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1
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0009283222
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R. Tacke, M. Mallak, R. Willeke, Angew. Chem. 2001, 113, 2401-2403;
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(2001)
Angew. Chem
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, pp. 2401-2403
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Tacke, R.1
Mallak, M.2
Willeke, R.3
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2
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0035907716
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Angew. Chem. Int. Ed. 2001, 40, 2339-2341.
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(2001)
Angew. Chem. Int. Ed
, vol.40
, pp. 2339-2341
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3
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0141974208
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R. Bertermann, A. Biller, M. Kaupp, M. Penka, O. Seiler, R. Tacke, Organometallics 2003, 22, 4104-4110.
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(2003)
Organometallics
, vol.22
, pp. 4104-4110
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Bertermann, R.1
Biller, A.2
Kaupp, M.3
Penka, M.4
Seiler, O.5
Tacke, R.6
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4
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28944433924
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O. Seiler, M. Büttner, M. Penka, R. Tacke, Organometallics 2005, 24, 6059-6062.
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(2005)
Organometallics
, vol.24
, pp. 6059-6062
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Seiler, O.1
Büttner, M.2
Penka, M.3
Tacke, R.4
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6
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34848895715
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D. Troegel, C. Burschka, S. Riedel, M. Kaupp, R. Tacke, Angew. Chem. 2007, 119, 7131-7135;
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(2007)
Angew. Chem
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, pp. 7131-7135
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Troegel, D.1
Burschka, C.2
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Kaupp, M.4
Tacke, R.5
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7
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34848824029
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Angew. Chem. Int. Ed. 2007, 46, 7001-7005.
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(2007)
Angew. Chem. Int. Ed
, vol.46
, pp. 7001-7005
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-
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8
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85153183494
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however, their identities have been established only by solution NMR spectroscopic studies: U. Herzog
-
The existence of two anionic pentacoordinate silicon(IV) complexes with SiS5 skeletons in solution has also been claimed;
-
5 skeletons in solution has also been claimed; however, their identities have been established only by solution NMR spectroscopic studies: U. Herzog, Main Group Met. Chem. 2001, 24, 757-759.
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(2001)
Main Group Met. Chem
, vol.24
, pp. 757-759
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-
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9
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85153318093
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2 skeletons has been claimed; however, the analytical evidence for this is rather poor, and some of the data reported are questionable: a) R. V. Singh, J. P. Tandon, Synth. React. Inorg. Met.-Org. Chem. 1981, 11, 109-131;
-
2 skeletons has been claimed; however, the analytical evidence for this is rather poor, and some of the data reported are questionable: a) R. V. Singh, J. P. Tandon, Synth. React. Inorg. Met.-Org. Chem. 1981, 11, 109-131;
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11
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85153184517
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Recent publications dealing with neutral penta- and hexacoordinate silicon compounds: a O. Seiler, C. Burschka, S. Metz, M. Penka, R. Tacke, Chem. Eur. J. 2005, 11, 7379-7386;
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Recent publications dealing with neutral penta- and hexacoordinate silicon compounds: a) O. Seiler, C. Burschka, S. Metz, M. Penka, R. Tacke, Chem. Eur. J. 2005, 11, 7379-7386;
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12
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29144449369
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b) R. Tacke, R. Bertermann, C. Burschka, S. Dragota, Angew. Chem. 2005, 117, 5426-5429;
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(2005)
Angew. Chem
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Tacke, R.1
Bertermann, R.2
Burschka, C.3
Dragota, S.4
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13
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24044521607
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Angew. Chem. Int. Ed. 2005, 44, 5292-5295;
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(2005)
Angew. Chem. Int. Ed
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, pp. 5292-5295
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14
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34447323100
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c) X. Kästele, P. Klüfers, R. Tacke, Angew. Chem. 2006, 118, 3286-3288;
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(2006)
Angew. Chem
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, pp. 3286-3288
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Kästele, X.1
Klüfers, P.2
Tacke, R.3
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15
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33746217400
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Angew. Chem. Int. Ed. 2006, 45, 3212-3214;
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(2006)
Angew. Chem. Int. Ed
, vol.45
, pp. 3212-3214
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16
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34447342548
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d) O. Seiler, C. Burschka, T. Fenske, D. Troegel, R. Tacke, Inorg. Chem. 2007, 46, 5419-5424;
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(2007)
Inorg. Chem
, vol.46
, pp. 5419-5424
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Seiler, O.1
Burschka, C.2
Fenske, T.3
Troegel, D.4
Tacke, R.5
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17
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34848879190
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e) S. Metz, C. Burschka, D. Platte, R. Tacke, Angew. Chem. 2007, 119, 7136-7139;
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(2007)
Angew. Chem
, vol.119
, pp. 7136-7139
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Metz, S.1
Burschka, C.2
Platte, D.3
Tacke, R.4
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18
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34848867177
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Angew. Chem. Int. Ed. 2007, 46, 7006-7009;
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(2007)
Angew. Chem. Int. Ed
, vol.46
, pp. 7006-7009
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19
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53849090990
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f) B. Theis, C. Burschka, R. Tacke, Chem. Eur. J. 2008, 14, 4618-4630;
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(2008)
Chem. Eur. J
, vol.14
, pp. 4618-4630
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Theis, B.1
Burschka, C.2
Tacke, R.3
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20
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53549102827
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g) G. González-García, J. A. Gutiérrez, S. Cota, S. Metz, R. Bertermann, C. Burschka, R. Tacke, Z. Anorg. Allg. Chem. 2008, 634, 1281-1286;
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(2008)
Z. Anorg. Allg. Chem
, vol.634
, pp. 1281-1286
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González-García, G.1
Gutiérrez, J.A.2
Cota, S.3
Metz, S.4
Bertermann, R.5
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22
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85153249668
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Selected reviews dealing with higher-coordinate silicon compounds: a R. R. Holmes, Chem. Rev. 1996, 96, 927-950;
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Selected reviews dealing with higher-coordinate silicon compounds: a) R. R. Holmes, Chem. Rev. 1996, 96, 927-950;
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23
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0000248075
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Eds, Z. Rappoport, Y. Apeloig, Wiley, Chichester
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b) V. Pestunovich, S. Kirpichenko, M. Voronkov in The Chemistry of Organic Silicon Compounds (Eds.: Z. Rappoport, Y. Apeloig), Wiley, Chichester, 1998, vol. 2, part 2, pp. 1447-1537;
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The Chemistry of Organic Silicon Compounds
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Pestunovich, V.1
Kirpichenko, S.2
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24
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0004286484
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Ed, K.-y. Akiba, Wiley-VCH, New York
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c) C. Chuit, R. J. P. Corriu, C. Reye in Chemistry of Hypervalent Compounds (Ed.: K.-y. Akiba), Wiley-VCH, New York, 1999, pp. 81-146;
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Chemistry of Hypervalent Compounds
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Chuit, C.1
Corriu, R.J.P.2
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77956750595
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d) R. Tacke, M. Pülm, B. Wagner, Adv. Organomet. Chem. 1999, 44, 221-273;
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Adv. Organomet. Chem
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Tacke, R.1
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Wiley, New York
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e) M. A. Brook, Silicon in Organic, Organometallic, and Polymer Chemistry, Wiley, New York, 2000, pp. 97-114;
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Brook, M.A.1
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7744237751
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Eds, P. Jutzi, U. Schubert, Wiley-VCH, Weinheim
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f) R. Tacke, O. Seiler in Silicon Chemistry: From the Atom to Extended Systems (Eds.: P. Jutzi, U. Schubert), Wiley-VCH, Weinheim, 2003, pp. 324-337;
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Silicon Chemistry: From the Atom to Extended Systems
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Tacke, R.1
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85153229950
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Selected recent publications dealing with higher-coordinate silicon compounds: a D. Gerlach, E. Brendler, T. Heine, J. Wagler, Organometallics 2007, 26, 234-240;
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Selected recent publications dealing with higher-coordinate silicon compounds: a) D. Gerlach, E. Brendler, T. Heine, J. Wagler, Organometallics 2007, 26, 234-240;
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c) Y. Liu, S. A. Steiner III, C. W. Spahn, I. A. Guzei, I. S. Toulokhonova, R. West, Organometallics 2007, 26, 1306-1307;
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Liu, Y.1
Steiner III, S.A.2
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Toulokhonova, I.S.5
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e) J. Wagler, D. Gerlach, G. Roewer, Inorg. Chim. Acta 2007, 360, 1935-1942;
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Wagler, J.1
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h) V. V. Negrebetsky, P. G. Taylor, E. P. Kramarova, A. G. Shipov, S. A. Pogozhikh, Y. E. Ovchinnikov, A. A. Korlyukov, A. Bowden, A. R. Bassindale, Y. I. Baukov, J. Organomet. Chem. 2008, 693, 1309-1320;
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J. Organomet. Chem
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Negrebetsky, V.V.1
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Korlyukov, A.A.7
Bowden, A.8
Bassindale, A.R.9
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i) K. Lippe, D. Gerlach, E. Kroke, J. Wagler, Inorg. Chem. Commun. 2008, 11, 492-496.
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Inorg. Chem. Commun
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38
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53549102288
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Würzburg, Germany, July 31-August 5, Book of Abstracts, Abstract P
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S. Metz, C. Burschka, R. Tacke, The 14th International Symposium on Organosilicon Chemistry/3rd European Organosilicon Days, Würzburg, Germany, July 31-August 5, 2005, Book of Abstracts, Abstract P 159, p. 202.
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The 14th International Symposium on Organosilicon Chemistry/3rd European Organosilicon Days
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Metz, S.1
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84949358525
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a) E. C. Alyea, A. Malek, P. H. Merrell, J. Coord. Chem. 1974, 4, 55-63;
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d) A. Salifoglou, A. Simopoulos, A. Kostikas, R. W. Dunham, M. G. Kanatzidis, D. Coucouvanis, Inorg. Chem. 1988, 27, 3394-3406;
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e) S. Sharma, R. K. Sharma, A. K. Rai, Y. Singh, J. Chem. Res. 2005, 457-460;
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g) J. Zhang, Y.-J. Lin, G.-X. Jin, Organometallics 2007, 26, 4042-4047.
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Zhang, J.1
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46
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85153207660
-
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VACP/MAS NMR spectroscopic studies of 11 failed.
-
VACP/MAS NMR spectroscopic studies of 11 failed.
-
-
-
-
47
-
-
85153181265
-
-
1H NMR signals of both isomers.
-
1H NMR signals of both isomers.
-
-
-
-
48
-
-
85153228934
-
-
3CN, and 8 are insoluble in water, they do not decompose during this separation step.
-
3CN, and 8 are insoluble in water, they do not decompose during this separation step.
-
-
-
-
49
-
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85153237253
-
-
In the crystal of 8, the molecule is disordered occupancy ratio 90%/10
-
In the crystal of 8, the molecule is disordered (occupancy ratio 90%/10%).
-
-
-
-
50
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85153236645
-
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2 or THF) failed.
-
2 or THF) failed.
-
-
-
-
51
-
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85153183146
-
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2) did not give any evidence for the existence of two different species.
-
2) did not give any evidence for the existence of two different species.
-
-
-
-
52
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-
0012294314
-
-
Ed, H. F. Holtzclaw Jr, McGraw-Hill, New York
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R. G. Neville, J. J. McGee in Inorganic Syntheses (Ed.: H. F. Holtzclaw Jr,), McGraw-Hill, New York, 1966, vol. VIII, pp. 23-31.
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Inorganic Syntheses
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-
-
Neville, R.G.1
McGee in, J.J.2
-
53
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85153256280
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Drying in vacuo over a longer period of time led to partial loss of the acetonitrile
-
Drying in vacuo over a longer period of time led to partial loss of the acetonitrile.
-
-
-
-
54
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-
85153243489
-
-
13C NMR shifts given are those of the major species.
-
13C NMR shifts given are those of the major species.
-
-
-
-
55
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0004150157
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University of Göttingen, Göttingen, Germany
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a) G. M. Sheldrick, SHELXS-97, University of Göttingen, Göttingen, Germany, 1997;
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(1997)
SHELXS-97
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Sheldrick, G.M.1
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57
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0004150157
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University of Göttingen, Göttingen, Germany
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G. M. Sheldrick, SHELXL-97, University of Göttingen, Göttingen, Germany, 1997.
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(1997)
SHELXL-97
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Sheldrick, G.M.1
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