Multiresidue analysis of 47 pesticides in cooked wheat flour and polished rice by liquid chromatography with tandem mass spectrometry

Biomedical Chromatography

Volumn 23, Issue 4, 2009, Pages 434-442

  Lee, Sung Jung ^a   Park, Hyeong Jin ^a   Kim, Wooseong ^b   Jin, Jong Sung ^c   El Aty, A M Abd ^d,e   Shim, Jae Han ^f   Shin, Sung Chul ^a  

^a Gyeongsang National University   (South Korea)

^b Korea Food and Drug Administration   (South Korea)

^c Korea Basic Science Institute (KBSI)   (South Korea)

^d Konkuk University   (South Korea)

^e Cairo University   (Egypt)

^f Chonnam National University   (South Korea)

Author keywords

Bioanalytical application; Multiresidue; Pesticide residues; Tandem mass spectrometry; Validation

Indexed keywords

CHEMICAL CONTAMINATION; ELECTROSPRAY IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

BIOANALYTICAL APPLICATIONS; FOOD AND DRUG ADMINISTRATION; MULTIRESIDUE; PESTICIDE RESIDUE; POLISHED RICE; RICE SAMPLES; TANDEM MASS SPECTROMETRY; TANDEM-MASS SPECTROMETRY; VALIDATION; WHEAT FLOURS;

PESTICIDES;

ALDICARB; BENDIOCARB; CARBARIL; ETHIOFENCARB; FENOBUCARB; ISOPROCARB; METHABENZTHIAZURON; METHIOCARB; METHOMYL; PESTICIDE; PIRIMICARB; PROPOXUR; PYRIPROXYFEN; TEBUFENOZIDE;

ARTICLE; COOKED FOOD; ELECTROSPRAY MASS SPECTROMETRY; FLOUR; FOOD ANALYSIS; KOREA; LIQUID CHROMATOGRAPHY; QUANTITATIVE ANALYSIS; RESIDUE ANALYSIS; RICE; TANDEM MASS SPECTROMETRY;

TRITICUM AESTIVUM;

EID: 65349140042     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.1140     Document Type: Article

References (33)

1. Alder L, Greulich K, Kempe G and Vieth B. Residue analysis of 500 high priority pesticides: better by GC-MS or LC-MS/MS? Mass Spectrometry Reviews 2006; 25: 838-865.
2. Cavaliere C, Foglia P, Pastorino E, Samperi R and Lagana A. Development of a multiresidue method for analysis of major Fusarium mycotoxins in corn meal using liquid chromatography/tandem mass spectrometry. Rapid Communications in Mass Spectrometry 2005; 19: 2085-2093.
3. Cech NB and Enke CG. Relating electrospray ionization response to nonpolar character of small peptides. Analytical Chemistry 2000; 72: 2717-2723.
4. Chen T and Chen G. Identification and quantitation of pyrethroid pesticide residues in vegetables by solid-phase extraction and liquid chromatography/electrospray ionization ion trap mass spectrometry. Rapid Communications in Mass Spectrometry 2007; 21: 1848-1854.
5. Choi BK, Hercules DM and Gusev AI. Effect of liquid chromatography separation of complex matrices on liquid chromatography-tandem mass spectrometry signal suppression. Journal of Chromatography A 2001; 907: 337-342.
6. Codex Alimentarius Commission. Codex Maximum Residue Limits for pesticides, http://apps.fao.org/faostat/collections?version= ext&hasbulk=0&subset=FoodQuality. FAO/WHO: Rome, 2005.
7. Eddleston M, Karalliedde L, Buckley N, Fernando R, Hutchinson G, Isbister G, Konradsen F, Murray D, Piola JC, Senanayake N, Sheriff R, Singh S, Siwach SB and Smit L. Pesticide poisoning in the developing world - a minimum pesticides list. Lancet 2002; 360: 1163-1167. European Union On-line, Plant Health. Pesticide Residue, http://europa.eu.int/comm/food/plant/protection/pesticides/ index-en.htm. European Union: Brussels, 2005.
8. Fong WG, Moye HA, Siber JN and Toth JP (eds). Pesticides Residues in Food. Wiley: New York, 1999.
9. Granby K, Andersen JH and Christensen HB. Analysis of pesticides in fruit, vegetables and cereals using methanolic extraction and detection by liquid chromatography-tandem mass spectrometry. Analytica Chimica Acta 2004; 520: 165-176.
10. Hernández F, Pozo OJ, Sancho JV, Bijlsma L, Barreda M and Pitarch E. Multiresidue liquid chromatography tandem mass spectrometry determination of 52 non gas chromatography-amenable pesticides and metabolites in different food commodities. Journal of Chromatography A 2006; 1109: 242-252.
11. Hiemstra M and de Kok A. Comprehensive multi-residue method for the target analysis of pesticides in crops using liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 2007; 1154: 3-25.
12. Hill ARC. Quality control procedures for pesticide residues analysis, European Commission Document 7826/VI/97. European Union: Brussels 1997.
13. Jansson C, Pihlstrom T, Osterdahl BG and Markides KE. A new multi-residue method for analysis of pesticide residues in fruit and vegetables using liquid chromatography with tandem mass spectrometric detection. Journal of Chromatography A 2004; 1023: 93-104.
14. King R, Bonfiglio R, Fernandez-Metzler C, Miller-Stein C and Olah T. Mechanistic investigation of ionization suppression in electrospray ionization. Journal of the American Society for Mass Spectrometry 2000; 11: 942-950.
15. Klein J and Alder L. Applicability of gradient liquid chromatography with tandem mass spectrometry to the simultaneous screening for about 100 pesticides in crops. Journal of AOAC International 2003; 86: 1015-1037.
16. Korea Food and Drug Administration. Maximum Residue Levels for Pesticides. KFDA: Seoul, 2005. Available at: http://www.kfda.go.kr
17. Mertz C, Cheynier V, Günata Z and Brat P. Analysis of phenolic compounds in two blackberry species (Rubus glaucus and Rubus adenotrichus) by high-performance liquid chromatography with diode array detection and electrospray ion trap mass spectrometry. Journal of Agricultural and Food Chemistry 2007; 55: 8616-8624.
18. Niessen WMA, Manini P and Andreoli R. Matrix effects in quantitative pesticide analysis using liquid chromatography-mass spectrometry. Mass Spectrometry Reviews 2006; 25: 881.
19. Ortelli D, Edder P and Corvi C. Multiresidue analysis of 74 pesticides in fruits and vegetables by liquid chromatography-electrospray-tandem mass spectrometry. Analytica Chimica Acta 2004; 520: 33-45.
20. Pang GF, Liu YM, Fan CL, Zhang JJ, Cao YZ, Li XM, Li ZY, Wu YP and Guo TT. Simultaneous determination of 405 pesticide residues in grain by accelerated solvent extraction then gas chromatography-mass spectrometry or liquid chromatography-tandem mass spectrometry. Analytical and Bioanalytical Chemistry 2006; 384: 1366-1408.
21. Payá P, Anastassiades M, Mack D, Sigalova I, Tasdelen B, Oliva J and Barba A. Analysis of pesticide residues using the Quick Easy Cheap Effective Rugged and Safe (QuEChERS) pesticide multiresidue method in combination with gas and liquid chromatography and tandem mass spectrometric detection. Analytical and Bioanalytical Chemistry 2007; 389: 1697-1714.
22. Picó Y, Font G, Moltó JC and Mañes J. Pesticide residue determination in fruit and vegetables by liquid chromatography-mass spectrometry. Journal of Chromatography A 2000; 882: 153-173.
23. Picó Y, Font G, Ruiz MJ and Fernández M. Control of pesticide residues by liquid chromatography-mass spectrometry to ensure food safety. Mass Spectrometry Reviews 2006; 25: 917-960.
24. Saieva C, Aprea C, Tumino R, Masala G, Salvini S, Frasca G, Giurdanella MC, Zanna I, Decarli A, Sciarra G and Palli D. Twenty-four-hour urinary excretion of ten pesticide metabolites in healthy adults in two different areas of Italy (Florence and Ragusa). The Science of the Total Environment 2004; 332: 71-80.
25. Sancho JV, Pozo OJ, Zamora T, Grimalt S and Hernández F. Direct determination of paclobutrazol residues in pear samples by liquid chromatography-electrospray tandem mass spectrometry. Journal of Agricultural and Food Chemistry 2003; 51: 4202-4206.
26. Sancho JV, Ibáñez M, Grimalt S, Pozo ÓJ and Hernández F. Residue determination cyromazine and its metabolite melamine in chard samples by ion-pair liquid chromatography coupled to electrospray tandem mass spectrometry. Analytica Chimica Acta 2005; 530: 237-243.
27. Sannino A, Bolzoni L and Bandini M. Application of liquid chromatography with electrospray tandem mass spectrometry to the determination of a new generation of pesticides in processed fruits and vegetables. Journal of Chromatography A 2004; 1036: 161-169.
28. Sannino A. Determination of three natural pesticides in processed fruit and vegetables using high-performance liquid chromatography/tandem mass spectrometry. Rapid Communications in Mass Spectrometry 2007; 21: 2079-2086.
29. Schwedler DA, Thomas AD and Yeh LT. Determination of spinosad and its metabolites in food and environmental matrices. 2. Liquid chomatography-mass spectrometry. Journal of Agricultural and Food Chemistry 2000; 48: 5138-5145.
30. Sherma J. Pesticide residue analysis (1999-2000): a review. Journal of AOAC International 2001; 84: 1303-1312.
31. Taylor MJ, Hunter K, Hunter KB, Lindsay D and Le Bouhellec S. Multiresidue method for rapid screening and confirmation of pesticides in crude extracts of fruits and vegetables using isocratic liquid chromatography with electrospray tandem mass spectrometry. Journal of Chromatography A 2002; 982: 225-236.
32. Taylor PJ. Matrix effects: the Achilles heel of quantitative high-performance liquid chromatography-electrospray-tandem mass spectrometry. Clinical Biochemistry 2005; 38: 328-334.
33. Zrostlíková J, Hajslova J, Kovalczuk T, Stěpán R and Poustka J. Determination of seventeen polar/ thermolabile pesticides in apples and apricots by liquid chromatography/ mass spectrometry. Journal of AOAC International 2003; 86: 612-622.