Rapid and automatable determination of ochratoxin A in wine based on microextraction by packed sorbent followed by HPLC-FLD

Food Control

Volumn 68, Issue , 2016, Pages 391-398

  Savastano, Maria Luisa ^a   Losito, Ilario ^b   Pati, Sandra ^a  

^a UNIVERSITY OF FOGGIA   (Italy)

^b UNIVERSITY OF BARI   (Italy)

Author keywords

Fluorescence detection; High performance liquid chromatography; Microextraction by packed sorbent; Ochratoxin A; Validation; Wine

Indexed keywords

EID: 84963575197     PISSN: 09567135     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodcont.2016.04.016     Document Type: Article

References (28)

1. Abdel-Rehim M. Recent advances in microextraction by packed sorbent for bioanalysis. Journal of Chromatography A 2010, 1217:2569-2580.
2. Abdel-Rehim M., Skansen P., Vita M., Hassan Z., Blomberg L., Hassan M. Microextraction in packed syringe/liquid chromatography/electrospray tandem mass spectrometry for quantification of ololoucine in human plasma samples. Analytica Chimica Acta 2005, 539:35-39.
3. Altun Z., Abdel-Rehim M., Blomberg L.G. New trends in sample preparation: on-line microextraction in packed syringe (MEPS) for LC and GC applications. Part III: determination and validation of local anaesthetics in human plasma samples using a cation-exchange sorbent, and MEPS-LC-MS-MS. Journal of Chromatography B 2004, 813:129-135.
4. Aresta A., Vatinno R., Palmisano F., Zambonin C.G. Determination of Ochratoxin A in wine at sub ng/mL levels by solid-phase microextraction coupled to liquid chromatography with fluorescence detection. Journal of Chromatography A 2006, 1115:196-201.
5. Battiliani P., Logrieco A., Giorni P., Cozzi G., Bertuzzi T., Pietri A. Ochratoxin A production by Aspergillus carbonarius on some grape vareties grown in Italy. Journal of the Science of Food and Agricolture 2004, 84:1736-1740.
6. Battiliani P., Magan N., Logrieco A. European research on ochratoxin A in grapes and wine. International Journal of Food Microbiology 2006, 111:S2-S4.
7. Bau M., Bragulat M.R., Abarca M.L., Minguez S., Cabañes F.J. Ochratoxin A producing fungi from Spanish vineyards. Advances in Experimental Medicine and Biology 2005, 571:173-179.
8. Bellver Soto J., Fernández-Franzón M., Ruiz M.-J., Juan-García A. Presence of ochratoxin a (OTA) mycotoxin in alcoholic drinks from southern European countries: wine and beer. Journal of Agricultural and Food Chemistry 2014, 62:7643-7651.
9. Bertuzzi T., Rastelli S., Mulazzi A., Donadini A.P. Mycotoxin occurrence in beer produced in several European countries. Food Control 2011, 22:2059-2064.
10. Brera C., Debegnach F., Minardi V., Prantera E., Pannunzi E., Faleo S., et al. Ochratoxin A contamination in Italian wine samples and evaluation of the exposure in the Italian population. Journal of Agricultural and Food Chemistry 2008, 56:10611-10618.
11. Covarelli L., Beccari G., Marini A., Tosi L. A review on the occurrence and control of ochratoxigenic fungal species and ochratoxin A in dehydrated grapes, non-fortified dessert wines and dried vine fruit in the Mediterranean area. Food Control 2012, 26:347-356.
12. Delage N., d'Harlingue A., Colonna Ceccaldi B., Bompeix G. Occurrence of mycotoxins in fruit juices and wine. Food Control 2003, 14:225-227.
13. Duarte S.C., Pena A., Lino C.M. A review on ochratoxin A occurrence and effects of processing of cereal and cereal derived food products. Food Microbiology 2010, 27:187-198.
14. EC Commission Regulation (EC) No. 401/2006, laying down the methods of sampling and analysis for the official control of the levels of mycotoxins in foodstuffs. Official Journal of the European Union 2006, L70:12-34.
15. EC Commission Regulation (EC) No. 1881/2006, setting maximum levels for certain contaminants in foodstuff. Official Journal of the European Communities 2006, L364:5-24.
16. EFSA Opinion of the Scientific Panel on Contaminants in the Food chain on a request from the commission related to ochratoxin A in food. The EFSA Journal 2006, 365:1-56.
17. El-Beqqali A., Kussak A., Abdel-Rehim M. Fast and sensitive environmental analysis utilizing microextraction in pace syringe online with gas chromatography-mass spectrometry. Determination of polycyclic aromatic hydrocarbons in water. Journal of Chromatography A 2006, 1114:234-238.
18. Gil-Serna J., Patiño B., Cortes L., Gonzalez-Jaen M.T., Vazquez C. Aspergillus steynii and Aspergillus westerdijkiaeas potential risk of OTA contamination in food products in warm climates. Food Microbiology 2015, 46:168-175.
19. Gonçalves J., Mendes B., Silva C.L., Câmara J.S. Development of a novel microextraction by packed sorbent-based approach followed by ultrahigh pressure liquid chromatography as a powerful technique for quantification phenolic constituents of biological interest in wines. Journal of Chromatography A 2012, 1229:13-23.
20. Hernández M.J., García-Moreni M.V., Durán E., Guillén D., Barroso C.G. Validation of two analytical methods for the determination of ochratoxin A by reversed-phased high-performance liquid chromatography coupled to fluorescence detection in musts and sweet wines from Andalusia. Analytica Chimica Acta 2006, 566:117-121.
21. IARC IARC monographs on the evaluation of carcinogenic risks to humans. Some naturally occurring substance: food items and constituents, heterocyclic aromatic amines and mycotoxins. Summary of data reported and evaluation. IARC Science Publication 1993, 56:489-521.
22. Miraglia M., Brera C. Assessment of dietary intake of ochratoxin A by the population of EU member states. Reports on tasks for scientific cooperation. Report of experts participating in SCOOP Task 3.2.7 2002, Directorate General Health and Consumer Protection, Rome, Italy.
23. OIV International Organisation of Vine and Wine, Resolution Oeno 16/2001 (revised by Oeno, 349-2011) 2001.
24. Otteneder H., Majerus P. Occurrence of ochratoxin A (OTA) in wines: influence of the type of wine and its geographical origin. Food Additives and Contaminants 2000, 17:793-798.
25. Quinto M., Spadaccino G., Nardiello D., Palermo C., Amodio P., Li D., et al. Microextraction by packed sorbent coupled with gas chromatography-mass spectrometry: a comparison between "draw-eject" and "extract-discard" methods under equilibrium conditions for the determination of polycyclic aromatic hydrocarbons in water. Journal of Chromatography A 2014, 1371:30-38.
26. Saracino M.A., Iacono C., Somaini L., Gerra G., Ghedini N., Raggi M.A. Multi-matrix assay of cortisol, cortisone and corticosterone using a combined MEPS-HPLC procedure. Journal of Pharmaceutical and Biomedical Analysis 2014, 88:643-648.
27. Visconti A., Pascale M., Centonze G. Determination of ochratoxin A in wine by means of immunoaffinity column clean-up and high-performance liquid chromatography. Journal of Chromatography A 1999, 864:89-101.
28. Wei Y., Longhui Q., Yu C.C.J., Lai E.P.C. Molecularly imprinted solid phase extraction in a syringe needle packed with polypyrrole-encapsulated carbon nanotubes for determination of ochratoxin a in red wine. Food Science and Technology International (London UK) 2007, 13:375-380.