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1
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0028243847
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-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünn efeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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Gallop, M.A.1
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Dower, W.J.3
Fodor, S.P.A.4
Gordon, E.M.5
-
2
-
-
0029065615
-
-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünn efeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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Terrett, N.K.1
Gardner, M.2
Gordon, D.W.3
Kobylecki, R.J.4
Steele, J.5
-
3
-
-
7044263277
-
-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünn efeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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Thompson, L.A.1
Ellman, J.A.2
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4
-
-
0000074870
-
-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünn efeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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-
-
Gordon, E.M.1
Gallop, M.A.2
Patel, D.V.3
-
5
-
-
21344450014
-
-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünn efeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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, vol.61
, pp. 171
-
-
Rinnova, M.1
Lebl, M.2
-
6
-
-
0030477258
-
-
Solid phase: a) Gallop, M. A.; Barrett, R. W.; Dower, W. J.; Fodor, S. P. A.; Gordon, E. M. J. Med. Chem. 1994, 37, 1233 and 1386. b) Terrett, N. K.; Gardner, M.; Gordon, D. W.; Kobylecki, R. J.; Steele, J. Tetrahedron 1995, 51, 8135. c) Thompson, L. A.; Ellman, J. A. Chem. Rev. (Washington, D.C.) 1996, 96, 555. d) Gordon, E. M.; Gallop, M. A.; Patel, D. V. Acc. Chem. Res 1996, 29, 144. e) Rinnova, M.; Lebl, M. Collect. Czech. Chem. Commun. 1996, 61, 171. f) Balkenhohl, F.; von dem Bussche-Hünnefeld, C.; Lansky, A.; Zechel, C. Angew. Chem., Int. Ed. Engl. 1996, 35, 2288.
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(1996)
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, pp. 2288
-
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Balkenhohl, F.1
Von dem Bussche-Hünnefeld, C.2
Lansky, A.3
Zechel, C.4
-
7
-
-
0030565531
-
-
Soluble polymers: a) Jung, K. W.; Zhao, X. Y.; Janda, K. D. Tetrahedron Lett. 1996, 37, 6491. b) Han, H. S.; Janda, K. D. J. Am. Chem. Soc. 1996, 118, 7632.
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Jung, K.W.1
Zhao, X.Y.2
Janda, K.D.3
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8
-
-
0029784123
-
-
Soluble polymers: a) Jung, K. W.; Zhao, X. Y.; Janda, K. D. Tetrahedron Lett. 1996, 37, 6491. b) Han, H. S.; Janda, K. D. J. Am. Chem. Soc. 1996, 118, 7632.
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-
-
Han, H.S.1
Janda, K.D.2
-
9
-
-
0029257836
-
-
Solution phase: a) Carell, T.; Wintner, E. A.; Sutherland, A. J.; Rebek, J., Jr.; Dunayevskiy, Y. M.; Vouros, P. Chemistry and Biology 1995, 2, 171. b) Boger, D. L.; Tarby, C. M.; Myers, P. L.; Caporale, L. H. J. Am. Chem. Soc. 1996, 118, 2109. c) Cheng, S.; Corner, D. D.; Williams, J. P.; Myers, P. L.; Boger, D. L. J. Am. Chem. Soc. 1996, 118, 2567.
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Carell, T.1
Wintner, E.A.2
Sutherland, A.J.3
Rebek Jr., J.4
Dunayevskiy, Y.M.5
Vouros, P.6
-
10
-
-
0029987185
-
-
Solution phase: a) Carell, T.; Wintner, E. A.; Sutherland, A. J.; Rebek, J., Jr.; Dunayevskiy, Y. M.; Vouros, P. Chemistry and Biology 1995, 2, 171. b) Boger, D. L.; Tarby, C. M.; Myers, P. L.; Caporale, L. H. J. Am. Chem. Soc. 1996, 118, 2109. c) Cheng, S.; Corner, D. D.; Williams, J. P.; Myers, P. L.; Boger, D. L. J. Am. Chem. Soc. 1996, 118, 2567.
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Boger, D.L.1
Tarby, C.M.2
Myers, P.L.3
Caporale, L.H.4
-
11
-
-
0029926720
-
-
Solution phase: a) Carell, T.; Wintner, E. A.; Sutherland, A. J.; Rebek, J., Jr.; Dunayevskiy, Y. M.; Vouros, P. Chemistry and Biology 1995, 2, 171. b) Boger, D. L.; Tarby, C. M.; Myers, P. L.; Caporale, L. H. J. Am. Chem. Soc. 1996, 118, 2109. c) Cheng, S.; Corner, D. D.; Williams, J. P.; Myers, P. L.; Boger, D. L. J. Am. Chem. Soc. 1996, 118, 2567.
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Cheng, S.1
Corner, D.D.2
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b) Dressman, B. A.; Spangle, L. A.; Kaldor, S. W. Tetrahedron Lett. 1996, 37, 937.
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Dressman, B.A.1
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18
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85034475347
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U.S. Patent no. 5,463,082, 1995
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b) Horváth, I. T.; Rábai, J., U.S. Patent no. 5,463,082, 1995.
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Horváth, I.T.1
Rábai, J.2
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20
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0005381744
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For new fluorous applications, see: a) Hughes, R. P.; Trujillo, H. A. Organomet. 1996, 15, 286. b) Di Magno, S. G.; Dussault, P. H.; Schultz, J. A. J. Am. Chem. Soc. 1996, 118, 5312. c) Pozzi, G.; Banfi, S.; Manfredi, A.; Montanari, F.; Quici, S. Tetrahedron 1996, 52, 11879.
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Hughes, R.P.1
Trujillo, H.A.2
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21
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0029898927
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For new fluorous applications, see: a) Hughes, R. P.; Trujillo, H. A. Organomet. 1996, 15, 286. b) Di Magno, S. G.; Dussault, P. H.; Schultz, J. A. J. Am. Chem. Soc. 1996, 118, 5312. c) Pozzi, G.; Banfi, S.; Manfredi, A.; Montanari, F.; Quici, S. Tetrahedron 1996, 52, 11879.
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Di Magno, S.G.1
Dussault, P.H.2
Schultz, J.A.3
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22
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0030565451
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For new fluorous applications, see: a) Hughes, R. P.; Trujillo, H. A. Organomet. 1996, 15, 286. b) Di Magno, S. G.; Dussault, P. H.; Schultz, J. A. J. Am. Chem. Soc. 1996, 118, 5312. c) Pozzi, G.; Banfi, S.; Manfredi, A.; Montanari, F.; Quici, S. Tetrahedron 1996, 52, 11879.
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Banfi, S.2
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Quici, S.5
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85034464590
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33644894918
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Interesting alternatives to the standard methyl and butyl reagents are available. For example, see: a) Vedejs, E.; Haight, A. R.; Moss, W. O. J. Am. Chem. Soc. 1992, 114, 6556. b) Brown, J. M.; Pearson, M.; Jastrzebski, J. T. B. H.; van Koten, G. J. Chem. Soc., Chem. Commun. 1992, 1440.
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0002448494
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Interesting alternatives to the standard methyl and butyl reagents are available. For example, see: a) Vedejs, E.; Haight, A. R.; Moss, W. O. J. Am. Chem. Soc. 1992, 114, 6556. b) Brown, J. M.; Pearson, M.; Jastrzebski, J. T. B. H.; van Koten, G. J. Chem. Soc., Chem. Commun. 1992, 1440.
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0000811923
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For a new separation and recyling procedure and references to other procedures, see: Crich, D.; Sun, S. R. J. Org. Chem. 1996, 61, 7200.
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58
-
-
85034481252
-
-
note
-
Most of the residual 10 - 20% remained in the organic phase. If desired, this can be removed by washing with FC-72, as shown in the Preparative procedure.
-
-
-
-
60
-
-
43949163594
-
-
See, Gronowitz, S.; Bjórk, P.; Malm, J.; Hórnfeldt, A.-B. J. Organomet. Chem. 1993, 460, 127. The yield problem can be solved by adding copper salts. This technique is likewise successful in the microwave variant of the fluorous Stille coupling (ref 12b).
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Gronowitz, S.1
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