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Volumn 3, Issue 2, 2001, Pages 205-215

Solid phase extraction purification of carboxylic acid products from 96-well format solution phase synthesis with DOWEX 1 x 8-400 formate anion exchange resin

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Indexed keywords

ARTICLE;

EID: 0008166837     PISSN: 15204766     EISSN: None     Source Type: Journal    
DOI: 10.1021/cc000086s     Document Type: Article
Times cited : (21)

References (44)
  • 6
    • 0034152278 scopus 로고    scopus 로고
    • (a) Recent multifaceted application: Ley, S. V.; Massi, A. J. Comb. Chem. 2000, 2, 104-107.
    • (2000) J. Comb. Chem. , vol.2 , pp. 104-107
    • Ley, S.V.1    Massi, A.2
  • 11
    • 0032537031 scopus 로고    scopus 로고
    • (a) Use of Amberlyst 21 (freebase tertiary amine) anion exchange resin for scavenging of HCl and carboxylic acids from a combinatorial acylation reaction: Suto, M. J.; Gayo-Fung, L. M.; Palanki, M. S. S.; Sullivan, R. Tetrahedron 1998, 54, 4141-4150.
    • (1998) Tetrahedron , vol.54 , pp. 4141-4150
    • Suto, M.J.1    Gayo-Fung, L.M.2    Palanki, M.S.S.3    Sullivan, R.4
  • 13
    • 0033515672 scopus 로고    scopus 로고
    • (a) Use of a mixed bed of DOWEX 50W x 8-200 strong acid cation exchange resin and Amberlite IRA-400 strong anion exchange resin to scavenge triethylammonium iodide: Boger, D. L.; Goldberg, J.; Andersson, C.-M. J. Org. Chem. 1999, 64, 2422-2427.
    • (1999) J. Org. Chem. , vol.64 , pp. 2422-2427
    • Boger, D.L.1    Goldberg, J.2    Andersson, C.-M.3
  • 14
    • 0032537038 scopus 로고    scopus 로고
    • (b) Use of Amberlyst A-15 calcium salt for the scavenging of tetrabutylammonium fluoride: Parlow, J. J.; Flynn, D. L. Tetrahedron 1998, 54, 4013-4031.
    • (1998) Tetrahedron , vol.54 , pp. 4013-4031
    • Parlow, J.J.1    Flynn, D.L.2
  • 15
    • 0000140378 scopus 로고    scopus 로고
    • (c) Use of Amberlite IRA-95 weak base (freebase tertiary amine) anion exchange resin to freebase catalytic quantities of tertiary amine HBr and HI salts: Ouyang, X.; Armstrong, R. W.; Murphy, M. M. J. Org. Chem. 1998, 63, 1027-1032.
    • (1998) J. Org. Chem. , vol.63 , pp. 1027-1032
    • Ouyang, X.1    Armstrong, R.W.2    Murphy, M.M.3
  • 20
    • 0031452355 scopus 로고    scopus 로고
    • Use of Amberlyst A-26 (hydroxide) anion exchange resin to effect combinatorial condensation and purification of 2,4-pyrrolidinones: Kulkarni, B. A.; Ganesan, A. Angew. Chem., Int. Ed. Engl. 1997, 36, 2454-2455.
    • (1997) Angew. Chem., Int. Ed. Engl. , vol.36 , pp. 2454-2455
    • Kulkarni, B.A.1    Ganesan, A.2
  • 22
    • 0006699970 scopus 로고    scopus 로고
    • Supelco, Supelco Park, Beliefonte, PA 16823-0048, Tel: 800-247-6628
    • Technical information bulletins on ion exchange chromatography. (a) Supelco Bulletin 910, Guide to Solid Phase Extraction, 1998. Supelco, Supelco Park, Beliefonte, PA 16823-0048, Tel: 800-247-6628.
    • (1998) Supelco Bulletin 910, Guide to Solid Phase Extraction
  • 24
    • 0041753276 scopus 로고    scopus 로고
    • Dow North America, P.O. Box 1206, Midland, MI 48641-1206, Tel: 800-447-4369
    • (c) DOWEX Fine Mesh Spherical Ion Exchange Resins, 1998. Dow North America, P.O. Box 1206, Midland, MI 48641-1206, Tel: 800-447-4369.
    • (1998) DOWEX Fine Mesh Spherical Ion Exchange Resins
  • 25
    • 0043256317 scopus 로고
    • Rohm and Haas, Philadelphia, PA 19105, Tel: 800-221-8992
    • (d) Rohm and Haas Ion Exchange Laboratory Guide, 1993. Rohm and Haas, Philadelphia, PA 19105, Tel: 800-221-8992.
    • (1993) Rohm and Haas Ion Exchange Laboratory Guide
  • 26
    • 0042253905 scopus 로고
    • Aldrich Chemical Co., Milwaukee, WI 53233, Tel: 800-231-8327
    • (e) Aldrich Technical Information Bulletin No. 142, 1987. Aldrich Chemical Co., Milwaukee, WI 53233, Tel: 800-231-8327.
    • (1987) Aldrich Technical Information Bulletin No. 142 , vol.142
  • 30
    • 0043256314 scopus 로고    scopus 로고
    • The usefulness of resin K in its freebase form has already been demonstrated for the scavenging of HCl and carboxylic acids; see ref 3
    • The usefulness of resin K in its freebase form has already been demonstrated for the scavenging of HCl and carboxylic acids; see ref 3.
  • 39
    • 0042755172 scopus 로고    scopus 로고
    • note
    • The LiCl additive was only necessary in the reaction with tributyl(vinyl)tin. In its absence, the vinyl coupling did not go to completion. While the mechanism for why LiCl is beneficial in some Stille couplings is still unclear, it has been seen previously to aid in driving reactions to completion; see refs 15b, 15e, and 15f.
  • 43
    • 0042755171 scopus 로고    scopus 로고
    • note
    • It is convenient to transfer ion exchange resin into 96-well plates as a 3:1 water:resin slurry using a Labsystems 12 channel (50-300 μL) Finnpipette fitted with Geno-DNA-Tip S 10-200 μL polypropylene pipette tips.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.