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3-Pyridylmethyldiphenylphosphine and imidazol-1-yl- methyldiphenylphosphine were kindly donated by Shell Research and Technology center, Amsterdam, The Netherlands.
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46
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P-PO3 = 111 Hz) suggests that phosphite coordination to the rhodium is at the equatorial and apical position in fast exchange on the NMR spectroscopy time-scale. The phosphorus-signal of the phosphite is at rather low field (δ = 179.8 ppm) which is attributed to steric constraints, as is also found for several other phosphine-phosphite rhodium complexes.
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