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Volumn 12, Issue 10, 2001, Pages 1451-1458

C2-Symmetric sulfur derivatives of 2,2′,3,3′'-tetramethoxybiphenyl

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Indexed keywords


EID: 0001739569     PISSN: 09574166     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0957-4166(01)00247-6     Document Type: Article
Times cited : (12)

References (87)
  • 66
    • 84956073521 scopus 로고
    • Prepared in two steps in 80% overall yield, by known procedure: Horner, L.; Weber, K. H. Chem. Ber. 1963, 96, 1568.
    • (1963) Chem. Ber. , vol.96 , pp. 1568
    • Horner, L.1    Weber, K.H.2
  • 69
    • 10644289464 scopus 로고
    • When 2,2′-dilithium-1,1′-biphenyl was quenched with elemental sulfur, dibenzo[c,e][1,2]-dithiin was recovered in 50% yield: Delogu, G.; Cossu, S.; Fabbri, D.; Maglioli, P. Org. Prep. Proc. Int. 1991, 23, 455.
    • (1991) Org. Prep. Proc. Int. , vol.23 , pp. 455
    • Delogu, G.1    Cossu, S.2    Fabbri, D.3    Maglioli, P.4
  • 70
    • 85037284032 scopus 로고    scopus 로고
    • note
    • (a) HPLC analysis was performed at rt using a Chiracel OD column (10 μm, 25 cm×0.46 I.D.) at flow rate of 0.6 mL/min, 254 UV detection, using different mixtures (w:w) of n-hexane:propan-2-ol as mobile phase (b) Separation of biphenyl 6 in two enantiomers was performed by chiral HPLC using a Chiracel OD column with 98:2 hexane:propan-2-ol as mobile phase, at a flow rate of 0.6 mL/min and with UV detector at 254 nm.
  • 74
    • 33751385897 scopus 로고
    • We applied conditions that were developed successfully by us for resolution of BINOL and biphenols: Fabbri, D.; Delogu, G.; De Lucchi, O. J. Org. Chem. 1993, 58, 1748.
    • (1993) J. Org. Chem. , vol.58 , pp. 1748
    • Fabbri, D.1    Delogu, G.2    De Lucchi, O.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.