In situ deformation and breakage of silica particles inside a SEM

Procedia Engineering

Volumn 102, Issue , 2015, Pages 201-210

  Romeis, Stefan ^a   Paul, Jonas ^a   Herre, Patrick ^a   Hanisch, Mathias ^a   Taylor, Robin N Klupp ^a   Schmidt, Jochen ^a   Peukert, Wolfgang ^a  

^a UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

Author keywords

heat treatment; in situ manipulation; mechanical properties; St ber silica; Submicron particles

Indexed keywords

CRACKS; DEFORMATION; ELASTIC MODULI; HEAT TREATMENT; MECHANICAL PROPERTIES; SCANNING ELECTRON MICROSCOPY; SILICA; STRUCTURAL PROPERTIES;

BRITTLE TO DUCTILE TRANSITION; FREE-STANDING STRUCTURES; MECHANICAL CHARACTERIZATIONS; MICRON-SIZED PARTICLES; STRUCTURE PROPERTY RELATIONSHIPS; SUB-MICRON PARTICLES; SUB-MICRON SIZE RANGE; TREATMENT TEMPERATURE;

FUSED SILICA;

EID: 84939778195     PISSN: 18777058     EISSN: 18777058     Source Type: Conference Proceeding    
DOI: 10.1016/j.proeng.2015.01.128     Document Type: Conference Paper

References (27)

1. D. Dingley A simple straining stage for the scanning electron microscope Micron 1 1969 206 210
2. H. Bangert, A. Wagendristel, and H. Aschinger Ultramicrohardness tester for use in a scanning electron-microscope Colloid. Polym. Sci. 259 1981 238 240
3. H. Bangert, A. Wagendristel, and H. Aschinger Ultra microhardness-measurements on thin-films, fibers and finely structured surfaces Vakuum-Tech. 31 1982 200 203
4. R. Rabe, J.-M. Breguet, P. Schwaller, S. Stauss, F.J. Haug, J. Patscheider, and J. Michler Observation of fracture and plastic deformation during indentation and scratching inside the scanning electron microscope Acta Metall. 469-470 2004 206 213
5. B. Moser, J. Kuebler, H. Meinhard, W. Muster, and J. Michler Observation of Instabilities during Plastic Deformation by in-situ SEM Indentation Experiments Adv. Eng. Mater 7 2005 388 392
6. R. Ghisleni, K.A. Rzepiejewska-Malyska, L. Philippe, P. Schwaller, and J. Michler In Situ SEM Indentation Experiments: Instruments Methodology, and Applications. Microsc. Res. Tech. 72 2009 242 249
7. H. Huang, H. Zhao, J. Mi, J. Yang, S. Wan, L. Xu, and Z. Ma A novel and compact nanoindentation device for in situ nanoindentation tests inside the scanning electron microscope AIP. Advances. 2 2012 p12104
8. T. Motoki, W. Gao, S. Kiyono, and T. Ono A nanoindentation instrument for mechanical property measurement of 3D micro/nano-structured surfaces Meas. Sci. Technol. 17 2006 495 499
9. D.S. Gianola, A. Sedlmayr, R. Moenig, C.A. Volkert, R.C. Major, E. Cyrankowski, S.A.S. Asif, O.L. Warren, and O. Kraft In situ nanomechanical testing in focused ion beam and scanning electron microscopes Rev. Sci. Instrum 82 2011 p63901
10. K.A. Rzepiejewska-Malyska, G. Buerki, J. Michler, R.C. Major, E. Cyrankowski, S.A.S. Asif, and O.L. Warren In situ mechanical observations during nanoindentation inside a high-resolution scanning electron microscope J. Mater. Res 23 2008 1973 1979
11. K.A. Rzepiejewska-Malyska, W.M. Mook, M. Parlinska-Wojtan, J. Hejduk, and J. Michler In situ scanning electron microscopy indentation studies on multilayer nitride films: Methodology and deformation mechanisms J. Mater. Res 24 2009 1208 1221
12. R. Legros, D.S. Gianola, and C. Motz Quantitative In Situ Mechanical Testing in Electron Microscopes MRS Bull 35 2010 354 360
13. S. Romeis, J. Paul, M. Ziener, and W. Peukert A novel apparatus for in situ compression of submicron structures and particles in a high resolution SEM Rev. Sci. Instrum 83 2012 p95105
14. J. Paul, S. Romeis, J. Tomas, and W. Peukert A review of models for single particle compression and their application to silica microspheres Adv. Powder. Technol. 25 2014 136 153
15. W. Stöber, A. Fink, and E. Bohn Controlled growth of monodisperse silica spheres in the micron size range J. Colloid Interf. Sci. 26 1968 62 69
16. S. Romeis, J. Paul, M. Hanisch, V.R.R. Marthala, M. Hartmann, R.N. Klupp Taylor, J. Schmidt, and W. Peukert Correlation of Enhanced Strength and Internal Structure for Heat-Treated Submicron Stöber Silica Particles Part. Part. Syst. Charact 2014
17. K. Zheng, C. Wang, Y.Q. Cheng, Y. Yue, X. Han, Z. Zhang, Z. Shan, S.X. Mao, M. Ye, Y. Yin, and E. Ma Electron-beam-assisted superplastic shaping of nanoscale amorphous silica Nat. Commun. 1 2010 1 8
18. H. Hertz Über die Berührung fester elastischer Körper J. Reine Angew. Math. 92 1882 156 171
19. W.R. Chang, I. Etsion, and D.B. Bogy An Elastic-Plastic Model for the Contact of Rough Surfaces J. Tribol 109 1987 p257
20. I. Etsion, Y. Kligerman, and Y. Kadin Unloading of an elastic-plastic loaded spherical contact Int. J. Solids Struct. 42 2005 3716 3729
21. P. McMillan, and R.L. Remmele Hydroxyl sites in SiO2 glass; a note on infrared and Raman spectra Amercian Mineralogist 1986 772 778
22. S.K. Sharma, J.F. Mammone, and M.F. Nicol Raman investigation of ring configurations in vitreous silica Nature 292 1981 140 141
23. F. Galeener Planar rings in glasses Solid State Communications 44 1982 1037 1040
24. T. Takamura, H. Yoshida, and K. Inazuka Infrared characteristic bands of highly dispersed silica Kolloid Z. Z. Polym. 195 1964 12 16
25. E.I. Kamitsos, A.P. Patsis, and G. Kordas Infrared-reflectance spectra of heat-treated sol-gel-derived silica Phys. Rev. B 48 1993 12499 12505
26. K. Schönert, and K. Steier Die Grenze der Zerkleinerung bei kleinen Korngrößen Chemie Ing. Techn 43 1971 773 777
27. K. Kendall The impossibility of comminuting small particles by compression Nature 272 1978 710 711