73. Stewart, P. J.; Blake, A. J.; Mountford, P. Organometallics 1998, 17, 3271-3281.
74. Blake, A. J.; Dunn, S. C.; Green, J. C.; Jones, N. M.; Moody, A. G.; Mountford, P. Chem. Commun. 1998, 1235-1236.
75. Horton, A. D.; DeWith, J.; vanderLinden, A. J.; vandeWeg, H. Organometallics 1996, 15, 2672-2674.