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Vinylepoxides 1a,b were obtained from the allylic alcohols using Sharpless asymmetric epoxidation followed by the Swern/Wittig procedure, see: Díez-Martin, D.; Kotecha, N. R.; Ley, S. L.; Mantegani, S.; Menéndez, J. C.; Organ, H. M.; White, A. D.; Banks, J. B. Tetrahedron 1992, 48, 7899-7938; was obtained from the corresponding dienol; for 1d, see: Weigand, S.; Brückner, R. Synlett 1997, 225-228. All vinylepoxides had ee > 95%.
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The stereochemistry was confirmed by converting amino alcohols 3, 5, and 6 into the corresponding oxazolidinones; see ref 18.
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