Preparation of spin-labeled styrene-divinylbenzene copolymers and a new approach for quantitative determination of the resin loading using ESR spectroscopy

Tetrahedron Letters

Volumn 40, Issue 3, 1999, Pages 407-410

  Katritzky, Alan R ^a   Belyakov, Sergei A ^a   Strah, Sonja ^a   Cage, Brant ^b   Dalal, Naresh S ^b  

^a University of Florida ^*  (United States)

^b FLORIDA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

COPOLYMER; FREE RADICAL; RESIN; STYRENE; STYRENE DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; ELECTRON SPIN RESONANCE; SPIN LABELING; SYNTHESIS;

EID: 0033555261     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)02382-X     Document Type: Article

References (11)

1. Fitch, W. L. Analytical methods for the Quality Control of Combinatorial Libraries. In Annual Reports in Combinatorial Chemistry and Molecular Diversity, Volume 1; Moos, W. H.; Pavia, M. R.; Kay, B. K.; Ellington, A. D., Eds.; ESCOM Science Publishers: Leiden, 1997, 59-68.
2. Xiao, X.-y.; Nova, M. P. In Combinatorial Chemistry: Synthesis and Application; Wilson, S. R.; Czarnik, A. W., Eds.; John Wiley & Sons, Inc.: New York, 1997, 135-152.
3. Geysen, H. M.; Wagner, C. D.; Bodnar, W. M.; Markworth, C. J.; Parke, G. J.; Schoenen, F. J.; Wagner, D. S.; Kinder, D. S. Chem. Biol. 1996, 3, 679-688.
4. Nicolaou, K. C.; Xiao, X.-Y.; Parandoosh, Z.; Senyei, A.; Nova, M. P. Angew. Chem., Int. Ed. Engl. 1995, 34, 2289-2291.
5. Cilli, E. M.; Marchetto, R.; Schreier, S.; Nakaie, C. R. Tetrahedron Lett. 1997, 38, 517-520.
6. Winter, H.; Gotschy, B.; Dormann, E.; Naarmann, H. Synth. Met. 1990, 38, 341-352.
7. Hmyene, M.; Naarmann, H.; Winter, H.; Pilawa, B.; Dormann, E. J. Phys.: Condens. Matter 1994, 6, L511-L515.
8. Leznoff, C. C.; Dixit, D. M. Can. J. Chem. 1977, 55, 3351-3355.
9. 2 (5 x 30 mL) and dried in vacuum overnight to give resins 6 or 7.
10. Neugebauer, F. A.; Bernhardt, R. Chem. Ber. 1974, 707, 529-536.
11. Neugebauer, F. A. Angew. Chem., Int. Ed. Engl. 1973, 12, 455-464.